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GB/T 19267.6-2008Physical and chemical examination of trace evidence in forensic sciences - Part 6:Scanning electron microscope/ X ray energy dispersive spectrometry (English PDF)

刑事技术微量物证的理化检验 第6部分:扫描电子显微镜/X射线能谱法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

August 14, 2008

Implementation date

March 1, 2009

Scope

GB/T 19267.6-2008 is the English-translated version of 刑事技术微量物证的理化检验 第6部分:扫描电子显微镜/X射线能谱法.

GB/T 19267.6-2008 is the sixth part of a series on the physical and chemical examination of trace evidence in forensic sciences. It describes the test method that combines a scanning electron microscope with an X-ray energy dispersive spectrometer (SEM/EDS).

It applies to physical and chemical testing of trace evidence in criminal investigation, and it may also be consulted in other fields. The document defines terms relating to scanning electron microscopy, including the environmental scanning electron microscope, and it refers to GB/T 13966.

The series has 12 parts, starting with infrared absorption, UV-visible absorption, molecular fluorescence, atomic emission and atomic absorption spectrometry. Issued on 14 August 2008 and applicable from 1 March 2009, it replaces GB/T 19267.6-2003.

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Document preview — GB/T 19267.6-2008

National Standard of the People's Republic of China

ICS
13.310
Classification
A 92
Replacing
GB/T 19267.6-2003

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Foreword
  • 1 Scope
  • 2 Normative references
  • 3 Terms and Definitions

Foreword

GB/T 19267 "criminal and chemical examination of trace evidence" is divided into 12 parts.

--- Part 1. Infrared absorption spectrometry;

--- Part 2. UV - visible absorption spectroscopy;

--- Part 3. Molecular Fluorescence Spectroscopy;

--- Part 4. atomic emission spectrometry;

--- Part 5. Atomic absorption spectrometry;

--- Part 6. Scanning electron microscopy/X-ray spectroscopy;

--- Part 7. Gas chromatography - mass spectrometry;

--- Part 8. microscopic spectrophotometry;

--- Part 9. thin layer chromatography;

--- Part 10. gas chromatography;

--- Part 11. High performance liquid chromatography;

--- Part 12. Thermal Analysis. This section GB/T Part of 619,267.

This Part replaces GB/T 19267.6-2003 "criminal and chemical examination of trace evidence in Part 6: Scanning Electron Microscopy Mirror method. " This portion of the GB/T 19267.6-2003 compared to the main changes are.

--- Standard name a "scanning electron microscopy/X-ray spectroscopy";

--- Increasing the term of the environmental electron microscope (this section 3.2,3.18);

--- Increasing the principle part of the environmental electron microscope (this section 4.1);

--- Instrument composed of indicators made the necessary changes (this part of GB/T 19267.6-2003 and Chapter 5 of);

--- Modify the content of the samples prepared (this section 6.4.1,6.4.2, GB/T 19267.6-2003 of 6.3, 6.4);

--- Increased working distance describes the content (in this section 7.2.4);

--- Modify the sample analysis of the content (in this section and GB/T 19267.6-2003 7.3).

This section presents the People's Republic of China Ministry of Public Security.

The criminal section of the National Standardization Technical Committee Physical Testing Standardization Technical Committee (SAC/TC179/SC4) Centralized.

This section is drafted. Shanghai Public Security Bureau Evidence Identification Center.

1 Scope

GB/T 19267 provisions of this part of the scanning electron microscope and X-ray spectrometer combined with the test method.

This section applies to the technical field of trace evidence in criminal physical and chemical testing, may also refer to other areas of use.

2 Normative references

The following documents contain provisions which, through reference GB/T 19267 in this section, constitute provisions of this part. For dated reference documents Member, all subsequent amendments (not including errata content) or revisions do not apply to this section, however, encouraged to reach under this section Parties to research agreement to use the latest versions of these documents. For undated reference documents, the latest versions apply to this section.

GB/T 13966 Analytical Instruments terms

3 Terms and Definitions

GB/T 13966 and established in the following terms and definitions apply to this section.

3.4 (SEM/EDS)

Micro-beam electron bombardment of the sample, the sample excitation of micro elements characteristic X-ray detection system displays the characteristics of each element microanalysis X Ray energy and intensity graph (called spectrum) and their distribution in the surface of the specimen.

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

Referenced standards

Similar standards

Editions of GB/T 19267.6

EditionTitleRevisionStatus
GB/T 19267.6-2008Physical and chemical examination of trace evidence in forensic sciences - Part 6:Scanning electron microscope/ X ray energy dispersive spectrometrycurrent editionCurrent
GB/T 19267.6-2003Physical and chemical examination of trace evidence in forensic sciences - Part 6:Scanning electron microscope/ X ray energy dispersive spectrometryprevious editionSuperseded

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