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GB/T 12496.10-1999Test methods of wooden activated carbon--Determination of methylene blue adsorption (English PDF)

木质活性炭试验方法 亚甲基蓝吸附值的测定

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Issued by

State Administration of Quality and Technical Supervision

Level / Type

National · Recommended

Issue date

November 10, 1999

Implementation date

April 1, 2000

Scope

GB/T 12496.10-1999 is the English-translated version of 木质活性炭试验方法 亚甲基蓝吸附值的测定.

GB/T 12496.10-1999 is the Chinese national standard on test methods of wooden activated carbon--determination of methylene blue adsorption, in the field of agriculture. The /T suffix marks it as a recommended standard: it is not compulsory by itself, but it becomes binding as soon as a contract, a tender or a customer specification calls it up - which in practice is how most foreign buyers meet it. It was issued on 10 November 1999 by the State Administration of Quality and Technical Supervision, and has been in force since 1 April 2000. Classification: ICS 65-050, CCS B73. This page is published from the official record of the standard held by the Chinese standards administration: the identification, the dates, the classification and the issuing body are taken from there. The clause text, the tables and the numeric limits are in the document itself, which is delivered complete in English translation.

Document preview — GB/T 12496.10-1999

National Standard of the People's Republic of China

ICS
65-050
Classification
B73

Issued by: State Administration of Quality and Technical Supervision

Contents

  • 2 Normative References
  • 3 Method Summary
  • 5 Reagents and Solutions
  • 5.4 Buffer solution: Weigh
  • 5.5 Methylene blue test solution (

Foreword

NATIONAL STANDARD OF THE PEOPLE'S REPUBLIC OF CHINA ICS

GB/T 12496.10-1999

Replacing GB/T 12496.2-1990

Test Methods of Wooden Activated Carbon - Determination of Methylene Blue Adsorption

8 Table of Contents Foreword ........................................................................................................................

31 Scope ...........................................................................................................................

42 Normative References .................................................................................................

43 Method Summary........................................................................................................

44 Main Instruments ........................................................................................................

45 Reagents and Solutions ...............................................................................................

56 Operation Procedures ..................................................................................................

67 Expression of Results..................................................................................................

Test Methods of Wooden Activated Carbon - Determination of Methylene Blue Adsorption 1 Scope

This Standard specifies the test methods for the methylene blue adsorption value of wooden activated carbon. This Standard applies to wooden activated carbon.

2 Normative References

The following standards contain provisions which, through reference in this Standard, constitute provisions of this Standard. At the time of publication, the editions indicated are valid. All standards are subject to revision. The parties who are using this Standard shall explore the possibility of using the latest version of the following standards.

GB/T 6682-1992 Water for laboratory use - Specifications

GB/T 9721-1988 Chemical reagent - General rules for the molecular absorption spectrophotometry (ultraviolet and visible)

3 Method Summary

The specimen is mixed with a certain amount (in milliliters) of methylene blue solution and then filtered. The absorbance of the filtrate is measured by a spectrophotometer. If the absorbance is lower than the absorbance of the standard solution at a specified concentration, the required number of milliliters of methylene blue is the methylene blue adsorption value of the activated carbon specimen.

4 Main Instruments 4.1 Electric oscillator (reciprocating), with frequency about 275 times/min.

5 Reagents and Solutions

The water used in this Standard shall comply with the Grade-3 water specifications in GB/T 6682. The listed reagents are analytically pure reagents unless otherwise specified.

5.1 Methylene blue, indicator.

5.2 Disodium hydrogen phosphate [Na2HPO4 -12H2O] (GB/T 1263).

5.3 Potassium dihydrogen phosphate (GB/T 1274).

5.4 Buffer solution: Weigh

3.6 g of potassium dihydrogen phosphate and

14.3 g of disodium hydrogen phosphate; and dissolve them in 1,000 mL of water. The pH value of this buffer solution is about 7.

5.5 Methylene blue test solution (

5.5.1 Preparation Since the properties of methylene blue change during the drying process, it shall be used without drying. Therefore, it is necessary to measure its moisture content after drying at (105 ± 0.5) °C for 4 h. The amount of undried methylene blue to be used is calculated according to Formula (1): Where: m1 - mass of undried methylene blue, in g; E - moisture content, in %; m - required amounts of dry products, in g; P - purity of methylene blue, in %. Calculate the amount of undried product equivalent to

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 8 pages — is available in the English PDF.

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Editions of GB/T 12496.10

EditionTitleRevisionStatus
GB/T 12496.10-1999Test methods of wooden activated carbon--Determination of methylene blue adsorptioncurrent editionCurrent
GB/T 12496.2-1990Test method of wooden activated carbon--Adsorption of methylene bluemerged into this editionSuperseded

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