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GB/T 2467-2008Pyrites and concentrate - Determination of lead content - Flame atomic absorption spectrometric and EDTA volumetric methods (English PDF)

硫铁矿和硫精矿中铅含量的测定 火焰原子吸收光谱法和EDTA容量法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

May 14, 2008

Implementation date

October 1, 2008

Scope

GB/T 2467-2008 is the English-translated version of 硫铁矿和硫精矿中铅含量的测定 火焰原子吸收光谱法和EDTA容量法.

GB/T 2467-2008 is the Chinese standard "Pyrites and concentrate - Determination of lead content - Flame atomic absorption spectrometric and EDTA volumetric methods".

Its scope clause reads: This standard specifies the flame atomic absorption spectrometric and EDTA volumetric method Pyrites and concentrate of lead content.

This standard flame atomic absorption spectrometry applied to the lead content of 0.01% to 1% Pyrites and concentrate products, EDTA content Method for the determination of Pyrites and concentrate products lead content greater than 0.1%. Its clauses include sample; general provisions; analysis.

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Document preview — GB/T 2467-2008

National Standard of the People's Republic of China

ICS
73.060.01
Classification
D 51
Replacing
GB/T 2467.3-1996

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • 1 Scope
  • 2 Normative references
  • 3 Sample
  • 4 General Provisions
  • 5 Analysis

1 Scope

This standard specifies the flame atomic absorption spectrometric and EDTA volumetric method Pyrites and concentrate of lead content.

This standard flame atomic absorption spectrometry applied to the lead content of 0.01% to 1% Pyrites and concentrate products, EDTA content

Method for the determination of Pyrites and concentrate products lead content greater than 0.1%.

2 Normative references

The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent

Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research

Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.

Preparation of GB/T 601 chemical reagent standard titration solution

GB/T 6003.1 woven wire mesh test sieve (GB/T 6003.1-1997, eqv ISO 3310-1.1990)

GB/T 6682 analytical laboratory use specifications and test methods (GB/T 6682-1992, neq ISO 3696. 1987)

GB/T 9723 Chemicals flame atomic absorption spectrometry General

3 Sample

The sample passes through 150µm test sieve (GB/T 6003.1), at 100 °C ~ 105 °C drying to constant weight, placed in a desiccator, cooled to

Room temperature.

4 General Provisions

The water of this standard shall comply with GB/T 6682 water in three specifications; reagents listed Unless otherwise specified, refer to analytical reagent.

5 Analysis

5.1 Flame Atomic Absorption Spectrometry

5.1.1 Method summary

Samples with hydrochloric acid - nitric acid is dissolved in dilute hydrochloric acid medium, using air - acetylene flame atomic absorption spectrometer at a wavelength of 283.3nm

The absorbance was measured to determine the lead content of working curve method.

5.1.2 Reagents and solutions
5.1.2.1

hydrochloric acid.

5.1.2.2 hydrochloric acid solution

1 + 1.

5.1.2.3

nitrate.

5.1.2.4 Lead standard solution

1.00mg/mL. Weigh 1.0000g purity metal lead in 250mL beaker, add 40mL of nitric acid

Solution (1 + 1), cover the surface of the pan, heat to dissolve completely cooled and transferred to 1000mL volumetric flask, dilute to the mark, shake. This solution

Liquid lead (Pb) amount of 1.00mg/mL.

5.1.2.5

Lead standard solution.200µg/mL. Draw 100.0mL lead standard solution (5.1.2.4) in 500mL flask with water

Dilute to the mark. This solution is lead (Pb) the amount of 200µg/mL.

GB/T 1868-1995 | GB/T 1870-1995 | GB/T 1873-1995 | GB/T 2468-2008 | GB/T 2466-2008 | GB/T 2463-2008 | […]

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

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Editions of GB/T 2467

EditionTitleRevisionStatus
GB/T 2467-2008Pyrites and concentrate - Determination of lead content - Flame atomic absorption spectrometric and EDTA volumetric methodscurrent editionCurrent
GB/T 2467.3-1996Pyrites and concentrate - Determination of lead content - Flame atomic absorption spectrometric and EDTA volumetric methodsprevious editionSuperseded

This page sells the current edition, GB/T 2467-2008. Earlier editions are listed for reference only.

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