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GB/T 24521-2018Method for the determination of specific resistance of carbon raw materials and coke (English PDF)

炭素原料和焦炭电阻率测定方法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

May 14, 2018

Implementation date

February 1, 2019

Scope

GB/T 24521-2018 is the English-translated version of 炭素原料和焦炭电阻率测定方法.

GB/T 24521-2018 gives the method for measuring the specific resistance of carbon raw materials and coke powders. It covers anthracite, graphite, roasted and crushed material, calcined petroleum coke, graphitized coke and needle coke used to make carbon products, as well as coke powder.

A dried specimen of set particle size is placed in a specimen cylinder and a current is passed through it under pressure; the standard describes the powder resistance measuring instrument, the drying oven, sampling and crushing of the specimen through a 0.5 mm sieve, weighing, the determination itself, the calculation of the result, repeatability limits and the content of the inspection report.

It is used by carbon producers and testing laboratories. It replaces GB/T 24521-2009, was issued on 14 May 2018 and has applied since 1 February 2019.

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Document preview — GB/T 24521-2018

National Standard of the People's Republic of China

ICS
75.160.10
Classification
H 32
Replacing
GB/T 24521-2009

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Foreword3
  • 1 Scope4
  • 2 Normative references4
  • 3 Method principle4
  • 4 Instruments and equipment4
  • 5 Sampling and specimen preparation5
  • 6 Test steps6
  • 7 Results calculation7
  • 8 Precision7
  • 9 Inspection report7

Foreword

This Standard was drafted in accordance with the rules given in GB/T 1.1-2009.

This Standard replaces GB/T 24521-2009 "Method for the determination of specific resistance of coke". Compared with GB/T 24521-2009, main content changes in this Standard are as follows.

-- modified the standard's name to "Method for the determination of specific resistance of carbon raw materials and coke";

-- modified the scope (see Clause 1 of this Edition, Clause 1 of Edition 2009);

-- modified the instruments and equipment (see Clause 4 of this Edition, Clause 4 of Edition 2009);

-- modified the requirements for preparation of particle size of specimen (see 5.3 of this Edition, 5.2 of Edition 2009);

-- modified the test steps (see Clause 6 of this Edition, Clause 6 of Edition 2009);

-- modified the results calculation (see Clause 7 of this Edition, Clause 7 of Edition 2009);

-- modified the precision (see Clause 8 of this Edition, Clause 7 of Edition 2009).

1 Scope

This Standard specifies method for the determination of specific resistance of carbon raw materials and coke powders.

This Standard is applicable to the determination of specific resistance of raw materials for carbon production such as anthracite, graphite, roasted and crushed, calcined petroleum coke, graphitized coke, needle coke, as well as coke powders.

2 Normative references

The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies.

GB/T 1997, Coke-sampling and preparation of samples

3 Method principle

Put a dry specimen with a certain particle size into the specimen tank. Pass a certain intensity of current under a certain pressure.

4 Instruments and equipment

4.1 Powder resistance measuring instrument

4.1.1 See Figure 1 for the schematic diagram of specimen device.

4.1.2 Height measuring device. measuring range is 15mm~17mm, precision is 0.01mm.

4.1.6 Specimen cylinder. inner diameter is 16.0mm~16.3mm.

4.2 Drying oven

The temperature can be controlled at 0°C~300°C. Temperature control precision is ±5°C, with blast.

5 Sampling and specimen preparation

5.1 For cokes, it shall be carried out according to GB/T 1997.

5.3 Crush the shrunken specimen 3~4 times to make them all pass the 0.5mm square hole standard sieve.

6 Test steps

6.1 Specimen weighing

Weigh 3.3g of specimen. In order to ensure the specimen height is between 15mm~17mm, the specimen volume can be adjusted if necessary.

6.2 Determination

6.2.1 Short-circuit the bottom of the specimen cylinder and the indenter. Then apply a pressure of 3.9MPa ± 0.03MPa. Connect the wires and turn on the power.

6.2.2 Add a specimen in the specimen cylinder (see 4.16). After compacting and smoothing the upper surface of the specimen, place the specimen tube in the testing machine (see 4.1.3).

6.3 Determination times

Determine twice independently. Each determination shall use the untested new specimen. Take the average value.

7 Results calculation

Calculate the resistance of powder, rho, according to formula (1).

8 Precision

8.1 Repeatability

Under repeatability conditions, the difference between the two measurement results of the specimen greater than 300µohm·m is not more than 5%. The relative deviation of the two measurement results of the specimen less than 300µohm·m is not more than 8%.

9 Inspection report

The inspection report shall at least contain the following information. […]

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

Referenced standards

Similar standards

Editions of GB/T 24521

EditionTitleRevisionStatus
GB/T 24521-2018Method for the determination of specific resistance of carbon raw materials and cokecurrent editionCurrent
GB/T 24521-2009Method for the determination of specific resistance of carbon raw materials and cokeprevious editionSuperseded

This page sells the current edition, GB/T 24521-2018. Earlier editions are listed for reference only.

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