MT 76-2011[MT/T 76-2011] Emulsifying oil, concentrate fluid and high-water content hydraulic fluid used for powered support (English PDF)
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Issued by
State Administration of Work Safety
Level / Type
National · Mandatory
Issue date
November 16, 2011
Implementation date
May 31, 2012
Scope
MT 76-2011 ([MT/T 76-2011] Emulsifying oil, concentrate fluid and high-water content hydraulic fluid used for powered support) is available as an English-translated PDF.
MT 76-2011 — This Standard specifies. the emulsifying type (HFAE) and solution type (HFAS) high- water content hydraulic fluids; and the terms and definitions, product classification, technical requirements, test methods, inspection rules and marking, packaging, transportation and storage of emulsifying oils and concentrate fluids for the preparation of the hydraulic fluid.
This Standard applies to the high-water content hydraulic fluids for hydraulic supports, outside-pourable single hydraulic props, etc. and the emulsifying oils and concentrate fluids for the preparation of the hydraulic fluids.
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Document preview — MT 76-2011
National Standard of the People's Republic of China
- ICS
- 73.100.99
- Classification
- D 97
Issued by: State Administration of Work Safety
Contents
- Foreword...3
- 1 Scope ..5
- 2 Normative references...5
- 3 Terms and definitions...6
- 4 Classification ..6
- 5 Technical requirements...7
- 6 Test methods ..8
- 7 Inspection rules ..12
- 8 Marking, packaging, transportation and storage...14
Foreword
Clauses 5.1, 5.2, 5.7, 5.14 and 5.15 of this Standard are voluntary; and the rest
are compulsory.
This Standard is a revision of MT 76-2002, Emulsifying oil concentrate and high-water
content hydraulic fluid used for powered support and prop. This Standard replaces MT
76-2002 from the data of implementation.
Compared with MT 76-2002, the major changes of this Standard are as follows.
-- the standard name is changed, in which "and prop" is deleted and "concentrate"
is changed into "concentrate liquid" (see the cover and text of 2002 edition and
this edition);
-- the product type specification is changed (see 4.2; 4.2 of 200d edition);
-- the relevant content of solid-state powder concentrate is deleted (see 5.2 of 2002
edition);
-- the technical requirements for open cup flash point are modified (see 5.3; 5.1.3
of edition 2002);
-- the technical requirements and test methods including odour, antifoaming
performance and refractometer reading (see 5.2, 5.14, 5.15, 6.3, 6.15 and 6.16);
-- the pH technical requirements are modified (see 5.8; 5.3.2 of 2002 edition);
-- the "preparation of test water" is added (see 6.1);
-- the test conditions and methods are modified (see 6.2, 6.4, 6.6, 6.9, 6.11 and 6.12;
6.1, 6.3, 6.4, 6.7, 6.9 and 6.10 of 2002 edition).
Annex A and Annex B of this Standard are normative.
This Standard was proposed by China Coal Industry Association.
This Standard shall be under the jurisdiction of the National Technical Committee on
Special Equipment for Coal Industry and Coal Mines.
China Coal Research Institute Testing Sub-Institute is responsible for the drafting of
this Standard; China Coal Research Institute Industrial Oils Business Division and
Datong Yunyan Petrochemical Co., Ltd. participate in the drafting.
1 Scope
This Standard specifies. the emulsifying type (HFAE) and solution type (HFAS) high-
water content hydraulic fluids; and the terms and definitions, product classification,
technical requirements, test methods, inspection rules and marking, packaging,
transportation and storage of emulsifying oils and concentrate fluids for the preparation
of the hydraulic fluid.
This Standard applies to the high-water content hydraulic fluids for hydraulic supports,
outside-pourable single hydraulic props, etc. and the emulsifying oils and concentrate
fluids for the preparation of the hydraulic fluids.
2 Normative references
The following referenced documents are indispensable for the application of this
document. For dated references, only the edition dated applies to this document. For
undated references, the latest edition of the referenced documents (including all
amendments) applies to This Standard.
GB 265-1988, Petroleum products - Determination of kinematic viscosity and
calculation of dynamic viscosity
GB/T 510-1983, Petroleum products - Determination of solidification point
GB/T 3142, Lubricants - Determination of load carrying capacity (four balls method)
GB/T 3536-2008, Petroleum products - Determination of flash and fire points -
Cleveland open cup method (ISO 2592.2000, MOD)
GB/T 4756, Method for manual sampling of petroleum liquids (GB/T 4756-1998,
ISO 3170.1988, NEQ)
GB/T 5231-2001, Wrought copper and copper alloys - Chemical composition limits
and forms of wrought products
GB/T 7631.2, Lubricants, industrial oils and related products (class L) -
Classification - Part 2. family H (hydraulic systems)
GB/T 11143-2008, Standard test method for rust-preventing characteristics of
Weigh accurately 2.922 g of sodium chloride (of analytical purity); dissolve in distilled
water or deionized water; and use distilled water or deionized water to dilute to 1 L.
