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GB/T 47119-2026Testing method for the thermal stability of organic heat transfer fluids - Gas chromatography with internal standard method (English PDF)

有机热载体热稳定性测定法 气相色谱内标法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

January 28, 2026

Implementation date

January 28, 2026

Scope

GB/T 47119-2026 is the English-translated version of 有机热载体热稳定性测定法 气相色谱内标法.

GB/T 47119-2026 is the Chinese standard "Testing method for the thermal stability of organic heat transfer fluids - Gas chromatography with internal standard method".

Its scope clause reads: This document describes a method for determining the thermal stability of organic heat transfer fluids using gas chromatography with internal standard.

This document applies to the thermal stability of unused synthetic organic heat transfer fluids with relatively simple components and a distillation range (at atmospheric pressure) of less than 55°C. Measurement.

This document is not applicable to the determination of the thermal stability of organosilicon heat transfer fluids. Its clauses include terms and definitions.

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Document preview — GB/T 47119-2026

National Standard of the People's Republic of China

ICS
27.060.30
Classification
E 34

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Preface
  • 1.Scope
  • 2 Normative References
  • 3.Terms and Definitions
  • 4.Method Overview
  • 5.Instruments and Equipment
  • 6 Materials and Reagents
  • 7.Samples and Sample Processing 3.
  • 8.Gas Chromatograph Setup
  • 9.Determination and Calculation of Relative Correction Factor
  • 10.Determination of samples after heating
  • 11 Precision
  • 12 Test Reports

1 Scope

This document describes a method for determining the thermal stability of organic heat transfer fluids using gas chromatography with internal standard.

This document applies to the thermal stability of unused synthetic organic heat transfer fluids with relatively simple components and a distillation range (at atmospheric pressure) of less than 55°C.

Measurement.

This document is not applicable to the determination of the thermal stability of organosilicon heat transfer fluids.

2 Normative references

The contents of the following documents, through normative references within the text, constitute essential provisions of this document. Dated citations are not included.

For references to documents, only the version corresponding to that date applies to this document; for undated references, the latest version (including all amendments) applies.

This document.

GB/T 4756 Manual Sampling Method for Petroleum Liquids

GB/T 4946 Gas Chromatography Terminology

GB 4962 Safety Technical Regulations for the Use of Hydrogen

GB/T 9722-2023 General Rules for Gas Chromatography of Chemical Reagents

GB/T 23800-2009 Determination of thermal stability of organic heat transfer fluids

GB 23971 Organic Heat Transfer Fluid

GB/T 30430-2019 Standard Columns for Gas Chromatography

HG/T 3115 Performance of Borosilicate Glass 3.3

3 Terms and Definitions

The terms and definitions defined in GB/T 4946 and GB 23971, as well as the following terms and definitions, apply to this document.

3.1

A certain amount of pure substance is added as an internal standard to a certain amount of the sample to be tested, and then the sample containing the internal standard is subjected to chromatography.

Analysis was performed, and the peak areas of the internal standard and the analyte were measured separately. Based on the measured relative correction factor, the content of the analyte in the sample was calculated.

The method.

3.2 thermal stability

Organic heat transfer fluids, under specified heating conditions, resist chemical reactions such as thermal decomposition, oxidation, and polymerization, and maintain their physicochemical properties (such as viscosity).

The ability of a substance (such as temperature, flash point, acid value, etc.) to remain within permissible ranges.

[Source. GB 23971-2009, 3.7, with modifications]

3.3 original sample

Samples without organic heat transfer fluid used for thermal stability testing.

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

Referenced standards

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