GB/T 2467-2008Pyrites and concentrate - Determination of lead content - Flame atomic absorption spectrometric and EDTA volumetric methods (English PDF)
硫铁矿和硫精矿中铅含量的测定 火焰原子吸收光谱法和EDTA容量法
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Issued by
SAMR; SAC
Level / Type
National · Recommended
Issue date
May 14, 2008
Implementation date
October 1, 2008
Scope
GB/T 2467-2008 is the English-translated version of 硫铁矿和硫精矿中铅含量的测定 火焰原子吸收光谱法和EDTA容量法.
GB/T 2467-2008 is the Chinese standard "Pyrites and concentrate - Determination of lead content - Flame atomic absorption spectrometric and EDTA volumetric methods".
Its scope clause reads: This standard specifies the flame atomic absorption spectrometric and EDTA volumetric method Pyrites and concentrate of lead content.
This standard flame atomic absorption spectrometry applied to the lead content of 0.01% to 1% Pyrites and concentrate products, EDTA content Method for the determination of Pyrites and concentrate products lead content greater than 0.1%. Its clauses include sample; general provisions; analysis.
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Document preview — GB/T 2467-2008
National Standard of the People's Republic of China
- ICS
- 73.060.01
- Classification
- D 51
- Replacing
- GB/T 2467.3-1996
Issued by: State Administration for Market Regulation; Standardization Administration of the PRC
Contents
- 1 Scope
- 2 Normative references
- 3 Sample
- 4 General Provisions
- 5 Analysis
1 Scope
This standard specifies the flame atomic absorption spectrometric and EDTA volumetric method Pyrites and concentrate of lead content.
This standard flame atomic absorption spectrometry applied to the lead content of 0.01% to 1% Pyrites and concentrate products, EDTA content
Method for the determination of Pyrites and concentrate products lead content greater than 0.1%.
2 Normative references
The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent
Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research
Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.
Preparation of GB/T 601 chemical reagent standard titration solution
GB/T 6003.1 woven wire mesh test sieve (GB/T 6003.1-1997, eqv ISO 3310-1.1990)
GB/T 6682 analytical laboratory use specifications and test methods (GB/T 6682-1992, neq ISO 3696. 1987)
GB/T 9723 Chemicals flame atomic absorption spectrometry General
3 Sample
The sample passes through 150µm test sieve (GB/T 6003.1), at 100 °C ~ 105 °C drying to constant weight, placed in a desiccator, cooled to
Room temperature.
4 General Provisions
The water of this standard shall comply with GB/T 6682 water in three specifications; reagents listed Unless otherwise specified, refer to analytical reagent.
5 Analysis
5.1 Flame Atomic Absorption Spectrometry
5.1.1 Method summary
Samples with hydrochloric acid - nitric acid is dissolved in dilute hydrochloric acid medium, using air - acetylene flame atomic absorption spectrometer at a wavelength of 283.3nm
The absorbance was measured to determine the lead content of working curve method.
5.1.2 Reagents and solutions
5.1.2.1
hydrochloric acid.
5.1.2.2 hydrochloric acid solution
1 + 1.
5.1.2.3
nitrate.
5.1.2.4 Lead standard solution
1.00mg/mL. Weigh 1.0000g purity metal lead in 250mL beaker, add 40mL of nitric acid
Solution (1 + 1), cover the surface of the pan, heat to dissolve completely cooled and transferred to 1000mL volumetric flask, dilute to the mark, shake. This solution
Liquid lead (Pb) amount of 1.00mg/mL.
5.1.2.5
Lead standard solution.200µg/mL. Draw 100.0mL lead standard solution (5.1.2.4) in 500mL flask with water
Dilute to the mark. This solution is lead (Pb) the amount of 200µg/mL.
GB/T 1868-1995 | GB/T 1870-1995 | GB/T 1873-1995 | GB/T 2468-2008 | GB/T 2466-2008 | GB/T 2463-2008 | […]
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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.
Similar standards
Editions of GB/T 2467
| Edition | Title | Revision | Status |
|---|---|---|---|
| GB/T 2467-2008 | Pyrites and concentrate - Determination of lead content - Flame atomic absorption spectrometric and EDTA volumetric methods | current edition | Current |
| GB/T 2467.3-1996 | Pyrites and concentrate - Determination of lead content - Flame atomic absorption spectrometric and EDTA volumetric methods | previous edition | Superseded |
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