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GB/T 23349-2020Determination of arsenic,cadmium,chromium,lead and mercury contents for fertilizers (English PDF)

肥料中砷、镉、铬、铅、汞含量的测定

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

November 19, 2020

Implementation date

June 1, 2021

Scope

GB/T 23349-2020 is the English-translated version of 肥料中砷、镉、铬、铅、汞含量的测定.

GB/T 23349-2020 sets the methods for determining the arsenic, cadmium, chromium, lead and mercury contents of fertilizers. It gives the test methods for each element, among them silver diethyldithiocarbamate spectrophotometry and atomic fluorescence spectrometry for arsenic, with their detection limits.

It applies to the determination of these five elements in fertilizers. Fertilizer producers, testing laboratories and market regulators use it. Issued on 19 November 2020, it has applied since 1 June 2021, replacing GB/T 23349-2009.

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Document preview — GB/T 23349-2020

National Standard of the People's Republic of China

ICS
65.080
Classification
G 20
Replacing
GB/T 23349-2009

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Foreword
  • 1 Scope
  • 2 Normative references
  • 3 Test method

Foreword

This standard was drafted in accordance with the rules given in GB/T 1.1-2009.

This standard replaces GB/T 23349-2009 "Ecological indicators of arsenic, cadmium, lead, chromium, and mercury in fertilizers". Compared with GB/T 23349-2009, In addition to editorial changes, the main technical changes are as follows.

---The detection limit of the method has been increased (see Chapter 1);

---Deleted limit requirements and inspection rules (see Chapter 3 and Chapter 5 of the 2009 edition);

---The atomic fluorescence spectrometry method of arsenic and mercury has been added (see 3.2.2 and 3.6.2).

1 Scope

This standard specifies methods for determining the content of arsenic, cadmium, chromium, lead and mercury in fertilizers.

This standard applies to the determination of arsenic, cadmium, chromium, lead and mercury content in fertilizers.

The detection limit of this standard method is. arsenic. 0.8mg/kg for silver diethyldithiocarbamate spectrophotometry, and atomic fluorescence spectrometry for 0.1µg/kg, cadmium is 0.4mg/kg, chromium is 0.1mg/kg, lead is 1mg/kg, mercury. hydride generation-atomic absorption spectrophotometry is 0.1mg/kg, 0.05µg/kg by atomic fluorescence spectrometry.

2 Normative references

The following documents are indispensable for the application of this document. For dated reference documents, only the dated version applies to this document.

For undated references, the latest version (including all amendments) applies to this document.

HG/T 2843 Commonly used standard titration solution, standard solution, reagent solution and indicator solution for chemical analysis of fertilizer products

NY/T 1978-2010 Fertilizer determination of mercury, arsenic, cadmium, lead, and chromium content

3 Test method

The preparation of reagents, water and solutions used in this standard shall be in accordance with HG/T 2843 when specifications and preparation methods are not indicated.

3.1 Preparation of sample solution

3.1.1 Sample preparation

Prepare according to the corresponding product standard.

3.1.2 Reagents and materials

3.1.2.1 Hydrochloric acid.

3.1.2.2 Nitric acid.

3.1.2.3 Hydrochloric acid solution. 15.Add 1 volume of hydrochloric acid to 5 volumes of water.

3.1.3 Instruments

3.1.3.1 Generally laboratory equipment.

3.1.3.2 Electric heating plate, the power is 1.8kW~2.4kW.

3.1.4 Preparation of sample solution

Make parallel determinations of two samples.

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

Referenced standards

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Editions of GB/T 23349

EditionTitleRevisionStatus
GB/T 23349-2020Determination of arsenic,cadmium,chromium,lead and mercury contents for fertilizerscurrent editionCurrent
GB/T 23349-2009Determination of arsenic,cadmium,chromium,lead and mercury contents for fertilizersprevious editionSuperseded

This page sells the current edition, GB/T 23349-2020. Earlier editions are listed for reference only.

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