GB/T 2466-2008Pyrites and concentrate - Determination of copper content - Flame atomic absorption spectrometric and spectrophotometric methods (English PDF)
硫铁矿和硫精矿中铜含量的测定 火焰原子吸收光谱法和分光光度法
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Issued by
SAMR; SAC
Level / Type
National · Recommended
Issue date
May 14, 2008
Implementation date
October 1, 2008
Scope
GB/T 2466-2008 is the English-translated version of 硫铁矿和硫精矿中铜含量的测定 火焰原子吸收光谱法和分光光度法.
GB/T 2466-2008 is the Chinese standard "Pyrites and concentrate - Determination of copper content - Flame atomic absorption spectrometric and spectrophotometric methods".
Its scope clause reads: This standard specifies the flame atomic absorption spectrometry and spectrophotometric determination of pyrite and sulfur concentrate copper content.
This standard applies to pyrite and sulfur concentrate products in the determination of copper content of 0.01% to 1%. Its clauses include sample; general provisions; analytical methods.
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Document preview — GB/T 2466-2008
National Standard of the People's Republic of China
- ICS
- 73.060.01
- Classification
- D 51
- Replacing
- GB/T 2466.3-1996
Issued by: State Administration for Market Regulation; Standardization Administration of the PRC
Contents
- 1 Scope
- 2 Normative references
- 3 sample
- 4 general provisions
- 5 analytical methods
1 Scope
This standard specifies the flame atomic absorption spectrometry and spectrophotometric determination of pyrite and sulfur concentrate copper content.
This standard applies to pyrite and sulfur concentrate products in the determination of copper content of 0.01% to 1%.
2 Normative references
The following documents contain provisions which, through reference in this standard and become the standard terms. All dated references, which are subsequently owned
Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to reach an agreement based on this standard research
Whether you can use the latest versions of these files. For undated references, the latest version applies to this standard.
GB/T 6003.1 woven wire mesh test sieve (GB/T 6003.1-1997, eqv ISO 3310-1..1990)
GB/T 6682 analytical laboratory water specifications and test methods (GB/T 6682-1992, neq ISO 3696. 1987)
GB/T 9721 chemical reagent molecular absorption spectrophotometry (UV and visible light part)
GB/T 9723 chemical reagent flame atomic absorption spectrometric method
3 sample
The sample was passed 150µm test sieve (GB/T 6003.1), dried at 100 °C ~ 105 °C to constant weight, placed in a desiccator, cooled to
Room temperature.
4 general provisions
The water used in this standard should be consistent with the three water GB/T 6682 specifications; listed reagents except for special provisions, are analytically pure reagents.
5 analytical methods
5.1 Flame atomic absorption spectrometry
5.1.1 Method summary
The sample was dissolved with hydrochloric acid-nitric acid, air-acetylene flame was used in a dilute hydrochloric acid medium, at a wavelength of 324.8 nm of an atomic absorption spectrometer
Absorbance was measured to determine the copper content by the working curve method.
5.1.2 Reagents and solutions
5.1.2.1
Hydrochloric acid.
5.1.2.2 hydrochloric acid solution
1 +1.
5.1.2.3
Nitric acid.
5.1.2.4 Copper standard solution
1.00mg/mL. Weigh 1.0000g of high-purity metallic copper in 250mL beaker, add 40mL nitric acid
Solution (1 + 1), cover the watch glass, heated to dissolve completely, cooled, transferred to 1000mL volumetric flask, diluted with water to the mark, shake. This solution
Liquid copper (Cu) content of 1.00mg/mL.
5.1.2.5 copper standard solution
100µg/mL. Pipette 50.0mL copper standard solution (5.1.2.4) in 500mL volumetric flask, diluted with water
Release to the mark, shake well. This solution contains copper (Cu) amount 100µg/mL.
5.1.3 Instruments
Flame atomic absorption spectrometer. should be consistent with the provisions of GB/T 9723.
GB/T 1868-1995 | GB/T 1870-1995 | GB/T 1873-1995 | GB/T 2468-2008 | GB/T 2467-2008 | GB/T 2463-2008 | […]
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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.
Similar standards
Editions of GB/T 2466
| Edition | Title | Revision | Status |
|---|---|---|---|
| GB/T 2466-2008 | Pyrites and concentrate - Determination of copper content - Flame atomic absorption spectrometric and spectrophotometric methods | current edition | Current |
| GB/T 2466.3-1996 | Pyrites and concentrate - Determination of copper content - Flame atomic absorption spectrometric and spectrophotometric methods | previous edition | Superseded |
This page sells the current edition, GB/T 2466-2008. Earlier editions are listed for reference only.
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