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GB/T 17280-2017Standard test method for distillation of crude petroleum - 15-theoretical plate column (English PDF)

原油蒸馏标准试验方法 15-理论塔板蒸馏柱

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Issued by

General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China; Standardization Administration of China

Level / Type

National · Recommended

Issue date

December 29, 2017

Implementation date

July 1, 2018

Scope

GB/T 17280-2017 is the English-translated version of 原油蒸馏标准试验方法 15-理论塔板蒸馏柱.

GB/T 17280-2017 is the Chinese standard "Standard test method for distillation of crude petroleum - 15-theoretical plate column". Its scope clause reads: This standard specifies the Reid vapor pressure is not greater than 82.7kPa stable crude oil distillation test method.

This standard specifies the distillation column using 14 to 18 theoretical plates, distilled at a reflux ratio of 5.

1, eventually reaching constant The mass of the liquefied gas, the distillation fraction and the residue fraction was obtained under the test conditions of a pressure-equivalent cutting temperature (AET) of 400 ° C, and each fraction Mass yield or volumetric yield, followed by a plot of the true boiling point (TBP) distillation curve with the cutting temperature.

This standard applies to liquefied petroleum gas, light naphtha and the initial boiling point higher than 400 °C distillate oil mixture outside. Its clauses include terms and definitions.

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Document preview — GB/T 17280-2017

National Standard of the People's Republic of China

ICS
75.040
Classification
E21

Issued by: General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China; Standardization Administration of China

Contents

  • Preface
  • 1 Scope
  • 2 Normative references
  • 3 Terms and definitions
  • 4 Test Method Summary
  • 5 instruments
  • 6 instrument performance evaluation
  • 7 samples
  • 8 Preparation of Instruments
  • 9 Test Procedure
  • 10 calculated
  • 11 Test Report
  • 12 precision and deviation
  • 13 Quality Assurance and Control
  • Appendix A (Normative) Distillation column dynamic retention test method for determination of
  • Appendix B (Normative) Distillation column efficiency test method
  • Appendix C (Normative) Distillation column heat loss test method (static conditions)
  • Appendix D (Normative) Back to the distribution valve inspection test method
  • Appendix E (Normative) Temperature sensor position test method
  • Appendix F (Normative) Temperature sensor response time determination test methods
  • Appendix G (Normative) Sensor calibration method
  • Appendix H (Normative) Measured vapor temperature and atmospheric equivalent temperature (AET) conversion
  • Appendix I (Informative) Distillation column performance test methods
  • Appendix J (Informative) Water-containing crude oil dehydration test method
  • References

1 Scope

This standard specifies the Reid vapor pressure is not greater than 82.7kPa stable crude oil distillation test method.

This standard specifies the distillation column using 14 to 18 theoretical plates, distilled at a reflux ratio of 5. 1, eventually reaching constant

The mass of the liquefied gas, the distillation fraction and the residue fraction was obtained under the test conditions of a pressure-equivalent cutting temperature (AET) of 400 ° C, and each fraction

Mass yield or volumetric yield, followed by a plot of the true boiling point (TBP) distillation curve with the cutting temperature.

This standard applies to liquefied petroleum gas, light naphtha and the initial boiling point higher than 400 °C distillate oil mixture outside.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version applies to this article

Pieces. For undated references, the latest edition (including all amendments) applies to this document.

GB/T 1884 Crude petroleum and liquid petroleum products - Laboratory density method (Densitometer method) (GB/T 1884-2000, eqvISO

3675.1998)

GB/T 4756 Petroleum liquid hand sampling method (GB/T 4756-2015, ISO 3170.2004, MOD)

GB/T 8929 Determination of crude oil water content distillation (GB/T 8929-2006, ISO 9029.1990, MOD)

GB/T 13377 Determination of the density or relative density of crude oil and liquid or solid petroleum products (capillary pyknometer and graduated double

Capillary pyknometer method) (GB/T 13377-2010, ISO 3838.2004, MOD)

GB/T 27867 oil liquid pipeline automatic sampling method (GB/T 27867-2011, ISO 3171.1988, IDT)

SH/T 0604 Crude petroleum and petroleum products densitometry (U-tube method) (SH/T 0604-2000, eqvISO 12185.1996)

3 Terms and definitions

The following terms and definitions apply to this document.

3.1 Adiabaticity

The entire distillation column has no significant increase in heat or loss of heat. When the distillation column heat loss occurs, the column back reflux than stigma

Flow abnormally increased. The column insulation sleeve overheating, the situation is the opposite.

3.2 Steamed rate boiluprate

The amount of steam entering the distillation column per unit of time.

3.3 Crude debutanizationofcrudepetroleum

Light hydrocarbons (including n-butane) before n-butane in crude oil are removed, leaving heavier hydrocarbons. In practice, crude oil is butane is meant to be present

More than 95% of C2-C4 and less than 5% of C5 hydrocarbons in the original sample are collected in the cold trap.

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 91 pages — is available in the English PDF.

Referenced standards

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Editions of GB/T 17280

EditionTitleRevisionStatus
GB/T 17280-2017Standard test method for distillation of crude petroleum - 15-theoretical plate columncurrent editionCurrent
GB/T 17280-2009Standard test method for distillation of crude petroleum - 15-theoretical plate columnprevious editionSuperseded

This page sells the current edition, GB/T 17280-2017. Earlier editions are listed for reference only.

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