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GB/T 24981.2-2020Test methods of rare earth long afterglow phosphors—Part 2: Determination of afterglow brightness (English PDF)

稀土长余辉荧光粉试验方法 第2部分:余辉亮度的测定

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

November 19, 2020

Implementation date

October 1, 2021

Scope

GB/T 24981.2-2020 is the English-translated version of 稀土长余辉荧光粉试验方法 第2部分:余辉亮度的测定.

GB/T 24981.2-2020 is the part of the Chinese series of test methods for rare earth long afterglow phosphors that determines the afterglow brightness. It gives the principle of the method, the terms and definitions, the instruments and devices, the sample preparation, the test procedure and the precision.

It applies to the determination of the afterglow brightness of these phosphors. Phosphor makers and test laboratories use it. Issued on 19 November 2020, it has applied since 1 October 2021, replacing GB/T 24981.2-2010.

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Document preview — GB/T 24981.2-2020

National Standard of the People's Republic of China

ICS
77.120.99
Classification
H 14
Replacing
GB/T 24981.2-2010

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Foreword3
  • 1 Scope5
  • 2 Method principle5
  • 3 Terms and definitions5
  • 4 Instruments and devices5
  • 5 Sample preparation6
  • 6 Test procedures6
  • 7 Precision7

1 Scope

This Part of GB/T 24981 specifies the determination method of afterglow brightness of rare earth long afterglow phosphors.

This Part applies to the determination of the afterglow brightness of rare earth long afterglow phosphors.

2 Method principle

Use a light source of a color temperature of 5 500 K ~ 6 500 K as the excitation light source; use the specified illuminance to directly illuminate the sample.

When the sample is excited and saturated, turn off the excitation light source; use a luminance meter to measure it; record the brightness value of the afterglow fluorescence of the sample at the specified time interval, to get the afterglow brightness of the sample.

3 Terms and definitions

The following terms and definitions are applicable to this document.

3.1 Saturating excitation

The excitation light source is 5 500 K ~ 6 500 K light source (xenon lamp, fluorescent lamp, LED lamp). Extend the excitation time, and the afterglow brightness of the phosphor changes within 5%.

4 Instruments and devices

4.1 Illumination test device

The illumination test device shall meet the following conditions:

a) The measurement range is 10 lx ~ 1 x 10^5 lx; the accuracy shall meet the requirements of the national grade-1 illuminometer. […]

6 Test procedures

6.1.3 During the measurement process, except for the illumination of the excitation light source within the specified excitation time, stray light interference such as visible light or ultraviolet light is not allowed.

6.2 Illumination correction

Turn on the light source and stabilize for 10 min ~ 30 min according to the requirements of the instrument. Place the photometric probe of the illumination test device on the sample to be excited; adjust the light source; ensure that the average illumination illuminating the tested sample is stable at 1 000 lx ± 5 lx or 25 lx ± 0.5 lx.

6.3 Afterglow brightness test

6.3.1 Load the sample into the sample pan; compact and make the surface flat.

6.3.2 Place the sample pan at the place to be excited, so that the sample is irradiated by the light source to reach a saturated excitation state; the excitation illumination on the test surface of the sample shall meet the requirements of 4.1c).

6.3.3 Turn off the light source; immediately use the afterglow brightness test device to test the afterglow brightness of the sample; record the afterglow brightness values of 10 min, 30 min, and 60 min. If the buyer has special requirements, the supplier and the buyer shall negotiate and determine.

6.3.4 Do 3 parallel tests; take the arithmetic average. The relative deviation of the test results shall not exceed 5%.

7 Precision

7.1 Repeatability

For the measured values of the afterglow brightness of two independent tests that are obtained under repeatability conditions, within the average range given below, the absolute difference between these two test results does not exceed the repeatability limit (r); the case of exceeding the repeatability limit (r) is not more than 5%; the repeatability limit (r) is obtained by linear interpolation according to the data in Table 1. […]

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

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Editions of GB/T 24981.2

EditionTitleRevisionStatus
GB/T 24981.2-2020Test methods of rare earth long afterglow phosphors—Part 2: Determination of afterglow brightnesscurrent editionCurrent
GB/T 24981.2-2010Test methods of rare earth long afterglow phosphors—Part 2: Determination of afterglow brightnessprevious editionSuperseded

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