GB/T 15592-2021Polyvinyl chloride paste resins (English PDF)
聚氯乙烯糊用树脂
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Issued by
SAMR; SAC
Level / Type
National · Recommended
Issue date
December 31, 2021
Implementation date
July 1, 2022
Scope
GB/T 15592-2021 is the English-translated version of 聚氯乙烯糊用树脂.
GB/T 15592-2021 is the Chinese national standard for polyvinyl chloride paste resins, the PVC powders that make a plastisol.
It gives the classification, the requirements - the K value or viscosity number, the volatile matter, the impurities and the behaviour of the paste - the sampling, the test methods, the inspection rules, the marks and the accompanying documents and the provisions on packaging, transport and storage.
It applies to the paste resins made by the emulsion and the related processes, used in coated fabrics, flooring, dip moulding and sealants. Resin producers and the works that compound with them use it.
It replaces GB/T 15592-2008, was issued on 31 December 2021 and has applied since 1 July 2022.
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Document preview — GB/T 15592-2021
National Standard of the People's Republic of China
- ICS
- 83.080.20
- Classification
- G 32
- Replacing
- GB/T 15592-2008
Issued by: State Administration for Market Regulation; Standardization Administration of the PRC
Contents
- Foreword3
- 1 Scope5
- 2 Normative References5
- 3 Terms and Definitions6
- 4 Classification6
- 5 Requirements8
- 6 Sampling8
- 7 Test Methods9
- 8 Inspection Rules11
- 9 Marking and Accompanying Documents12
- 10 Packaging, Transportation and Storage12
1 Scope
This document specifies the classification, requirements, sampling, test methods, inspection rules, marking, accompanying documents, packaging, transportation and storage of polyvinyl chloride paste resins.
This document applies to polyvinyl chloride paste resins produced using emulsion method, micro-suspension method, and other polymerization methods.
2 Normative References
The contents of the following documents constitute indispensable clauses of this document through the normative references in the text. In terms of references with a specified date, only versions with a specified date are applicable to this document. In terms of references without a specified date, the latest version (including all the modifications) is applicable to this document.
GB/T 191 Packaging - Pictorial Markings for Handling of Goods
GB/T 2914-2008 Plastics - Homopolymer and Copolymer Resins of Vinyl Chloride - Determination of Volatile Matter (including water)
GB/T 3401 Determination of the Viscosity of Poly (vinyl chloride) Resins in Dilute Solution Using Capillary Viscometers
GB/T 3402.1 Plastics - Homopolymer and Copolymer Resins of Vinyl Chloride - Part 1. Designation System and Basis for Specifications
GB/T 3402.2 Plastics - Homopolymer and Copolymer Resins of Vinyl Chloride - Part 2. Preparation of Test Samples and Determination of Properties
GB/T 5761-2018 Suspension Polyvinyl Chloride Resins of General Purpose
GB/T 6678 General Principles for Sampling Chemical Products
GB/T 6679 General Rules for Sampling Solid Chemical Products
GB/T 8170 Rules of Rounding off for Numerical Values & Expression and Judgement of Limiting Values
GB/T 9350 Plastics - Homopolymer and Copolymer Resins of Vinyl Chloride - Determination of pH of Aqueous Extract
GB/T 12004.4 Polyvinyl Chloride Paste - Determination of Apparent Viscosity by the Brookfield Test Method
GB/T 16613 Plastics - Preparation of PVC Pastes for Test Purposes - Dissolver Method
GB/T 21988 Plastics - Vinyl Chloride Homopolymer and Copolymer Resins - Sieve Analysis in Water
GB/T 21990 Polyvinyl Chloride (PVC) Pastes - Determination of Fineness of Grind
GB/T 21991-2008 Plastics - Preparation of PVC Paste for Test Purpose - Planetary-mixer Method
GB/T 21992 Polyvinyl Chloride Resins for Paste - Determination of Number of Impurities Particles and Foreign Particles
GB/T 29874 Plastics - Homopolymer and Copolymer Resins of Vinyl Chloride - Determination of Residual Vinyl Chloride Monomer by Gas-chromatographic Analysis of Dry Powder
JJF 1070 Rules of Metrological Testing for Net Quantity of Products in Prepackages with Fixed Content
3 Terms and Definitions
This document does not have terms or definitions that need to be defined.
