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GB/T 1843-2008Plastics - Determination of izod impact strength (English PDF)

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Issued by

General Administration of Quality Supervision, Inspection and Quarantine of PRC

Level / Type

National · Recommended

Issue date

August 4, 2008

Implementation date

April 1, 2009

Scope

GB/T 1843-2008 (Plastics - Determination of izod impact strength) is available as an English-translated PDF.

GB/T 1843-2008 is the Chinese standard "Plastics - Determination of izod impact strength". Its scope clause reads: 1.1 This standard specifies the method for determining the plastic Izod impact strength under standard conditions, as well as various types of specimens and test types.

Different test parameters are specified according to the material, specimen, notch. 1.2 This method is used to study the impact behavior of the specified type of specimen under standard conditions.

It is used to evaluate the brittleness and toughness of the specimen under test conditions.

1.3 This standard applies to the following materials: - Rigid thermoplastic molding and extrusion materials, including filled and reinforced composite materials, as well as unfilled types; rigid thermoplastic sheets; - Rigid thermosetting molding materials, including filled and reinforced composite materials; rigid thermosetting sheets, including laminates; - Fiber-reinforced thermosetting and thermoplastic composites, including sheets containing unidirectional or non-unidirectional reinforcement materials such as felt, fabric, textile roving, chopped strands, composite reinforcements, rovings, milled fibers and sheet made from prepregs; - Thermotropic liquid crystal polymers.

1.4 This standard is not generally applicable to rigid foam materials and sandwich structures containing foam materials. Notched specimens are not generally applicable to long fiber reinforced composites or thermotropic liquid crystal polymers.

1.5 This standard applies to specimens molded to the selected size, specimens machined from the middle of standard multi-purpose specimens (see GB/T 11997), or specimens machined from finished or semi-finished products such as molded parts, laminates, extruded or cast sheets.

1.6 This standard specifies the preferred dimensions of the specimens. The results of tests with different notches or specimens prepared by different methods are not comparable.

Other factors, such as the energy of the device, the impact velocity, the state conditioning of the specimen, can also affect the test results. Therefore, when data comparison is required, these factors shall be carefully controlled and recorded.

1.7 This standard shall not be used as a basis for design. However, by testing at different temperatures, changing the notch radius and (or) thickness, and preparing specimens under different conditions, can obtain the information on typical properties of the material.

Its clauses include principle; devices; specimens; operation steps; calculation and expression of results. It was issued by the General Administration of Quality Supervision, Inspection and Quarantine of PRC on 2008-08-04 and took effect on 2009-04-01.

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Document preview — GB/T 1843-2008

National Standard of the People's Republic of China

ICS
83.080.01
Classification
G 32

Issued by: General Administration of Quality Supervision, Inspection and Quarantine of PRC

Contents

  • Foreword...3
  • 1 Scope...5
  • 2 Normative references...6
  • 3 Terms and definitions...7
  • 4 Principle...8
  • 5 Devices...8
  • 6 Specimens...8
  • 7 Operation steps...12
  • 8 Calculation and expression of results...13
  • 9 Precision...14
  • 10 Test report...14

1 Scope

1.1 This standard specifies the method for determining the plastic Izod impact strength under standard conditions, as well as various types of specimens and test types.

Different test parameters are specified according to the material, specimen, notch.

1.2 This method is used to study the impact behavior of the specified type of specimen under standard conditions. It is used to evaluate the brittleness and toughness of the specimen under test conditions.

1.3 This standard applies to the following materials:

- Rigid thermoplastic molding and extrusion materials, including filled and reinforced composite materials, as well as unfilled types; rigid thermoplastic sheets;

- Rigid thermosetting molding materials, including filled and reinforced composite materials; rigid thermosetting sheets, including laminates;

- Fiber-reinforced thermosetting and thermoplastic composites, including sheets containing unidirectional or non-unidirectional reinforcement materials such as felt, fabric, textile roving, chopped strands, composite reinforcements, rovings, milled fibers and sheet made from prepregs;

- Thermotropic liquid crystal polymers.

1.4 This standard is not generally applicable to rigid foam materials and sandwich structures containing foam materials. Notched specimens are not generally applicable to long fiber reinforced composites or thermotropic liquid crystal polymers.

