GB/T 20772-2008Determination of 461 pesticides and related chemicals residues in animal muscles - LC-MS-MS method (English PDF)

1 Scope

This standard specifies the pork, beef, lamb, rabbit, chicken 461 pesticides and related chemicals (see Appendix A and Appendix E) residues

Allowance liquid chromatography - tandem mass spectrometry.

This standard applies to qualitative identification of pork, beef, lamb, rabbit, chicken 461 pesticides and related chemicals, and 396 kinds of pesticides

Quantitative determination of relevant chemical residues.

396 kinds of pesticides and related chemicals present standard quantitative determination of detection limit of 0.04µg/kg ~ 4.82mg/kg (see Appendix A).

2 Normative references

The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent

Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research

Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.

GB/T 6379.1 measurement methods and results of Accuracy (trueness and precision) - Part 1. General principles and definitions (GB/T 6379.1-

2004, ISO 5725-1.1994, IDT)

GB/T 6379.2 measurement methods and results of Accuracy (trueness and precision) - Part 2. Determine the standard measurement method to repeat

Of the basic methods of reproduction (GB/T 6379.2-2004, ISO 5725-2.1994, IDT)

GB/T 6682 analytical laboratory use specifications and test methods (GB/T 6682-2008, ISO 3696. 1987, MOD)

GB/T 9695.19 Meat and meat products - Sampling Methods

Principle 3

Cyclohexane - ethyl acetate extract homogeneous sample, purified by gel permeation chromatography, liquid chromatography - tandem mass spectrometer, external standard.

4 Reagents and materials

Water as a water GB/T 6682 regulations.