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GB/T 14699-2023Feed—Sampling (English PDF)

饲料 采样

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Issued by

State Administration for Market Regulation; Standardization Administration of China

Level / Type

National · Recommended

Issue date

August 6, 2023

Implementation date

March 1, 2024

Scope

GB/T 14699-2023 is the English-translated version of 饲料 采样.

GB/T 14699-2023 — This Standard specifies methods of sampling animal feeding stuffs, including fish feed, for quality control for commercial, technical and legal purposes. This Standard is not applicable to pet foods. Nor are the methods intended for sampling for the purpose of microbiological examination. Conditions of, and requirements for, sampling are specified separately for feeding stuffs of different physical natures. For certain categories of animal feeding stuff, specific methods of sampling are specified in other International Standards. A list of these can be found in the bibliography. Methods of sampling for the determination of substances likely to be non-uniformly distributed are described in Annex A.

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Document preview — GB/T 14699-2023

National Standard of the People's Republic of China

ICS
65.120
Classification
B20

Issued by: State Administration for Market Regulation; Standardization Administration of China

Contents

  • Foreword...3
  • 1 Scope...4
  • 2 Terms and Definitions...4
  • 3 General Principles...5
  • 4 Sampling Personnel...6
  • 5 Identification and General Inspection of the Lot Prior to Sampling...6
  • 6 Sampling Equipment...6
  • 7 Sample Containers...7
  • 8 Procedure...8
  • 9 Packing, Sealing and Marking of Samples and Sample Containers...20
  • 10 Sampling Report...21

Foreword

This Standard equivalently adopts the international standard ISO 6497.2002 Animal Feeding

Stuffs – Sampling.

This Standard made the following editorial modifications.

--- Change the standard name from "Animal Feeding Stuffs - Sampling" into "Feeding Stuffs

- Sampling";

--- Delete the "Foreword" and "Introduction" in the international Standard;

--- Change "this International Standard" into "this Standard";

--- Change the comma "," that serves as decimal point in the international standard into

decimal point ".".

This Standard replaced GB/T 14699.1-1993 Method for Sampling of Feed.

Annex A of this Standard is informative.

This Standard was jointly proposed by General Administration of Quality Supervision,

Inspection and Quarantine, and Ministry of Agriculture of PRC.

This Standard shall be under the jurisdiction of National Technical Committee on Feed Industry

of Standardization Administration of China.

Drafting organizations of this Standard. China National Feed Quality Inspection and Testing

Center (Beijing); and Feed Quality Inspection Center of the Ministry of Agriculture (Shenyang,

Jinan).

Chief drafting staffs of this Standard. Su Xiaoou, Chen Xin, Feng Zhonghua, Yang Shuming,

Li Xiangming, and Shao Chuanming.

Feeding Stuffs – Sampling

1 Scope

This Standard specifies methods of sampling animal feeding stuffs, including fish feed, for

quality control for commercial, technical and legal purposes.

This Standard is not applicable to pet foods. Nor are the methods intended for sampling for the

purpose of microbiological examination. Conditions of, and requirements for, sampling are

specified separately for feeding stuffs of different physical natures.

For certain categories of animal feeding stuff, specific methods of sampling are specified in

other International Standards. A list of these can be found in the bibliography. Methods of

sampling for the determination of substances likely to be non-uniformly distributed are

described in Annex A.

2 Terms and Definitions

For the purposes of this Standard, the following terms and definitions apply.

2.1 Consignment

A specified quantity of feeding stuff on offer, dispatched or received at one time.

NOTE. It may consist of one or more lots (see 2.2).

2.2 Lot

An identified quantity of a consignment having characteristics presumed to be uniform.

2.3 Increment

A quantity of material taken at one time from a single point in a lot.

2.4 Bulk sample

A quantity of material obtained by combining and mixing all the increments taken from the

same lot.

NOTE. A collection of distinct and identifiable increments intended for separate investigation may be

denoted the "gross sample".

2.5 Reduced sample

A representative part of the bulk sample, obtained by a process of successive division or

reduction in such a manner that the mass or volume approximates to that of the laboratory

samples.

2.6 Laboratory sample

A sample representative of the quality and condition of the lot, obtained by division of the

reduced sample and intended for analysis or other examination.

NOTE. For each sample taken, three or four laboratory samples are normally produced. One of these

should be submitted for testing and at least one stored for reference purposes. If more than four laboratory

samples are required, the quantity of the reduced sample will have to be increased so that the minimum

quantity requirement for all laboratory samples can be met.

3 General Principles

3.1 Representative sampling

The purpose of representative sampling is to obtain a small fraction from a lot in such a way

that a determination of any particular characteristic of this fraction will represent the mean value

of the characteristic of the lot.

3.2 Selective sampling

If portions of the material to be sampled show a noticeable difference in quality from the rest

of the material, such portions shall be separated from the material and treated as a separate lot.

In such cases, mention shall be made of this fact in the sampling report.

3.3 Statistical considerations

Acceptance sampling is the usual method of sampling for animal feeding stuffs. For sampling

by attributes, there is a theoretical sampling plan based on a binomial distribution, but, for

practical purposes, this plan has been simplified to a square-root relationship between the lot

size and the number of increments.

NOTE 1.With bulk products, sample variances can be expected to be acceptably uniform if, for lots up

to 2.5 tonnes, at least seven increments are taken and, for lots between 2.5 tonnes and 80 tonnes, the

number of increments taken is at least equal to sqrt20𝑚, where m is the mass, in tonnes, of the lot. If the

lot exceeds 80 tonnes, the square-root relationship is still applicable, but the risk of making incorrect

decisions on the basis of the samples increases. However, this can be the subject of agreement between

the interested parties.

NOTE 2.The application of the square-root relationship is somewhat different for the sampling of

packaged animal feeding stuffs, for liquids and semi-liquids, for blocks and licks and for roughages,

because the sample size may vary.

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — all pages — is available in the English PDF.

Referenced standards

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