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GB/T 483-2007General rules for analytical and testing methods of coal (English PDF)

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Issued by

General Administration of Quality Supervision, Inspection and Quarantine (AQSIQ)

Level / Type

National · Recommended

Issue date

November 1, 2007

Implementation date

June 1, 2008

Scope

GB/T 483-2007 (General rules for analytical and testing methods of coal) is available as an English-translated PDF.

GB/T 483-2007 — This Standard specifies the following contents relevant to coal analysis test. terms and definitions, symbols, analysis test of coal sample, solution concentration, determination, test result expression, result conversion, method precision and test record.

This Standard is applicable to various coal analysis test method standards, documents, books and periodicals, teaching materials and manuals.

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Document preview — GB/T 483-2007

National Standard of the People's Republic of China

Classification
D 21

Issued by: General Administration of Quality Supervision, Inspection and Quarantine (AQSIQ)

Contents

  • Foreword...3
  • 1 Scope...5
  • 2 Normative References...5
  • 3 Terms and Definitions...6

Foreword

This Standard corresponds to BS 1016-100.1999 "Methods for Analysis and

Testing of Coal and Coke - Part 100.General Introduction and Methods for

Reporting Results" and ISO 1213-2.1992 "Solid Mineral Fuels - Vocabulary -

Part 2.Terms Relating to Sampling, Testing and Analysis". The consistency

degree of the standard and the above 2 standards is not equivalent. The main

differences are as follows.

- The technical contents of this Standard only include "3 Definition and Symbol",

"5 Result Report Basis" and "Result Expression" in BS 1016-100.1999.In

addition, "Coal Sample", "Determination" and "Solution Concentration" are

added.

- Some terms relevant to the coal analysis test in ISO 1213-2.1992 are adopted

as part of Terms and Definitions in this Standard. According to ISO 1213-2.1992

"Hard Coal and Coke - Mechanical Sampling - Part 1.General Introduction",

some terms and definitions in this Standard are modified.

This Standard replaces GB/T 483-1998 "General Rules for Analytical and

Testing Methods of Coal".

Compared with GB/T 483-1998, The following modifications are made in this

Standard.

- "Terms and Definitions" is added (Chapter 3 in this edition);

- "Method precision - the statistical calculation formula for the repeatability limit

and reproducibility critical difference" is added (Chapter 5 in Edition-1998;

Chapter 8 in this edition);

- The list of relevant standards is deleted in "Scope" (Chapter 1 in this edition).

This Standard was proposed by the China National Coal Association.

This Standard shall be under the jurisdiction of the National Technical

Committee on Coal of Standardization Administration of China.

Drafting organization of this Standard. the Coal Analysis Laboratory of Coal

Research Institute.

Chief drafting staffs of this Standard. Shi Yuying, and Duan Yunlong.

The previous editions replaced by this Standard are as follows.

- GB 483-1981, GB 483-1987, and GB/T 483-1998.

NATIONAL STANDARD

OF THE PEOPLE'S REPUBLIC OF CHINA

Replacing GB/T 483-1998

General Rules for Analytical and

Testing Methods of Coal

1 Scope

This Standard specifies the following contents relevant to coal analysis test.

terms and definitions, symbols, analysis test of coal sample, solution

concentration, determination, test result expression, result conversion, method

precision and test record.

This Standard is applicable to various coal analysis test method standards,

documents, books and periodicals, teaching materials and manuals.

2 Normative References

The following standards contain provisions which, through reference in this text,

constitute provisions of this Standard. For dated reference, subsequent

amendments (excluding correction) or revisions of these publications do not

apply. However, the parties who enter into agreement based on this Standard

are encouraged to investigate the possibility of applying the most recent editions

of the standards. For undated references, the latest edition of the normative

document referred to applies.

