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Issued by
State Administration for Market Regulation; Standardization Administration of China
Level / Type
National · Recommended
Issue date
August 6, 2023
Implementation date
March 1, 2024
Scope
GB/T 14699-2023 is the English-translated version of 饲料 采样.
GB/T 14699-2023 — This Standard specifies methods of sampling animal feeding stuffs, including fish feed, for quality control for commercial, technical and legal purposes. This Standard is not applicable to pet foods. Nor are the methods intended for sampling for the purpose of microbiological examination. Conditions of, and requirements for, sampling are specified separately for feeding stuffs of different physical natures. For certain categories of animal feeding stuff, specific methods of sampling are specified in other International Standards. A list of these can be found in the bibliography. Methods of sampling for the determination of substances likely to be non-uniformly distributed are described in Annex A.
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Document preview — GB/T 14699-2023
National Standard of the People's Republic of China
- ICS
- 65.120
- Classification
- B20
Issued by: State Administration for Market Regulation; Standardization Administration of China
Contents
- Foreword...3
- 1 Scope...4
- 2 Terms and Definitions...4
- 3 General Principles...5
- 4 Sampling Personnel...6
- 5 Identification and General Inspection of the Lot Prior to Sampling...6
- 6 Sampling Equipment...6
- 7 Sample Containers...7
- 8 Procedure...8
- 9 Packing, Sealing and Marking of Samples and Sample Containers...20
- 10 Sampling Report...21
Foreword
This Standard equivalently adopts the international standard ISO 6497.2002 Animal Feeding
Stuffs – Sampling.
This Standard made the following editorial modifications.
--- Change the standard name from "Animal Feeding Stuffs - Sampling" into "Feeding Stuffs
- Sampling";
--- Delete the "Foreword" and "Introduction" in the international Standard;
--- Change "this International Standard" into "this Standard";
--- Change the comma "," that serves as decimal point in the international standard into
decimal point ".".
This Standard replaced GB/T 14699.1-1993 Method for Sampling of Feed.
Annex A of this Standard is informative.
This Standard was jointly proposed by General Administration of Quality Supervision,
Inspection and Quarantine, and Ministry of Agriculture of PRC.
This Standard shall be under the jurisdiction of National Technical Committee on Feed Industry
of Standardization Administration of China.
Drafting organizations of this Standard. China National Feed Quality Inspection and Testing
Center (Beijing); and Feed Quality Inspection Center of the Ministry of Agriculture (Shenyang,
Jinan).
Chief drafting staffs of this Standard. Su Xiaoou, Chen Xin, Feng Zhonghua, Yang Shuming,
Li Xiangming, and Shao Chuanming.
Feeding Stuffs – Sampling
1 Scope
This Standard specifies methods of sampling animal feeding stuffs, including fish feed, for
quality control for commercial, technical and legal purposes.
This Standard is not applicable to pet foods. Nor are the methods intended for sampling for the
purpose of microbiological examination. Conditions of, and requirements for, sampling are
specified separately for feeding stuffs of different physical natures.
For certain categories of animal feeding stuff, specific methods of sampling are specified in
other International Standards. A list of these can be found in the bibliography. Methods of
sampling for the determination of substances likely to be non-uniformly distributed are
described in Annex A.
2 Terms and Definitions
For the purposes of this Standard, the following terms and definitions apply.
2.1 Consignment
A specified quantity of feeding stuff on offer, dispatched or received at one time.
NOTE. It may consist of one or more lots (see 2.2).
2.2 Lot
An identified quantity of a consignment having characteristics presumed to be uniform.
2.3 Increment
A quantity of material taken at one time from a single point in a lot.
2.4 Bulk sample
A quantity of material obtained by combining and mixing all the increments taken from the
same lot.
NOTE. A collection of distinct and identifiable increments intended for separate investigation may be
denoted the "gross sample".
2.5 Reduced sample
A representative part of the bulk sample, obtained by a process of successive division or
reduction in such a manner that the mass or volume approximates to that of the laboratory
samples.
2.6 Laboratory sample
A sample representative of the quality and condition of the lot, obtained by division of the
reduced sample and intended for analysis or other examination.
NOTE. For each sample taken, three or four laboratory samples are normally produced. One of these
should be submitted for testing and at least one stored for reference purposes. If more than four laboratory
samples are required, the quantity of the reduced sample will have to be increased so that the minimum
quantity requirement for all laboratory samples can be met.
3 General Principles
3.1 Representative sampling
The purpose of representative sampling is to obtain a small fraction from a lot in such a way
that a determination of any particular characteristic of this fraction will represent the mean value
of the characteristic of the lot.
3.2 Selective sampling
If portions of the material to be sampled show a noticeable difference in quality from the rest
of the material, such portions shall be separated from the material and treated as a separate lot.
In such cases, mention shall be made of this fact in the sampling report.
3.3 Statistical considerations
Acceptance sampling is the usual method of sampling for animal feeding stuffs. For sampling
by attributes, there is a theoretical sampling plan based on a binomial distribution, but, for
practical purposes, this plan has been simplified to a square-root relationship between the lot
size and the number of increments.
NOTE 1.With bulk products, sample variances can be expected to be acceptably uniform if, for lots up
to 2.5 tonnes, at least seven increments are taken and, for lots between 2.5 tonnes and 80 tonnes, the
number of increments taken is at least equal to sqrt20𝑚, where m is the mass, in tonnes, of the lot. If the
lot exceeds 80 tonnes, the square-root relationship is still applicable, but the risk of making incorrect
decisions on the basis of the samples increases. However, this can be the subject of agreement between
the interested parties.
NOTE 2.The application of the square-root relationship is somewhat different for the sampling of
packaged animal feeding stuffs, for liquids and semi-liquids, for blocks and licks and for roughages,
because the sample size may vary.
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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — all pages — is available in the English PDF.
Referenced standards
Cited by
- GB 7300.105-2025Feed additives - Part 1: Amino acids,their salts and analogues - Taurine
- GB 7300.1301-2025Feed additives - Part 13: Others - Bile acid
- GB 7300.205-2025Feed additives - Part 2: Vitamins, provitamins and chemically well-defined substances having similar effect - Riboflavin (Vitamin B2)
- GB 7300.206-2025Feed additives - Part 2: Vitamins,provitamins and chemically well-defined substances having similar effects - Choline chloride
- GB 7300.207-2025Feed additives - Part 2: Vitamins, provitamins and chemically well-defined substances having similar effects - Nicotinamide
- GB 7300.208-2025Feed additives - Part 2: Vitamins,provitamins and chemically well-defined substances having similar effects - Calcium L-Ascorbate
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