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GB/T 29748-2013Coal direct liquefaction - Determination of ash in coal liquefaction residue (English PDF)

煤炭直接液化 液化残渣灰分的测定方法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

September 18, 2013

Implementation date

March 1, 2014

Scope

GB/T 29748-2013 is the English-translated version of 煤炭直接液化 液化残渣灰分的测定方法.

GB/T 29748-2013 is the Chinese standard "Coal direct liquefaction - Determination of ash in coal liquefaction residue".

Its scope clause reads: This standard specifies the determination of the terms and definitions of direct coal liquefaction residue ash, Method summary, reagents and materials, equipment, measuring step Suddenly, the results of the calculation, method precision and test reports.

This standard applies to the determination of direct coal liquefaction residue of ash. Its clauses include terms and definitions; method summary; reagents and materials.

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Document preview — GB/T 29748-2013

National Standard of the People's Republic of China

ICS
73.040
Classification
D 21

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • 1 Scope
  • 2 Normative references
  • 3 Terms and Definitions
  • 4 Method summary
  • 5 Reagents and materials

1 Scope

This standard specifies the determination of the terms and definitions of direct coal liquefaction residue ash, Method summary, reagents and materials, equipment, measuring step

Suddenly, the results of the calculation, method precision and test reports.

This standard applies to the determination of direct coal liquefaction residue of ash.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein

Member. For undated references, the latest edition (including any amendments) applies to this document.

GB/T 23251-2009 coal chemical coal Technical Guidelines

3 Terms and Definitions

GB/T 23251-2009 define the following terms and definitions apply to this document.

3.1 Direct coal liquefaction

Coal under the action of high pressure, high temperature and the hydrogenation reaction catalyst with hydrogen, whereby liquid fuel directly into the process.

[GB/T 23251-2009, the definition 3.8]

3.2 CLR coalliquefactionresidue

Direct coal liquefaction product by heavy liquid separation (mainly for the vacuum distillation) after solid mixture containing liquefied heavy oil, bitumen class

Substances, unconverted organic matter in coal, minerals and catalyst.

3.3 Liquefaction residue ash

After liquefaction residue under specified conditions for complete combustion resulting residue accounted for liquefaction residue mass fraction.

4 Method summary

Weigh a certain amount of liquefaction residue sample, placed in a muffle furnace at a certain speed was raised to 500 °C and stay 30min, continue to heat up

To 850 °C, ignition to constant mass, the mass fraction remaining after burning a sample substances accounted for as liquefaction residue ash.

5 Reagents and materials

5.1 Crucible

porcelain, 50mL. Mouth outer diameter 52mm, high 46mm, bottom outside diameter 30mm (see Fig. 1).

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

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