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GB/T 24981.1-2020Test methods of rare earth long afterglow phosphors—Part 1: Determination of emission dominantpeak and chromaticity coordinates (English PDF)

稀土长余辉荧光粉试验方法 第1部分:发射主峰和色品坐标的测定

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

November 19, 2020

Implementation date

October 1, 2021

Scope

GB/T 24981.1-2020 is the English-translated version of 稀土长余辉荧光粉试验方法 第1部分:发射主峰和色品坐标的测定.

GB/T 24981.1-2020 is the part of the Chinese series of test methods for rare earth long afterglow phosphors that determines the emission dominant peak and the chromaticity coordinates.

It gives the principle of the method, the instruments and devices, the test procedure and the precision. It applies to the determination of the emission dominant peak and chromaticity coordinates of these phosphors.

Phosphor makers and test laboratories use it. Issued on 19 November 2020, it has applied since 1 October 2021, replacing GB/T 24981.1-2010.

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Document preview — GB/T 24981.1-2020

National Standard of the People's Republic of China

ICS
77.120.99
Classification
H 14
Replacing
GB/T 24981.1-2010

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Foreword3
  • 1 Scope4
  • 2 Method principle4
  • 3 Instruments and devices4
  • 4 Test procedures5
  • 5 Precision6
  • References7

1 Scope

This Part of GB/T 24981 specifies the determination method of emission dominantpeak and chromaticity coordinates of rare earth long afterglow phosphors.

This Part applies to the determination of emission dominantpeak and chromaticity coordinates of rare earth long afterglow phosphors.

2 Method principle

The sample emits visible light of 380 nm ~ 720 nm under the excitation of 365 nm ultraviolet rays; the monochromatic light signal is converted into an electrical signal by the spectral radiation tester for spectroscopy and photoelectric conversion; then, the electrical signal value corresponding to the light intensity is obtained by correction of the standard lamp. Measure the entire visible light band at a certain wavelength interval; obtain the relative emission spectral power distribution of the sample in the entire visible light band; calculate the chromaticity coordinates and emission dominantpeak of the light emitted by the sample with reference to CIE 1931.

3 Instruments and devices

3.1 Spectral radiation tester

The spectral radiation tester shall meet the following conditions:

a) Wavelength accuracy: ±2 nm;

b) Accuracy of chromaticity coordinates: ±0.001;

c) Spectral range: 380 nm ~ 720 nm.

3.2 Excitation light source

The 365 nm ultraviolet low pressure mercury lamp is equipped with a color filter; the peak transmittance of the filter shall be greater than 10%; transmittance of 380 nm ~ 720 nm shall not be greater than 0.01%; the radiation intensity stability of 365 nm shall be better than 0.2%/10 min, otherwise, it shall be compensated.

3.3 Sample pan

The sample pan is black, with an inner diameter of 20 mm and a depth of 3 mm.

4 Test procedures

4.1 Test conditions

4.1.1 Ambient temperature: 22 °C ~ 27 °C

4.1.2 Relative humidity: <=70%

4.1.3 During the measurement process, in addition to the specified excitation light source, there shall be no stray light interference such as visible light or ultraviolet light.

4.2 Instrument calibration

Be stable for 10 min ~ 30 min according to the requirements of the instrument. Refer to the instrument manual to calibrate the instrument.

4.3 Test

4.3.1 Load the sample into the sample pan; compact and make the surface flat.

4.3.2 Place the sample pan in the sample chamber to be excited, so that the sample is excited by the ultraviolet lamp.

4.3.3 Irradiate the sample under an ultraviolet lamp for more than 1 min; scan from the 380 nm ~ 720 nm wavelength range; measure the relative spectral power distribution of the sample and the peak wavelength of the emission dominantpeak. The emission dominantpeak is expressed by the peak wavelength (lambda).

4.3.4 According to the measured relative spectral power distribution, calculate the chromaticity coordinates (x, y) with reference to CIE 1931.

4.3.5 Repeat the test 3 times for a sample; take the arithmetic mean value. […]

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

Similar standards

Editions of GB/T 24981.1

EditionTitleRevisionStatus
GB/T 24981.1-2020Test methods of rare earth long afterglow phosphors—Part 1: Determination of emission dominantpeak and chromaticity coordinatescurrent editionCurrent
GB/T 24981.1-2010Test methods of rare earth long afterglow phosphors—Part 1: Determination of emission dominantpeak and chromaticity coordinatesprevious editionSuperseded

This page sells the current edition, GB/T 24981.1-2020. Earlier editions are listed for reference only.

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