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GB/T 34102-2017Determination of 2,6-ditertbutyl-p-cresol in jet fuels—Differential pulse voltammetry (English PDF)

喷气燃料中2,6-二叔丁基对甲酚含量的测定 微分脉冲伏安法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

July 31, 2017

Implementation date

February 1, 2018

Scope

GB/T 34102-2017 is the English-translated version of 喷气燃料中2,6-二叔丁基对甲酚含量的测定 微分脉冲伏安法.

GB/T 34102-2017 is the Chinese standard "Determination of 2,6-ditertbutyl-p-cresol in jet fuels—Differential pulse voltammetry". Its scope clause reads: This standard specifies the use of differential pulse voltammetry jet fuel 2,6-di-tert-butyl-p-cresol antioxidant method.

This standard applies to 2,6-di-tert-butyl-p-cresol content of 8mg/L ~ 31mg/L of jet fuel. This standard can also be used beyond the scope of jet fuel 2,6-di-tert-butyl-p-cresol determination, but the precision did not do inspection. Its clauses include terms and definitions; method summary.

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Document preview — GB/T 34102-2017

National Standard of the People's Republic of China

ICS
75.160.20
Classification
E 31

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • 1 Scope
  • 2 Normative references
  • 3 Terms and definitions
  • 4 Method summary

1 Scope

This standard specifies the use of differential pulse voltammetry jet fuel 2,6-di-tert-butyl-p-cresol antioxidant method.

This standard applies to 2,6-di-tert-butyl-p-cresol content of 8mg/L ~ 31mg/L of jet fuel.

This standard can also be used beyond the scope of jet fuel 2,6-di-tert-butyl-p-cresol determination, but the precision did not do inspection.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version applies to this article

Pieces. For undated references, the latest edition (including all amendments) applies to this document.

GB/T 4756 Petroleum liquids - Manual sampling method

Petroleum products - Test methods - Determination of precision data

3 Terms and definitions

The following terms and definitions apply to this document.

3.1 Voltammetry

Electrochemical analysis based on the measurement of the current-voltage relationship (volt-ampere characteristic curve) during electrolysis using solid electrodes.

3.2 Differential pulse voltammetry

Using a solid electrode, a fixed voltage pulse with a smaller amplitude is periodically superimposed on a DC voltage linearly increasing with time to

Determination of electrolysis process before and after the addition of current difference between the voltage - voltage based electrochemical analysis.

3.3 Composite electrode

An electrode that encapsulates a working electrode, an auxiliary electrode and a reference electrode on one electrode body.

4 Method summary

Jet fuel was added to a specific electrolyte solution, using the specified composite electrode, differential pulse voltammetry 2,6-di-tert-butyl-methyl

Determination of phenol antioxidants. Differential pulse voltammetry analysis, when the working electrode voltage is higher than the oxidation potential of the antioxidant, the antioxidant is oxygen

As a result, the anodic current increases, forming an oxidation voltammetric peak of the anode current with the change of the scanning voltage. Peak voltammetry peak current and solution resistance […]

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

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