GB 474 Method for Preparation of Coal Sample

GB 475 Sampling for Commercial Coal

GB/T 6379.2 Accuracy (Trueness and Precision) of Measurement Methods

and Results Part 2.Basic Method for the Determination of Repeatability and

Reproducibility of a Standard Measurement Method (GB/T 6379.2-2004, ISO

5725-2.1994, IDT)

GB/T19494.1 Mechanical Sampling of Coal - Part 1.Method for Sampling

(GB/T 19494.1-2004, ISO 13909-1.2001, ISO 13909-2.2001, ISO

13909-3.2001, NEQ)

3 Terms and Definitions

For the purpose of this Standard, the following terms and definitions apply.

3.1 Terms and Definitions for Coal Sampling and Sample Preparation

3.1.1 Coal sample

A portion of representative coal taken out of coal for determining some features

of coal.

3.1.2 Seam-sample of coal

Coal sample taken from one seam in the excavating working face, exploring

tunnel or gallery as required.

3.1.10 Common sample of coal

Coal sample taken for multiple tests.

3.1.11 Moisture sample of coal

Coal sample taken specifically for the determination of total moisture.

3.1.12 Air-dried sample of coal

Coal sample reaching air drying state.

3.1.13 General-analysis test sample of coal

Coal sample, crushed to the particle size less than 0.2mm, reaching the air

drying state and used for the determination of most physical and chemical

properties.

4 Coal Sample

4.1 Sampling and Preparation of Coal Sample

The coal sample for analysis test (hereinafter referred to as coal sample) is

taken according to GB/T 19494.1 or GB 474; and prepared according to GB/T

19494.2 or GB 475.

4.2 Preservation of Coal Sample

Moisture sample of coal shall be put in the non-absorbent and airtight sealed

container; general analysis test sample of coal shall be put in the tight vessel

after the sample reaches air-dried state.

4.3 Reserve Coal Sample

Reserve coal sample is taken separately in some stage of the original coal

sample preparation, and shall be in as less brokenness and division as possible

with the particle size and quality in accordance with the requirements of the

relevant standard(s).

5 Solution and Its Concentration

5.1 Solution

As for the solution applied in the coal analysis test, all the solutions with water as

the solvent are referred as "aqueous solution" shortened as "solution"; as for the

solution with other liquids as the solvent, the solvent name is put before

"solution", e.g. the solution with ethyl alcohol (or benzene) as the solvent is

referred to as "ethyl alcohol (or benzene) solution".

5.2 Solution Concentration

The following are the commonly applied solution concentration in coal analysis

tests.

5.2.3 Mass concentration

The solute mass divided by solution volume, expressed by gram per liter or its

multiple, fraction unit, e.g. g /L, mg/ml.

5.2.4 Volume ratio or mass ratio

Volume ratio or mass ratio between one reagent and another reagent (or water,

expressed by (V1+V2) or (m1+m2), e.g.

6 Determination

6.1 Determination Times

Except special requirements, two times of determination (it is generally duplicate

determination) shall be conducted on the same coal sample in the analysis test

for each item. If the difference value of two determination values does not

exceed repeatability limit T, the arithmetic mean of the determination values

shall be taken as the final result;

6.2 Moisture Determination Term

6.2.1 The total moisture shall be determined after the coal sample preparation;

if the determination cannot be conducted immediately, the coal sample shall be

weighed accurately and placed in the vessel required in Section 4.2 before the

determination conducted as soon as possible.

7 Expression of Test Result

7.1 Symbol for Result Expression

7.1.1 Item symbol

As for the coal analysis tests, the first letters or the abbreviations of the English

names for all the items of analysis tests are adopted, and the element symbols

or molecular formula of all the chemical constituents are taken as their

representative symbols.

7.1.2 Sub-item symbol

A further division of the item, expressed with the first letter or abbreviation of the

corresponding English name adopted and marked at the lower right hand corner

of the item symbol.

8 Method Precision

The precision of coal analysis test method is expressed by repeatability limit and

reproducibility critical difference.

9 Test Record and Test Report

9.1 Test Record

The test record shall be filled according to the specified format, terms, symbols,

and legal measurement units and shall include the following contents at least.

Item name and record number for analysis test;

9.2 Test Report

The test report shall be filled according to the specified format, terms, symbols,

and legal measurement units and shall include the following contents at least.

......

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 6 pages — is available in the English PDF.

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