1.5 This standard applies to specimens molded to the selected size, specimens machined from the middle of standard multi-purpose specimens (see GB/T 11997), or specimens machined from finished or semi-finished products such as molded parts, laminates, extruded or cast sheets.

1.6 This standard specifies the preferred dimensions of the specimens. The results of tests with different notches or specimens prepared by different methods are not comparable. Other factors, such as the energy of the device, the impact velocity, the state conditioning of the specimen, can also affect the test results. Therefore, when data comparison is required, these factors shall be carefully controlled and recorded.

1.7 This standard shall not be used as a basis for design. However, by testing at different temperatures, changing the notch radius and (or) thickness, and preparing specimens under different conditions, can obtain the information on typical properties of the material.

2 Normative references

The provisions in following documents become the provisions of this Standard through reference in this Standard. For the dated references, the subsequent amendments (excluding corrections) or revisions do not apply to this Standard; however, parties who reach an agreement based on this Standard are encouraged to study if the latest versions of these documents are applicable. For undated references, the latest edition of the referenced document applies.

GB/T 2918-1998 Plastics - Standard atmospheres for conditioning and testing (IDT

ISO 291:1997)

GB/T 5471-2008 Plastics - Compression moulding of test specimens of thermosetting materials (ISO 295:2004, IDT)

GB/T 9352-2008 Plastic - Compression moulding of test specimens of thermoplastic materials (ISO 293:2004, IDT)

GB/T 11997-2008 Plastic - Multipurpose test specimens (ISO3167:2002, IDT)

GB/T 17037.1-1997 Injection moulding of test specimens of thermoplastic materials

- Part 1: General principles and moulding of multipurpose and bar test specimens (IDT ISO294-1: 1996)

GB/T 21189-2007 Verification of pendulum impact-testing machines used for

Charpy Izod and tensile impact-testing of plastics (ISO13802: 1999, IDT)

ISO 1268 1) Fiber-reinforced plastics - Methods of producing test sheets - Part 1:

General conditions

ISO 2602:1980 Statistical interpretation of test results - Estimation of the mean -

Confidence interval

ISO 2818:1994 Plastics - Preparation of test specimens by machining

ISO 10724-1:1998 Plastics - Injection moulding of test specimens of thermosetting powder moulding compounds (PMCs) - Part 1: General principles and moulding of multipurpose test specimens

1 It is being revised into 11 parts.

4 Principle

A pendulum of known energy strikes a specimen supported as a vertical Izod once, to measure the energy absorbed when the specimen fails. The impact line is a fixed distance from the specimen fixture; for notched specimens, the distance from the impact line to the notch centerline is the fixed distance (see Figure 2).

5 Devices

5.1 Testing machine

5.1.1 For the principle, characteristics, identification of the testing machine, please refer

to GB/T 21189-2007.

5.1.2 Some plastics are very sensitive to clamping force. When testing such materials, a standardized clamping force method shall be used and the clamping force shall be noted in the test report. The clamping force can be controlled by a calibrated torque wrench or a pneumatic or hydraulic device on the screw tightened by the vise.

5.2 Micrometer and gauge

Measure the main dimensions of the specimen, using a micrometer or gauge which has an accuracy of 0.02 mm. In order to measure the dimension of the notched specimen bN, a measuring probe which has a width of 2 mm ~ 3 mm and a shape suitable for the shape of the notch shall be installed on the micrometer.

6 Specimens

6.1 Preparation

6.1.1 Molded and extruded materials

The materials shall be prepared in accordance with the relevant material standards. If there is no such standard or otherwise specified, the specimens shall be directly compression molded or injection molded in accordance with the corresponding standards of GB/T 9352-2008, GB/T 17037.1-1997, GB/T 5471-2008 or ISO 10724-

1:1998, or machined from compression molded or injected sheets. The specimens may also be cut from type A multi-purpose specimens conforming to GB/T 11997-2008.

6.1.2 Sheets

The specimens shall be machined from sheets in accordance with ISO 2818:1994, using type A notches whenever possible. During testing, the machined surface of the unnotched specimen shall not be in tension.

material is to be obtained, specimens with notches of Type A and Type B shall be tested.

6.3.3 Sheets, including long fiber reinforced materials

The recommended thickness h is 4 mm. If the specimen is cut from a sheet or component, its thickness shall be the same as the original thickness of the sheet or component, which shall not exceed 10.2 mm.

