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GB/T 31125-2014Test method of adhesive tapes—Loop tack (English PDF)

胶粘带初粘性试验方法 环形法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

September 3, 2014

Implementation date

January 1, 2015

Scope

GB/T 31125-2014 is the English-translated version of 胶粘带初粘性试验方法 环形法.

GB/T 31125-2014 is the Chinese standard "Test method of adhesive tapes - Loop tack". Its scope clause reads: This standard specifies a test method for determining the initial tack of adhesive tapes, by the loop tack method.

This standard applies to the determination of the initial tack of adhesive tapes. It can be used for product quality control and research. Its clauses include terms and definitions; principles; categories; method a: tensile testing machine method; method b: automatic loop tack testing machine method.

It was issued by the General Administration of Quality Supervision, Inspection and Quarantine on SEPTEMBER 03, 2014 and took effect on JANUARY 01, 2015.

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Document preview — GB/T 31125-2014

National Standard of the People's Republic of China

ICS
83.180
Classification
G 38

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Foreword3
  • 1 Scope4
  • 2 Normative references4
  • 3 Terms and definitions4
  • 4 Principles4
  • 5 Categories5
  • 6 Method A: Tensile testing machine method5
  • 7 Method B: Automatic loop tack testing machine method9

1 Scope

This standard specifies a test method for determining the initial tack of adhesive tapes, by the loop tack method.

This standard applies to the determination of the initial tack of adhesive tapes. It can be used for product quality control and research.

2 Normative references

The following documents are essential to the application of this document. For the dated documents, only the versions with the dates indicated are applicable to this document; for the undated documents, only the latest version (including all the amendments) is applicable to this standard.

GB/T 2523-2008 Measuring method of surface roughness and peak count for cold-rolled metal sheet (strip)

GB/T 3280-2007 Cold rolled stainless steel plate, sheet and strip

GB/T 22396 Terminology relating to pressure sensitive adhesive products

3 Terms and definitions

The terms and definitions as defined in GB/T 22396, as well as the following terms and definitions, apply to this document.

3.1 Loop tack

The separation force, after contacting a loop adhesive tape material (adhesive side outwards) with a standard test panel of a certain area, at a certain speed.

4 Principles

The loop adhesive tape is brought into contact with the test panel of the specified area, under the action of its own weight, to measure the force to pull the adhesive tape away from the test panel

6 Method A: Tensile testing machine method

6.4.8 The failure modes of the bonding between the specimen ring and the test panel are divided into three cases: interface failure, cohesive failure, transfer failure.

6.4.9 After the test is completed, use reagents, to clean the stainless steel test panel in the test fixture. Use dust-free cloth to cover the stainless steel test panel, to prevent the surface from being scratched.

6.3.1 Specimen ring

6.3.1.1 Size of specimen ring: Width 24 mm, circumference 175 mm.

6.3.1.3 If the test sample is an unsupported adhesive tape, it is necessary to transfer the sample to a 0.05 mm PET film, to make a specimen ring. The PET film is used here as the support carrier, for the unsupported adhesive tape.

6.3.1.2 Number of specimen rings: At least 3

6.3.2 Test panel

6.3.2.1 The thickness of the stainless steel test panel is 1.5 mm ~ 2.0 mm; the width is 24 mm; the length is 100 mm.

6.3.2.2 The material of the stainless steel test panel is the 0Cr18Ni9 or 1Cr18Ni9Ti test panel, which is specified in GB/T 3280-2007. The surface roughness (GB/T 2523-2008) is (50 ± 25) nm. When there is permanent contamination or scars on the surface of the test panel, replace it in time.

6.3.2.3 If PVC, ABS, PE, glass materials are used for the test panel, the material and surface conditions shall be stated in the test report.

6.3.2.4 The stainless steel test panel, which is fixed by the fixture, shall be able to accommodate the bonding area of 24 mm × 24 mm.

6.3.3 Cleaning agents and wiping materials
6.3.3.1 Cleaning agent

One or more of the following solvents:

- Diacetone alcohol (4-hydroxy-4-methyl-2-pentanone);

- Isopropyl alcohol;

- Methanol;

- Methyl ethyl ketone;

- Acetone;

- N-heptanone;

- Mixture off n-heptane and a fluorinated hydrocarbon (e.g.: refrigerant) (applicable under conditions of toxicity or flammability restrictions).

Solvents are of common chemical grade AND placed in suitable containers.

6.5 Test results

From the adhesive tape sample, collect the data from at least three specimen rings. The initial viscosity shall be expressed as the average value of the maximum tensile force of the specimen rings, in the unit of N.

6.6 Test report

The test report contains the following items:

a) Test methods;

b) Information of adhesive tape sample;

c) Reagents and cleaning methods used for cleaning stainless steel sheets;

d) Dwelling time of sample;

e) Type and thickness of adhesive tape, unit: mm;

f) Support material for the adhesive tape;

g) Release paper used for adhesive tape;

h) Dwelling time during the test of the specimen ring;

i) Average value of tensile force, unit: N;

j) Visual failure mode;

k) Non-standard test conditions.

7 Method B: Automatic loop tack testing machine method

7.4.2 Turn on the power switch.

7.4.3 Confirm that the upper gripper is at the topmost position.

7.4.4 Loosen the fixing screw. Then remove the stainless steel test panel.

7.4.5 Put the cleaned stainless steel test panel back into the test fixture. Tighten the fixing screws.

7.4.6 Peel off the release paper, which covers the specimen.

7.4.7 Turn the specimen completely over, taking care not to crease it. Bend the specimen into a teardrop-shaped annular specimen ring, which has a perimeter of 98 mm. The adhesive side faces outside, as shown in Figure 6.

7.4.8 Use a 13 mm wide adhesive tape, to fasten the ends of the specimen ring together.

7.4.9 Insert the specimen ring into the upper gripper, to ensure that the specimen ring is in the proper position, to form the upper assembly.

7.4.10 Zero the dynamometer, according to the manufacturer's instructions.

7.4.11 Long press the "Inching" button, to make the upper assembly start to move downwards. The upper assembly stops automatically, after completing a complete cycle. At this point, the dynamometer returns to its initial position.

7.4.12 A complete cycle begins with the upper assembly moving down; the specimen ring contacts with the test panel, to form a bond. Then, the assembly is moved upward, at a speed of 300 mm/min ± 10 mm/min. The dynamometer records the tensile force, which is required to pull the specimen ring away from the test panel. At the end of a […]

7.1 Test devices

Figure 5 is a schematic diagram of an automatic loop tack performance testing machine. […]

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

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