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GB/T 19650-2006Method for determination of 478 pesticides and related chemicals residues in animal muscles - GC-MS method (English PDF)

动物肌肉中478种农药及相关化学品残留量的测定 气相色谱-质谱法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

December 31, 2006

Implementation date

March 1, 2007

Scope

GB/T 19650-2006 is the English-translated version of 动物肌肉中478种农药及相关化学品残留量的测定 气相色谱-质谱法.

GB/T 19650-2006 is the Chinese standard "Method for determination of 478 pesticides and related chemicals residues in animal muscles - GC-MS method".

Its scope clause reads: This standard specifies the pork, mutton,, rabbit, beef, chicken in 478 kinds of pesticides and related chemicals (see Appendix A) the amount of residual gas chromatography-mass spectrometry.

This standard applies to pork, chicken Determination 478 kinds of pesticides and related chemicals residues, mutton,, rabbit beef.

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Document preview — GB/T 19650-2006

National Standard of the People's Republic of China

Classification
X 04
Replacing
GB/T 19650-2005

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Foreword
  • 1 Scope
  • 2 Normative references
  • 3 Principle
  • 4 Reagents and materials
  • 5 Apparatus
  • 6 Preparation and preservation of the test specimens
  • 7 Determination procedure
  • 8 Calculation of the results
  • 9 Precision
  • Annex A (informative) Table of the limits of detection of the method, the grouping, the solvent selection and the concentrations of the mixed standard solutions for the 478 pesticides and related chemicals
  • Annex B (informative) Retention times, quantitative ions, qualitative ions and abundance ratios of the quantitative ions to the qualitative ions of the 478 pesticides and related chemicals and of the internal standard compounds
  • Annex C (informative) Selected ion monitoring grouping table of the five groups A, B, C, D and E of pesticides and related chemicals determined by GC-MS
  • Annex D (informative) Selected ion monitoring GC-MS chromatogram of the reference materials in a chicken meat matrix
  • Annex E (informative) Table of the precision data of the 478 pesticides and related chemicals
  • Annex F (informative) Comparison index of the English and Chinese names of the 478 pesticides and related chemicals

3 Principle

4 Reagents and materials

5 Apparatus

6 Preparation and preservation of the test specimens

7 Determination procedure

8 Calculation of the results

9 Precision

Foreword

This document was issued on 31 December 2006 by the State Administration for Market Regulation and the Standardization Administration of the People's Republic of China, and has been in force since 1 March 2007.

It replaces GB/T 19650-2005.

The document is under the responsibility of the Ministry of Agriculture and Rural Affairs.

Classification: CCS X 04.

About this edition

GB/T 19650-2006 is the current edition. It was issued on 31 December 2006 and has been in force since 1 March 2007, replacing GB/T 19650-2005.

GB/T 19650-2005 has been superseded: a specification that still cites it is citing a withdrawn edition.

The interval between issue and effect is the transition period. It exists so that producers, laboratories and buyers can requalify products, revise procedures and use up documentation before the new text becomes the one that applies. The date on this page is the official one from the record of the Standardization Administration.

Edition history and citation

GB/T 19650-2006 replaces GB/T 19650-2005. A specification, drawing or test report that cites the older number is pointing at a document that is no longer the one in force, and the two editions can differ in requirements, in test methods or in scope.

Where an edition is replaced, the Chinese standardization system keeps the number and changes the year: the number identifies the subject, the year identifies the text. That is why a citation without a year is ambiguous and a citation with one is not.

Classification and status

GB/T 19650-2006 carries no ICS number in the official record.

Its Chinese Standard Classification code is CCS X 04. CCS is the domestic scheme, a letter for the sector and two digits for the subject within it, and it is the code by which the standard is filed and searched in China.

The GB/T prefix marks a recommended national standard. It is not, in itself, law: it becomes binding when a contract names it, when a regulation or a mandatory standard refers to it, or when a producer declares conformity with it. In practice that covers most of the cases in which it will be read — a purchase specification, an inspection agreement or a certification scheme.

The document is under the responsibility of the Ministry of Agriculture and Rural Affairs, which is the body that maintains it and that will answer a formal question about its interpretation.

How this standard is designated

The full designation is GB/T 19650-2006. A citation should carry the number with its year, because the year identifies the text that applies.

In a catalogue or a filing system it is found under CCS X 04, the Chinese classification scheme by which a standard on this subject is filed and searched.

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 50 pages — is available in the English PDF.

Referenced standards

Similar standards

Editions of GB/T 19650

EditionTitleRevisionStatus
GB/T 19650-2006Method for determination of 478 pesticides and related chemicals residues in animal muscles - GC-MS methodcurrent editionCurrent
GB/T 19650-2005Method for determination of 478 pesticides and related chemicals residues in animal muscles - GC-MS methodprevious editionSuperseded

This page sells the current edition, GB/T 19650-2006. Earlier editions are listed for reference only.

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