GB/T 23349-2020Determination of arsenic,cadmium,chromium,lead and mercury contents for fertilizers (English PDF)
肥料中砷、镉、铬、铅、汞含量的测定
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Issued by
SAMR; SAC
Level / Type
National · Recommended
Issue date
November 19, 2020
Implementation date
June 1, 2021
Scope
GB/T 23349-2020 is the English-translated version of 肥料中砷、镉、铬、铅、汞含量的测定.
GB/T 23349-2020 sets the methods for determining the arsenic, cadmium, chromium, lead and mercury contents of fertilizers. It gives the test methods for each element, among them silver diethyldithiocarbamate spectrophotometry and atomic fluorescence spectrometry for arsenic, with their detection limits.
It applies to the determination of these five elements in fertilizers. Fertilizer producers, testing laboratories and market regulators use it. Issued on 19 November 2020, it has applied since 1 June 2021, replacing GB/T 23349-2009.
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Document preview — GB/T 23349-2020
National Standard of the People's Republic of China
- ICS
- 65.080
- Classification
- G 20
- Replacing
- GB/T 23349-2009
Issued by: State Administration for Market Regulation; Standardization Administration of the PRC
Contents
- Foreword
- 1 Scope
- 2 Normative references
- 3 Test method
Foreword
This standard was drafted in accordance with the rules given in GB/T 1.1-2009.
This standard replaces GB/T 23349-2009 "Ecological indicators of arsenic, cadmium, lead, chromium, and mercury in fertilizers". Compared with GB/T 23349-2009, In addition to editorial changes, the main technical changes are as follows.
---The detection limit of the method has been increased (see Chapter 1);
---Deleted limit requirements and inspection rules (see Chapter 3 and Chapter 5 of the 2009 edition);
---The atomic fluorescence spectrometry method of arsenic and mercury has been added (see 3.2.2 and 3.6.2).
1 Scope
This standard specifies methods for determining the content of arsenic, cadmium, chromium, lead and mercury in fertilizers.
This standard applies to the determination of arsenic, cadmium, chromium, lead and mercury content in fertilizers.
The detection limit of this standard method is. arsenic. 0.8mg/kg for silver diethyldithiocarbamate spectrophotometry, and atomic fluorescence spectrometry for 0.1µg/kg, cadmium is 0.4mg/kg, chromium is 0.1mg/kg, lead is 1mg/kg, mercury. hydride generation-atomic absorption spectrophotometry is 0.1mg/kg, 0.05µg/kg by atomic fluorescence spectrometry.
2 Normative references
The following documents are indispensable for the application of this document. For dated reference documents, only the dated version applies to this document.
For undated references, the latest version (including all amendments) applies to this document.
HG/T 2843 Commonly used standard titration solution, standard solution, reagent solution and indicator solution for chemical analysis of fertilizer products
NY/T 1978-2010 Fertilizer determination of mercury, arsenic, cadmium, lead, and chromium content
3 Test method
The preparation of reagents, water and solutions used in this standard shall be in accordance with HG/T 2843 when specifications and preparation methods are not indicated.
3.1 Preparation of sample solution
3.1.1 Sample preparation
Prepare according to the corresponding product standard.
3.1.2 Reagents and materials
3.1.2.1 Hydrochloric acid.
3.1.2.2 Nitric acid.
3.1.2.3 Hydrochloric acid solution. 15.Add 1 volume of hydrochloric acid to 5 volumes of water.
3.1.3 Instruments
3.1.3.1 Generally laboratory equipment.
3.1.3.2 Electric heating plate, the power is 1.8kW~2.4kW.
3.1.4 Preparation of sample solution
Make parallel determinations of two samples.
......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.
Referenced standards
Normative references
NY/T 1978-2010
Cited by
- GB/T 42828.1-2023General technology for saline-alkali land improvement—Part 1: Improvement technology by iron tailings
- GB/T 40750-2021Biogas slurry for agricultural use
- GB/T 18877-2020Organic inorganic compound fertilizer
- GB/T 39700-2020Treatment and disposal method for boron mud
- DL/T 1996-2019Specification of performance test for ammonia flue gas desulfurization
- GB 38400-2019Limitation requirements of toxic and harmful substance in fertilizers
Similar standards
Editions of GB/T 23349
| Edition | Title | Revision | Status |
|---|---|---|---|
| GB/T 23349-2020 | Determination of arsenic,cadmium,chromium,lead and mercury contents for fertilizers | current edition | Current |
| GB/T 23349-2009 | Determination of arsenic,cadmium,chromium,lead and mercury contents for fertilizers | previous edition | Superseded |
This page sells the current edition, GB/T 23349-2020. Earlier editions are listed for reference only.
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