When the thickness of the sheet is uniform and contains only one regularly distributed reinforcement material, when its thickness is greater than 10.2 mm, it shall be machined from one side of the sheet to 10.2 mm ± 0.2 mm. When testing unnotched specimens, in order to avoid surface effects, the original surface of the specimen shall be in tension during the test.

During the test, the side of the impact specimen is impacted; the impact direction is parallel to the plane of the sheet. Only when h = b = 10 mm can the test be carried out parallel or perpendicular to the sheet surface (see Figure 1).

6.4 Number of specimens

6.4.1 Unless otherwise specified in the standard of the test material, a group of specimens shall be 10. When the coefficient of variation (see ISO 2602:1980) is less than 5%, 5 specimens can be tested.

6.4.2 If the laminated material is tested in the vertical and parallel directions, 10 specimens shall be tested in each direction.

6.5 State conditioning

Unless otherwise specified in the standard of the test material, the test shall be conditioned for at least 16 hours at 23 °C and 50% relative humidity in accordance with

GB/T 2918-1998, or according to the conditions agreed upon by the relevant parties.

The conditioning time of the notched specimen shall be calculated after the notch processing.

7 Operation steps

7.1 Unless the relevant parties agree to use other conditions, such as testing at high or low temperatures, the test shall be carried out in the same environment as the state conditioning.

7.2 Measure the thickness h and width b of the middle part of each specimen or the residual width bN of the notched specimen, accurate to 0.02 mm.

When the specimen is injection molded, it is not necessary to measure every specimen size. Just make sure that the dimensions are listed in Table 1 and only measure one specimen in a group. When using a multi-cavity mold, ensure that the dimensions of the specimens in each cavity are the same.

7.3 Determine whether the testing machine has a specified impact velocity and an appropriate energy range. The energy absorbed by the punched specimen shall be within

10% ~ 80% of the nominal energy of the pendulum. If more than one pendulum meets these requirements, the pendulum with the largest energy shall be selected.

7.4 Determine the friction loss and corrected absorbed energy according to GB/T

21189-2007.

7.5 Lift and lock the pendulum. Install the specimen as shown in Figure 1 and meet the requirements of 5.1.2. When measuring the notched specimen, the notch shall be on the side of the pendulum impact edge.

7.6 Release the pendulum. Record the impact energy absorbed by the specimen. Make

necessary corrections for its friction loss (see 7.4).

7.7 The following characters are used to name the four types of impact:

C - Complete failure: The specimen is broken into two or more sections.

H - Hinge failure: An incomplete failure in which the specimen is not connected by a very thin rigid surface.

P - Partial failure: Incomplete failure except hinge failure.

N - No failure: No failure, only bending deformation; stress whitening may occur.

8 Calculation and expression of results

8.1 Unnotched specimen

The Izod unnotched impact strength aiU is calculated according to formula (1), in kilojoule per square meter (kJ/m2):

Where:

Ec - Corrected specimen fracture absorption energy, in joule (J);

h - Specimen thickness, in millimeter (mm);

b - Specimen width, in millimeter (mm).

d) Description of the material properties and shape, i.e., finished product, semi- finished product, test piece or specimen, including main dimensions, shape, processing method, etc.;

e) Impact velocity;

f) Nominal energy of the pendulum;

g) If a uniform clamping force is used, indication of the clamping force (see 5.1.2);

h) Method of specimen preparation;

i) Direction of specimen cutting (if the material is a finished or semi-finished product);

j) Number of specimens;

k) Conditioning used and standard test environment, as well as special treatments required by the test material and product standards;

l) Type of failure observed;

m) Individual test results, as follows (see also Table 2):

1) Grouped into three types of failure:

C: Complete failure, including hinge failure H;

P: Partial failure;

N: No failure - no failure occurred.

2) Select the failure type that occurs most frequently and record the average value x of the impact strength of this failure type; record the corresponding failure type with the letter C or P;

3) If the most common failure type is N, only record the letter N;

4) For the failure type that occurs less frequently, add the letter C, P or N between the two brackets, only when the number of occurrences is higher than 1/3 (otherwise insert a "*" sign).

n) Standard deviation of the mean value if necessary;

o) Test date.

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 14 pages — is available in the English PDF.

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