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GB/T 226-2015Test method for macrostructure and defect of steel by etching (English PDF)

钢的低倍组织及缺陷酸蚀检验法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

September 11, 2015

Implementation date

June 1, 2016

Scope

GB/T 226-2015 is the English-translated version of 钢的低倍组织及缺陷酸蚀检验法.

GB/T 226-2015 sets out the etching tests that reveal the macrostructure and defects of steel.

Clause 1 states that the standard specifies the hot acid etching method, the cold acid etching method, including the dendrite corrosion method, and the electrolytic etching method which test the macrostructure and defect of steel, that it is applicable to the acid etching test of the macrostructure and defect of steel, and that the acid etching test of other materials can be implemented according to it.

The contents list clause 3 Specimen, clause 4 Test Method, clause 5 Test Results, clause 6 Specimen Retention, clause 7 Lab Environment Safety and clause 8 Test Report.

Clause 3 covers specimen cutting, machining and dimension: the specimen may be cut by hot saw, cold saw, flame cutting, shearing or other methods and the deformation or heat affected zone caused by sampling has to be removed during machining, the reference dimension from the test surface to the cutting surface and the test surface roughness Ra after machining are both provided for, and the specimen thickness is generally about 20 mm to 30 mm while a longitudinal specimen is generally about 1.5 times the edge or diameter in length.

Clause 4 recommends the hot acid etching method for arbitration inspection where the technical conditions make no special provision, selects the acid liquid for hot acid etching according to the steel type, has the test surface reprocessed to a depth of 1 mm or more and re-etched if over corrosion occurs in cold acid etching, and splits electrolytic etching into an AC and a DC method, the DC method working at room temperature with an acid solution of 100 mL of water plus 6 mL to 12 mL of hydrochloric acid for a specimen area below 130 cm2 and of 100 mL of water plus 6 mL of hydrochloric acid and 1 g of boric acid above it.

Clause 5 allows the macrostructure and defect shapes displayed by the hot acid, routine cold acid and electrolytic etching methods to be obtained by photo-optical or digital imaging, clause 6 recommends methods for keeping the specimen for a certain period, and clause 7 requires the residual waste acid left after etching to be treated according to the discharge provision for second pollutants in 4.2.1.2 of GB 8978-1996, which clause 2 cites.

The foreword records the changes against the 1991 edition, among them the modified specimen cutting provision, the modified reference dimension from the test surface to the cutting surface, the new requirement on test surface roughness after machining, the added dendrite corrosion and cold acid etching method, the modified ingredients, etching time and temperature of some hot and cold acid etching methods, the added DC electrolytic corrosion method, the new way of expressing test results, the removal of the evaluation provision for test results and the new provision on lab environment safety; it also records that the standard was proposed by the China Iron and Steel Industry Association and is under the jurisdiction of SAC/TC 183.

It replaces GB/T 226-1991, was issued on 11 September 2015 and has applied since 1 June 2016.

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Document preview — GB/T 226-2015

National Standard of the People's Republic of China

ICS
77.040.99
Classification
H 24
Replacing
GB/T 226-1991

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • 1 Scope4
  • 2 Normative References4
  • 3 Specimen4
  • 4 Test Method6
  • 5 Test Results10
  • 6 Specimen Retention11
  • 7 Lab Environment Safety11
  • 8 Test Report11
Foreword

This Standard was drafted as per the rules specified in GB/T 1.1-2009.

This Standard replaces GB/T 226-1991 Test Method for Macrostructure and Defect of Steel by Etching.

Compared with GB/T 226-1991, this Standard mainly has the following changes.

--- Modifying the provision of specimen cutting method;

--- Modifying the provision of reference dimension from specimen test surface to the cutting surface;

--- Increasing the requirement of specimen test surface roughness after machining;

--- Increasing the dendrite corrosion and cold acid etching method;

--- Modifying and increasing the ingredients, etching time and temperature of partial hot and cold acid etching methods;

--- Increasing the DC electrolytic corrosion method;

--- Increasing the expressing method of test results;

--- Removing the evaluation provision of test results;

--- Increasing the provision on lab environment safety.

This Standard was proposed by China Iron and Steel Industry Association.

This Standard shall be under the jurisdiction of National Technical Committee for Standardization of Steel (SAC/TC 183).

The previous versions that are replaced by this Standard are as follows.

--- GB/T 226-1997 and GB/T 226-1991.

1 Scope

This Standard specifies the hot acid etching method, cold acid etching method (including dendrite corrosion method), and.electrolytic etching method, which test the macrostructure and defect of steel.

This Standard is applicable to the acid etching test of the macrostructure and defect of steel. Other material's acid etching test can be implemented as per this Standard.

2 Normative References

The following documents are essential to the application of this document. For the dated documents, only the versions with the dates indicated are applicable to this document; for the undated documents, only the latest version (including all the amendments) are applicable to this standard.

GB 8978-1996 Integrated Wastewater Discharge Standard

3 Specimen

3.1 Specimen cutting

3.2 Specimen machining

3.2.1 Specimen can be cut through hot saw, cold saw, flame cutting, shearing and other methods. The deformation or heat affected zone caused by sampling shall be removed during the specimen machining process.

3.2.2 The reference dimension from the test surface to the cutting surface of specimen.

3.2.3 After machining, the specimen's test surface roughness Ra shall meet the following requirements. […]

3.3 Specimen dimension

3.3.1 Specimen thickness is generally about 20mm~30mm.

3.3.2 Length of longitudinal specimen is generally about 1.5 times of edge or diameter.

4 Test Method

4.1 Overview

4.1.1 In the following methods, the parameters shall be selected on the premise of guaranteeing to display the macrostructure and defect of steel. The proportion of all kinds of strong acids is as follows.

4.1.2 During the arbitration inspecting process, if the technical conditions have no special provisions, then the hot acid etching method is recommended to be subject to.

4.2 Hot acid etching method

4.2.1 Corresponding acid liquid shall be selected as per the different steel types.

4.3 Cold acid etching method

4.3.4 If over corrosion occurs, re-process the test surface of the specimen, remove 1mm-above depth and then re-etch.

4.4 Electrolytic etching method

4.4.1 AC electrolytic etching method
4.4.2.2

DC is used under room temperature to conduct electrolytic etching, when specimen area is less than 130cm2, the acid solution shall be prepared by 100mL of water added with 6mL~12mL of hydrochloric acid; when specimen area is more than 130cm2, the acid solution shall be prepared by 100mL of water added with 6mL of hydrochloric acid and 1g of boric acid.

5 Test Results

5.1 The macrostructure and defect shape of steel displayed by hot acid etching method, routine cold acid etching method, and electrolytic etching method can be obtained through photo-optical or digital imaging method.

6 Specimen Retention

In order to keep the specimen for certain period, the following methods are recommended to use.

7 Lab Environment Safety

Residual waste acid after etching operation shall be treated as per the discharge provision of second pollutant specified in Clause 4.2.1.2 of GB 8978-1996. […]

8 Test Report

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

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Editions of GB/T 226

EditionTitleRevisionStatus
GB/T 226-2015Test method for macrostructure and defect of steel by etchingcurrent editionCurrent
GB/T 226-1991Test method for macrostructure and defect of steel by etchingprevious editionSuperseded

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