GB/T 15726-2021Glassware—Stress examination methods (English PDF)
玻璃仪器 内应力检验方法
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Issued by
SAMR; SAC
Level / Type
National · Recommended
Issue date
August 20, 2021
Implementation date
March 1, 2022
Scope
GB/T 15726-2021 is the English-translated version of 玻璃仪器 内应力检验方法.
GB/T 15726-2021 is the Chinese national method for examining the internal stress of glassware. It gives the terms and definitions, the principle of the polarised light examination, the specimens, the instruments, the test steps, the calculation of the result and the examination report.
It applies to the examination of the internal stress left in glassware after annealing, the stress that makes a glass break in use. Glassworks and their quality laboratories use it.
It replaces GB/T 15726-1995, was issued on 20 August 2021 and has applied since 1 March 2022.
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Document preview — GB/T 15726-2021
National Standard of the People's Republic of China
- ICS
- 81.040.01
- Classification
- N 64
- Replacing
- GB/T 15726-1995
Issued by: State Administration for Market Regulation; Standardization Administration of the PRC
Contents
- Foreword3
- 1 Scope4
- 2 Normative references4
- 3 Terms and definitions4
- 4 Principle4
- 5 Specimens5
- 6 Instruments5
- 7 Test steps5
- 8 Result calculation7
- 9 Examination report8
1 Scope
This document specifies the terms and definitions, principle, specimens, instruments, test steps, result calculation, and examination report for the internal stress examination of glassware.
This document apples to the internal stress examination of glassware after annealing.
2 Normative references
This document has no normative references.
3 Terms and definitions
For the purpose of this document, the following terms and definitions apply.
3.1 Polarizer
An optical device, through which natural light is converted into plane polarized light with a certain vibration direction.
NOTE: Polarizer is usually placed between the light source and the specimen being tested, also known as a polarizer [Translator's note. Only different Chinese names are given here.].
3.2 Analyzer
An optical device, through which natural light is converted into plane polarized light with a certain vibration direction.
NOTE: Analyzer is usually placed between the observer and the specimen being tested, also known as an analyzer [Translator's note. Only different Chinese names are given here.].
4 Principle
4.1 Glass is usually an isotropic homogeneous material. When internal stress exists, it exhibits anisotropy and produces birefringence of light. This method uses a polarizing stress meter to measure the birefringence optical path difference, and the value of the birefringence optical path difference per unit thickness is used to represent the magnitude of the product's internal stress.
4.2 The stress optical constants of the same type of glass are the same, and the value of the birefringence optical path difference per unit thickness is used to represent the magnitude of its internal stress.
4.3 This method uses a polarizing stress meter to measure the birefringence optical path difference, and calculates the magnitude of internal stress through the birefringence optical path difference.
5 Specimens
5.1 The specimens shall be glassware that have not been subjected to other tests after annealing.
5.2 The specimens shall be placed in the laboratory for more than 30 min in advance.
5.3 Wear gloves during examination to avoid direct contact with the specimens with your hands.
6 Instruments
6.1 When using polarizing elements and protective parts for observation, the brightness of the edge of the light field shall not be less than 120 cd/m2.
6.2 The polarizing element used shall ensure that the polarization degree at any point in the bright field is not less than 99 %.
6.3 The polarization field shall not be less than 85 mm.
6.4 A 565 nm full-wave plate (sensitive color plate) and a quarter-wave plate can be placed between the polarizer and the analyzer. The slow axis of the wave plate is 90° to the polarization plane of the polarizer.
6.5 The analyzer rotates relative to the polarizer and the full-wave plate or quarter-wave plate, and there is a device for measuring the rotation angle (the scale value is 1°).
6.6 The accuracy of the polarizing stress meter is >= 3 nm.
7 Test steps
7.4 Quantitative test method for internal stress of colorless glass specimens
7.1 Environmental requirements for polarizing stress meter
The polarizing stress meter shall be installed in an environment with a temperature of 10 °C ~ 35 °C, a relative humidity of less than 80 %, and dim light.
7.2 Zero-point adjustment of polarizing stress meter
When a quarter-wave plate is placed, the field of view shall be the darkest; when a full- wave plate is placed, the field of view shall be purple-red.
7.3 Qualitative measurement of birefringence optical path difference
Place a full-wave plate, place the specimen to be tested in the field of view, and observe the interference color. If it is still purple-red or only slightly changed, it means that the optical path difference of the specimen is very small; if the interference color of a certain part of the specimen is sky blue, green or orange-red, yellow, it means that the birefringence optical path difference of that part is large, and the internal stress trend of that part can be judged.
7.4.1 Measurement of bottom or similar bottom of colorless glass specimens
Place a quarter-wave plate in the field of view and adjust the zero point of the polarizing stress meter to make it a dark field of view. Place the specimen in the field of view and observe the bottom from the mouth. At this time, a dark cross will appear in the field of view. If the stress of the specimen is small, the dark cross will be blurred. Rotate the analyzer to separate the dark cross into two arcs moving in opposite directions. As the dark area moves outward, blue-gray appears on the concave side of the arc and brown appears on the convex side. If the stress value of a selected point is measured, rotate the analyzer until the blue-gray color at that point is just replaced by brown. Rotate the specimen around the axis to find the maximum stress point, rotate the analyzer until the blue-gray color is replaced by brown, record the rotation angle of the analyzer at this time, and measure the specimen thickness at that point.
7.4.2 Measurement of side wall of colorless glass specimens
Place a quarter-wave plate in the field of view and adjust the zero point of the polarizing stress meter to make it a dark field of view. Place the specimen in the field of view so that the axis of the specimen is 45° to the polarization plane. At this time, different bright and dark areas appear on the side wall. Rotate the analyzer until the dark areas on the side wall gather and just completely replace the bright areas. Rotate the specimen around the axis to determine the maximum stress area. Record the analyzer placement angle where the maximum stress area is measured, and measure the thickness of the two side walls of this area (the sum of the thickness of the two side walls). If the light and dark changes unsteadily at the dark gathering area, find a reference area nearby.
The optical path difference of this reference area shall be small or constant, or both. At this time, first measure the optical path difference of the reference area, and then slightly tilt it so that the light passes through a layer of reference area and a layer of wall thickness of the area to be measured. The optical path difference value minus half of the optical path difference of the reference area is the optical path difference of the
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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 23 pages — is available in the English PDF.
Referenced standards
Cited by
- GB/T 15723-2024Laboratory glassware - Desiccators
- GB/T 15724-2024Laboratory glasswarehBeakers
- GB/T 22362-2023Laboratory glass apparatus - Flasks
- GB/T 42387-2023Volumetric glass - Technical requirements for quality classification
- GB 17762-2022Safe requirements of thermotolerant glassware
- GB/T 35596-2022Heat resistant blowed from borosilicate glass
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Editions of GB/T 15726
| Edition | Title | Revision | Status |
|---|---|---|---|
| GB/T 15726-2021 | Glassware—Stress examination methods | current edition | Current |
| GB/T 15726-1995 | Glassware—Stress examination methods | previous edition | Superseded |
This page sells the current edition, GB/T 15726-2021. Earlier editions are listed for reference only.
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