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GB/T 16145-2022Gamma-ray spectrometry method for the determination of radionuclides in environmental and biological samples (English PDF)

环境及生物样品中放射性核素的γ能谱分析方法

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Issued by

State Administration for Market Regulation; Standardization Administration of China

Level / Type

National · Recommended

Issue date

December 30, 2022

Implementation date

July 1, 2023

Scope

GB/T 16145-2022 is the English-translated version of 环境及生物样品中放射性核素的γ能谱分析方法.

GB/T 16145-2022 is the Chinese standard "Gamma-ray spectrometry method for the determination of radionuclides in environmental and biological samples".

Its scope clause reads: This document specifies the method for analyzing the activity concentration of gamma radionuclides in environmental and biological samples by high-purity germanium (HPGe) gamma spectrometer.

This document is applicable to the measurement of gamma radionuclide activity concentration in environmental and biological samples, similar to the measurement of gamma radionuclide activity in matrix samples.

The measurement of concentration is carried out according to the reference. Its clauses include terms and definitions.

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Document preview — GB/T 16145-2022

National Standard of the People's Republic of China

ICS
13.280
Classification
C57

Issued by: State Administration for Market Regulation; Standardization Administration of China

Contents

  • Preface
  • 1 Scope
  • 2 Normative references
  • 3 Terms and Definitions
  • 4 Summary of method
  • 5 Measurement system
  • 6 Energy Scale
  • 7 Efficiency Scale
  • 8 Sample preparation and measurement
  • 9 Gamma Spectroscopy
  • 10 Uncertainty assessment
  • 11 Results report
  • Appendix A (Informative) Monoenergetic and Polyenergetic Nuclides for Energy and Efficiency Calibration
  • Appendix B (informative) Example of a typical sample box for measuring low activity samples
  • Appendix C (Informative) Sample self-absorption correction method
  • Appendix D (Informative) Coincidence additive correction caused by cascading radiation
  • Appendix E (informative) Soil, sediment (sediment) sample collection, preparation and measurement
  • Appendix F (informative) Water sample collection, preparation and measurement
  • Appendix G (Informative) Collection, Preparation and Measurement of Biological Samples
  • Appendix H (Informative) Air Sample Collection, Preparation and Measurement
  • Appendix K (Informative) Examples of Uncertainty Evaluation Methods in gamma-ray Spectroscopy
  • Appendix L (informative) Detection limit

1 Scope

This document specifies the method for analyzing the activity concentration of gamma radionuclides in environmental and biological samples by high-purity germanium (HPGe) gamma spectrometer.

This document is applicable to the measurement of gamma radionuclide activity concentration in environmental and biological samples, similar to the measurement of gamma radionuclide activity in matrix samples.

The measurement of concentration is carried out according to the reference.

2 Normative references

This document has no normative references.

3 Terms and Definitions

The following terms and definitions apply to this document.

3.1 environmental sample

The basic link of the environmental system, the basic unit of the environmental structure.

Note. The environmental samples referred to in this document include water, air, soil, rocks, etc.

3.2 biological sample

Representative biological substances collected according to the requirements of bioradiation detection and used as test samples.

Note. The biological samples referred to in this document include food crops, fruits and vegetables, tea, grass, milk, mushrooms, livestock, poultry, indicative wild animals and plants and other terrestrial animals and plants

Fish, shrimp, crab, algae and other aquatic organisms in sea or fresh water, as well as human and animal hair, tissue, blood and excrement, etc.

3.3 energy calibration

The process of determining the corresponding relationship between the gamma ray energy of the gamma spectrometer system and the track site.

3.4

For a given measurement condition and gamma-ray energy, the net counts within the detected full-energy peak are comparable to those emitted by the radiation source during the same time interval.

The ratio of the total number of gamma photons of this energy.

3.5

Under the given measurement conditions, establish the relationship curve between gamma-ray energy and its all-energy peak efficiency, or determine some specific nuclide calibration coefficients.

3.6 radioactive aerosol

Dispersion system formed by solid or liquid radioactive particles suspended in air or gaseous medium.

3.7 Detection limit detection limit; DL

The lowest activity that can be detected by a spectrometer at a given confidence level.

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 45 pages — is available in the English PDF.

Referenced standards

Similar standards

Editions of GB/T 16145

EditionTitleRevisionStatus
GB/T 16145-2022Gamma-ray spectrometry method for the determination of radionuclides in environmental and biological samplescurrent editionCurrent
GB/T 16145-2020Gamma spectrometry method of analysing radionuclides in biological samplesprevious editionSuperseded
GB/T 16140-2018Determination of radionuclides in water by gamma spectrometrymerged into this editionSuperseded
GB/T 11743-2013Determination of Radionuclides in Soil by Gamma Spectrometrymerged into this editionSuperseded

This page sells the current edition, GB/T 16145-2022. Earlier editions are listed for reference only.

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