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GB/T 10504-2017Molecular sieve 3A (English PDF)

3A分子筛

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

September 7, 2017

Implementation date

April 1, 2018

Scope

GB/T 10504-2017 is the English-translated version of 3A分子筛.

GB/T 10504-2017 is the Chinese national product standard for 3A molecular sieve, the potassium-sodium type A molecular sieve with an effective pore diameter of about 3 Å, made from 4A molecular sieve by potassium ion exchange.

It sorts the product into bar-shaped, spherical, spherical for insulating glass and powder types, with technical requirements for each.

The test methods cover appearance, wear rate, bulk density, static and dynamic water adsorption, particle size, crush force, static ethylene and nitrogen adsorption, moisture of the packaged product, water absorption rate, temperature rise, falling powder, gas desorption and potassium exchange rate, followed by inspection rules and packaging, marking, storage and transport.

It applies to products used as industrial desiccants in chemicals, petroleum, natural gas, insulating glass and medicine. It replaces GB/T 10504-2008, was issued on 7 September 2017 and has applied since 1 April 2018.

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Document preview — GB/T 10504-2017

National Standard of the People's Republic of China

ICS
71.100.99
Classification
G 85
Replacing
GB/T 10504-2008

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Foreword
  • 1 Scope
  • 2 Normative references
  • 3 Terms and definitions
  • 4 technical requirements
  • 4.1 Product Category
  • 4.2 strip 3A molecular sieve technical requirements
  • 4.3 spherical 3A molecular sieve technical requirements
  • 4.4 hollow glass with spherical 3A molecular sieve technology requirements
  • 4.5 3A molecular sieve powder technical requirements
  • 5 test methods
  • 5.1 Appearance
  • 5.2 Determination of wear rate
  • 5.3 Determination of bulk density
  • 5.4 Determination of static water adsorption
  • 5.5 Determination of particle size
  • 5.6 Determination of crush force
  • 5.7 Determination of static ethylene and nitrogen adsorption
  • 5.8 Determination of dynamic water adsorption
  • 5.9 Determination of moisture content of packaging
  • 5.10 Determination of water absorption rate
  • 5.11 Determination of temperature rise
  • 5.12 Determination of falling powder degree
  • 5.13 Determination of gas desorption amount
  • 5.14 potassium exchange rate determination potassium tetraphenylborate overlap method
  • 5.15 Determination of the amount of sieve
  • 6 Inspection rules
  • 7 Packaging, Labeling, Storage and Transportation

Foreword

This standard was drafted in accordance with the rules given in GB/T 1.1-2009.

This standard replaces GB/T 10504-2008 "3A molecular sieve", compared with GB/T 10504-2008, the main technical changes are as follows.

--- Improve some of the main technical requirements of the product (see Chapter 4);

--- Modify spherical 3A molecular sieve and hollow glass spherical 3A molecular sieve specifications (see 4.3 and 4.4);

--- Increasing the spherical glass 3A molecular sieve gas desorption amount, powder falling and temperature rise technical requirements (see 4.4);

--- Remove the hollow glass with spherical 3A zeolite wear rate and crushing resistance of the technical requirements (see 4.4);

--- Modify the hollow glass with spherical 3A molecular sieve adsorption of static water test conditions (see 5.4).

1 Scope

This standard specifies the 3A molecular sieve terms and definitions, technical requirements, test methods, inspection rules and packaging, labeling, storage and transportation.

This standard applies to 3A molecular sieve powder, spherical and bar products, the main uses for the chemical, petroleum, natural gas, insulating glass, medicine Industrial desiccants.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version applies to this document. For undated references, the latest edition (including all amendments) applies to this document.

GB/T 191-2008 Packaging - Pictorial signs

GB/T 6286 zeolite bulk density determination method

GB/T 6287 molecular sieve static water adsorption determination

GB/T 6288 granular molecular sieve particle size determination method

GB/T 6678-2003 General principles of sampling of chemical products

GB/T 6679-2003 General Principles of Sampling for Solid Chemical Products

GB/T 8170-2008 Representation and determination of rules for repair of numerical values and limit values

GB/T 8770 molecular sieve dynamic water adsorption method

HG/T 2783 zeolite crush resistance test method

HG/T 2843 chemical analysis of fertilizer products commonly used standard titration solution, standard solution, reagent solution and indicator solution

3 Terms and definitions

The following terms and definitions apply to this document.

3.1 3A molecular sieve

Type A molecular sieve crystal structure, the effective pore diameter of about 3 Å potassium sodium type molecular sieve.

Note 1. By 4A molecular sieve after potassium ion exchange process.

Note 2. The crystal structure can be determined by X-ray diffraction.

Note 3. 1 Å = 0.1 nm.

The formula is XK2O · YNa2O · Al2O3 · 2SiO2 · 9/2H2O (XY = 1); Si-Al ratio M(SiO2)/M(Al2O3) ~2.

4 Technical requirements

4.1 Product Classification

According to different uses and appearances, the 3A molecular sieve is divided into four types.

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 17 pages — is available in the English PDF.

Referenced standards

Similar standards

Editions of GB/T 10504

EditionTitleRevisionStatus
GB/T 10504-2017Molecular sieve 3Acurrent editionCurrent
GB/T 10504-2008Molecular sieve 3Aprevious editionSuperseded

This page sells the current edition, GB/T 10504-2017. Earlier editions are listed for reference only.

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