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GB/T 20082-2006Hydraulic fluid power -- Fluid contamination -- Determination of particulate contamination by the counting method using an optical microscope (English PDF)

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Issued by

General Administration of Quality Supervision, Inspection and Quarantine of the PRC

Level / Type

National · Recommended

Issue date

January 23, 2006

Implementation date

August 1, 2006

Scope

GB/T 20082-2006 (Hydraulic fluid power -- Fluid contamination -- Determination of particulate contamination by the counting method using an optical microscope) is available as an English-translated PDF.

GB/T 20082-2006 — This Standard specifies methods for determining the level of particulate contamination in liquids used in hydraulic systems by counting the number of particles deposited on the surface of a membrane filter using an optical microscope.

It includes particle counting by two manual methods and image analysis, using either transmitted or incident lighting systems. Particle sizes >= 2 µm can be sized and counted by this method, but the resolution and accuracy of the results will depend upon the optical system used and the capabilities of the operator.

All hydraulic fluids with a wide range of contamination levels can be analysed according to this Standard. However, the counting uncertainty at the larger particle sizes increases if the volume filtered is reduced to allow smaller sized particles to be counted, where a fine precipitate or a high particle concentration is present.

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Document preview — GB/T 20082-2006

National Standard of the People's Republic of China

ICS
23.100.60
Classification
J 20

Issued by: General Administration of Quality Supervision, Inspection and Quarantine of the PRC

Contents

  • Foreword...3
  • Introduction...4
  • 1 Scope...5
  • 2 Normative references...5
  • 3 Terms and definitions...6
  • 4 Counting principle...8
  • 5 Apparatus...9
  • 6 Reagents and chemicals...12
  • 7 Glassware cleaning procedure...12
  • 8 Calibration procedures...13
  • 9 Membrane filter preparation...14
  • 10 Particle sizing and counting procedure...18
  • 11 Expression of results...21
  • 12 Identification statement (Reference to this Standard)...21

Foreword

This Standard is identical to the international standard ISO 4407:2002

"Hydraulic fluid power - Fluid contamination - Determination of particulate

contamination by the counting method using an optical microscope" (English

edition).

For ease of use, this Standard makes the following modifications to ISO

4407:2002:

- ADD a view to Figure 1 and re-arrange the key;

- CHANGE Figure 3 to Table 2 and the "Note" of Figure 3 to the table note of

Table 2;

- For reference standards, replace international standards with

corresponding national standards.

This Standard was proposed by China Machinery Industry Federation.

This Standard shall be under the jurisdiction of National Technical Committee 3

on Hydraulic Pneumatics of Standardization Administration of China (SAC/TC

3).

Drafting organization of this Standard: China Aviation Industry Granularity

Measurement and Test Station.

Main drafters of this Standard: Lu Hong, Zhang Sufang, Guo Guixia, Wang Yan.

This Standard is first issued.

Hydraulic fluid power - Fluid contamination -

Determination of particulate contamination by the

counting method using an optical microscope

WARNING: The use of this Standard may involve hazardous materials,

operations and equipment. This Standard does not purport to address all

the safety problems associated with its use. It is the responsibility of the

user of this Standard to establish appropriate safety and health practices

and determine the applicability of regulative limitations prior to use.

1 Scope

This Standard specifies methods for determining the level of particulate

contamination in liquids used in hydraulic systems by counting the number of

particles deposited on the surface of a membrane filter using an optical

microscope. It includes particle counting by two manual methods and image

analysis, using either transmitted or incident lighting systems.

Particle sizes >= 2 µm can be sized and counted by this method, but the

resolution and accuracy of the results will depend upon the optical system used

and the capabilities of the operator.

All hydraulic fluids with a wide range of contamination levels can be analysed

according to this Standard. However, the counting uncertainty at the larger

particle sizes increases if the volume filtered is reduced to allow smaller sized

particles to be counted, where a fine precipitate or a high particle concentration

is present.

2 Normative references

The following documents contain provisions which, through reference in this

Standard, constitute provisions of this Standard. For the dated references, their

subsequent amendments (excluding corrections) or revisions do not apply to

this Standard. However, the parties who enter into agreement based on this

Standard are encouraged to investigate whether the latest editions of these

documents are applicable. For undated reference documents, the latest

editions apply to this Standard.

GB/T 12804 Laboratory glassware - Graduated measuring cylinders (GB/T

12804-1991, eqv ISO 4788:1980)

8.2.4 Unclamp, carefully remove the membrane filter from the base and

measure the diameter [effective filtration diameter (EFD)] of the stain in at least

two planes to within 0.1 mm. Average the at least two measurement results and

calculate the effective filtration area (EFA). Mark the funnel with a suitable code

and record the result in a suitable calibration recording system.

9 Membrane filter preparation

9.1 Sample preparation

9.1.1 After noting all sample identification details, remove any tied-up or loosely

attached labels ensuring that sample identity is retained. Thoroughly clean the

outside of the sample bottle, particularly around the cap, by washing with

filtered solvent.

9.1.2 If the sample has been standing for a period of time, particle settlement,

and hence agglomeration, will occur. It is essential that the agglomerates are

broken up, and the contaminant particles are re-dispersed evenly within the

contents of the sample before analysis.

9.1.3 Redistribute the contaminants within the contents of the bottle by either

hand shaking the sample vigorously for at least 1 min, or by using an acceptable

method of mixing such as a three-axis paint shaker for at least 5 min. The

method chosen should not alter the original distribution of the contaminant

9.1.4 If ultrasonic is used to break up any agglomerates, stand the sample

container so that the level of the liquid in the bath is either just below the fluid

level in the sample bottle, or 3/4 up the side of the container, whichever is least.

The period of immersion shall not exceed 1 min. Hand shake for 30 s afterwards.

9.2 Blank analysis

9.2.1 A blank analysis should be performed before each sample analysis,

unless it can be demonstrated that acceptable blanks can be consistently

obtained. If so, a blank analysis should be performed before starting a counting

programme and at least once during it.

9.2.2 Proceed as in 9.3, using solvent instead of sample liquid. Dispense a 100

mL volume of filtered solvent into the vacuum apparatus fitted with the selected

membrane filter, vacuum filter and aspirate to dryness.

9.2.3 Perform size analysis as specified in 10.3 at >= 5 µm. If the count at >= 5

µm exceeds the count levels given in the note below, this indicates insufficient

cleaning. Clean the apparatus again and repeat 9.2.2 to 9.2.3.

......

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 21 pages — is available in the English PDF.

Referenced standards

Normative references

GB/T 12804 · ISO 4788

Cited by

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