4 Classification
4.1 Models of Polyvinyl Chloride Paste Resins
The models of resin for polyvinyl chloride paste are composed of 6 parts as specified in GB/T 3402.1.product name, polymerization method, application, viscosity number code, standard paste proportion, and standard paste viscosity code.
5 Requirements
5.1 Appearance
White powder.
5.2 Properties
The viscosity number, K value, or average degree of polymerization of the polyvinyl chloride paste resins shall meet the requirements of Table 1; the standard paste viscosity shall meet the requirements of Table 3; and other physical and chemical properties shall meet the requirements of Table 4.
6 Sampling
6.1 Batching
A batch consists of products obtained from a single reactor or several reactors produced under the same polymerization conditions, thoroughly mixed.
6.2 Sampling
6.2.1 For bagged products, in accordance with the provisions of GB/T 6678, determine the number of sampling units. Use a suitable sampling probe specified in GB/T 6679, vertically insert it into the center of the packaging bag to a depth of 3/4 to collect the samples. During exit-factory inspection and type inspection, manufacturing enterprises may use automatic sampling devices (or manual sampling) at intervals on the packaging line to collect representative samples. The sampling quantity shall not be less than 2 kg.
6.2.2 Thoroughly mix the collected samples, place them in a clean, dry container (or plastic bag), and tightly seal (samples used for determining residual vinyl chloride monomer content shall be stored in a well-sealed sample bottle and compacted to the brim). Label the container with the manufacturing enterprise's name, product name, model, batch number or production date, sampling quantity and sampling date, etc.
7 Test Methods
7.2 Determination of Viscosity Number, K Value and Average Degree of Polymerization
7.1 Appearance
Visually observe under natural light.
7.2.1 Description of determination methods
Any method may be chosen for determining viscosity number, K value and average degree of polymerization. Among them, GB/T 3401 is the arbitration method.
7.2.2 Determination of viscosity number
Determine in accordance with the method specified in GB/T 3401.
7.2.3 Determination of K value
Determine in accordance with the method specified in GB/T 3401.
7.2.4 Determination of average degree of polymerization
Determine in accordance with the method specified in Appendix A of GB/T 5761-2018.
7.3 Determination of Standard Paste Viscosity
7.3.1 Use the standard paste proportions in Table 2, in accordance with the method specified in
GB/T 21991-2008 or GB/T 16613, prepare paste. The paste prepared using method B specified
......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 24 pages — is available in the English PDF.
Referenced standards
Normative references
- GB/T 191Graphical symbols marking for handling and storage of packages
- GB/T 2914-2008Plastics -- Homopolymer and copolymer resins of vinyl chloride -- Determination of volatile matter (including water)
- GB/T 3401Determination of the viscosity of Poly (vinyl chloride) resins in dilute solution using capillary viscometers
- GB/T 3402.1Plastics - Homopolymer and copolymer resins of vinyl chloride - Part 1: Designation system and basis for specifications
- GB/T 3402.2Plastics - Homopolymer and copolymer resins of vinyl chloride - Part 2: Preparation of test samples and determination of properties
- GB/T 5761-2018Suspension polyvinyl chloride resins of general purpose
Similar standards
Editions of GB/T 15592
| Edition | Title | Revision | Status |
|---|---|---|---|
| GB/T 15592-2021 | Polyvinyl chloride paste resins | current edition | Current |
| GB/T 15592-2008 | Polyvinyl chloride paste resins | previous edition | Superseded |
This page sells the current edition, GB/T 15592-2021. Earlier editions are listed for reference only.
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Related Standards
GB/T 12004.4-2003 — Polyvinyl chloride paste -- Determination of apparent viscosity by the Brookfield test method
GB/T 16613-2008 — Plastics -- Preparation of PVC pastes for test purposes -- Dissolver method
GB/T 191-2025 — Graphical symbols marking for handling and storage of packages
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GB/T 15592-2021
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