GB/T 5121.14-2008Methods for chemical analysis of copper and copper alloys -- Part 14: Determination of manganese content (English PDF)
铜及铜合金化学分析方法 第14部分:锰含量的测定
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Issued by
Standardization Administration of China
Level / Type
National · Recommended
Issue date
June 17, 2008
Implementation date
December 1, 2008
Scope
GB/T 5121.14-2008 is the English-translated version of 铜及铜合金化学分析方法 第14部分:锰含量的测定.
GB/T 5121.14-2008 — This method specifies the method for determination of copper and copper alloy of manganese content. This method is applicable to the determination of copper and copper alloy of manganese content. Measurement range. 0.00005% to 0.0010%.
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Document preview — GB/T 5121.14-2008
National Standard of the People's Republic of China
- ICS
- 77.120.30
- Classification
- H 13
- Replacing
- GB/T 5121.14-1996; GB/T 13293.3-1991
Issued by: Standardization Administration of China
Contents
- Foreword
- 1 Method, a Zeeman effect electrothermal atomic absorption spectrometry
- 1.1 Scope
- 1.2 Principle of the method
- 1.3 Reagents
Foreword
GB/T 5121 "Copper and copper alloy chemical analysis method" a total of 27 sections.
--- Part 1. Determination of copper content;
--- Part 2. Determination of phosphorus content;
--- Part 3. Determination of lead content;
--- Part 4. Carbon, Determination of sulfur content;
--- Part 5. Determination of nickel content;
--- Part 6. Determination of bismuth content;
--- Part 7. Determination of arsenic content;
--- Part 8. Determination of oxygen content;
--- Part 9. Determination of iron content;
--- Part 10. Determination of tin content;
--- Part 11. Determination of zinc content;
--- Part 12. Determination of antimony content;
--- Part 13. Determination of aluminum content;
--- Part 14. Determination of manganese content;
--- Part 15. Determination of cobalt content;
--- Part 16. Determination of chromium content;
--- Part 17. Determination of beryllium content;
--- Part 18. Determination of magnesium content;
--- Part 19. Determination of silver content;
--- Part 20. Determination of zirconium content;
--- Part 21. Determination of titanium content;
--- Part 22. Determination of cadmium content;
--- Part 23. Determination of silicon content;
--- Part 24. selenium, tellurium content was measured;
--- Part 25. Determination of boron content;
--- Part 26. Determination of mercury content;
--- Part 27. Inductively coupled plasma atomic emission spectrometry.
This is Part 14.
This section includes a method, second method, Method three.
The second method to modify the part using ISO 2543. 1973 "Copper and copper alloys - Determination of manganese content - spectrophotometric method." Major technology within the volume, and ISO 2543. 1973 the same structure does not correspond exactly to write. Specific technical difference in Appendix A, Appendix B.
This Part replaces GB/T 5121.14-1996 "Copper and copper alloys - Determination of manganese content" and GB/T 13293.3-1991 "Methods for chemical analysis of high purity copper cathode Zeeman effect electrothermal atomic absorption spectrometric method for the determination of chromium, manganese and cadmium." this portion of the GB/T 5121.14-1996, GB/T 13293.3-1991 compared to the main changes are as follows.
--- One method of GB/T 13293.3-1991 amendment complements the quality assurance and control provisions, increasing the precision of the terms;
--- Second method "for Determination of the amount of the first chapter potassium periodate spectrophotometric method" of GB/T 5121.14-1996 of repair Order to supplement the provisions of quality assurance and control, increasing the precision of the terms;
--- Method three is GB/T 5121.14-1996 in "Method 2 The second ammonium ferrous sulfate titration method for the determination of manganese content" amendments Supplemented with quality assurance and control provisions, increasing the precision of the terms.
This section in Appendix A, Appendix B is an informative annex.
This part is proposed by the China Nonferrous Metals Industry Association.
The non-ferrous metal part by the National Standardization Technical Committee.
This section Chinalco Luoyang Copper Co., Ltd., Beijing General Research Institute of Mining and Metallurgy, China Nonferrous Metals Industry is responsible Institute of Standards Metrology and Quality Drafted.
A method in this section was drafted by Beijing General Research Institute of Mining and Metallurgy.
This section a method Jiangxi Copper Co., Ltd., Jinchuan Group Co., Ltd. participated in the drafting.
1 Method, a Zeeman effect electrothermal atomic absorption spectrometry
1.1 Scope
This method specifies the method for determination of copper and copper alloy of manganese content.
This method is applicable to the determination of copper and copper alloy of manganese content. Measurement range. 0.00005% to 0.0010%.
1.2 Principle of the method
Sample was dissolved in nitric acid, a volume of the test solution injected into the electrothermal atomizer with Zeeman effect atomic absorption spectrometer 279.5nm wavelength absorbance measurement manganese, mass fraction calculated by working curve method.
1.3 Reagents
Unless otherwise indicated in the analysis using only recognized as analytical grade reagents and distilled or deionized water or equivalent purity. experiment the utensils were soaked 12h, washed thoroughly with water and nitric acid (1.3.3).
1.3.1 Copper (Cu mass fraction >=99.99%, manganese content
......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 6 pages — is available in the English PDF.
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Related Standards
GB/T 5121.1-2008 — Methods for chemical analysis of copper and copper alloys -- Part 1: Determination of copper content
GB/T 5121.10-2008 — Methods for chemical analysis of copper and copper alloys -- Part 10: Determination of tin content
GB/T 5121.11-2008 — Methods for chemical analysis of copper and copper alloys -- Part 11: Determination of zinc content
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