6.2 Appearance
At 10°C ~ 35°C, inject the emulsifying oil or concentrated fluid to be tested to the 100-
ml scale of a 100-ml colorimetric tube of diameter 30 mm; use a stopper to seal; use a
5 W/220 V incandescent light bulb to irradiate the side of the colorimetric tube; and
observe the filament through the test sample. if the filament can be seen clearly, it is
transparent; if the filament is invisible or blurry, it is non-transparent. Reverse the
colorimetric tube; the film formed on the wall of the colorimetric tube shall be uniform.
6.3 Odour
Through olfactory test, emulsifying oils or concentrated fluids shall have no pungent
smell.
6.4 Open cup flash point
The flash point of emulsifying oils and concentrated fluids is tested as specified in GB/T
3536-2008, but the provision of 10.3 is not implemented. The bottom of thermometer
bulb is 6 mm from the bottom of test cup. If forming or overflow occurs during the
heating process, slow down the temperature-rise speed; and restore the normal
temperature-rise speed after foam reduces. If a fluid overflows from test cup, then the
test is invalid, and test shall be conducted once again. For some samples, they are
heated until water is nearly evaporated dry; and when the sample in test cup is in the
viscous semi-solid state or the upper part of thermometer bulb emerges above the fluid
level and the steam on the surface of the sample does not flash, then the flash point
of the sample is determined to be "none".
6.5 Kinetic viscosity
The kinetic viscosity of emulsifying oils or concentrated fluids are tested as specified
in GB/T 265-1988, but the provision of 4.1 is not implemented.
6.6 Condensation point
The condensation point of emulsifying oils or concentrated liquids are tested as
specified in GB/T 510-1983, but the provision of 4.2 is not implemented. For some
samples, temperature rise occurs during the test, so the maximum temperature during
the temperature reduction process before the temperature rise.
6.7 Freeze-thaw resistance
Inject emulsifying oils or concentrated fluids to the 100-ml scale of a 100-ml
colorimetric tube of diameter 300 mm; use a stopper for sealing; place into a
refrigeration equipment for 8 h at - 21°C ~ - 16°C; take it out and store for 16 h at 10°C
~ 35°C. This is deemed as a freeze-thaw process. After repeating 5 cycles, observe
concentration for oscillation stability test specified in Table A.2 in Annex A; inject into
the treated 100-ml measuring cylinder with a stopper to the 50-ml scale; plug the
cylinder closely with the stopper; use hand to hold the cylinder to oscillate for 1 min
under the conditions of temperature 10°C ~ 35°C, amplitude 200 mm ~ 300 mm and
frequency 100 times/min ~ 120 time/min; allow to stand; and observe the test liquid
after foam disappears.
6.11 Anti-corrosion property
Emulsifying oils or concentrated liquids and artificial hard-water of corresponding
hardness are prepared into a test solution in accordance with the specified working
concentration. Test pieces are made of cast iron HT 300. At first, use abrasive cloth
made of no. 120 aluminium oxide (brown aluminium oxide) to remove rust completely;
then use no. 240 abrasive cloth to polish until smooth and bright. There shall be no
visible machining marks. Use degreasing cotton and filter paper to wipe clean. If
necessary, use solvent naphtha specified in SH 0004 for cleaning before drying. Drip
the test fluid 5 drops on the surface of cast iron test pieces uniformly in the shape of
plum blossom, with the diameter of each drop 6 mm ~ 7 mm. Use a watch glass of
diameter 60 mm for coverage; store for 24 h at 10°C ~ 35°C; and observe the rusting
conditions.
The material of cast iron test pieces is HT 300; and the diameter of test pieces is 50
mm.
6.12 Corrosion resistance
Use emulsifying oils or concentrated fluids and sodium chloride solution 0.05 mol/L to
prepare the test fluid in accordance with the liquid concent...
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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 14 pages — is available in the English PDF.
Referenced standards
Normative references
- GB/T 510-1983Determination of solidification point for petroleum products
- GB/T 3142Standard test method for determination of load-carrying capacity of lubricants—Four-ball method
- GB/T 3536-2008Petroleum products -- Determination of flash and fire points -- Cleveland open cup method
- GB/T 5231-2001Designation and chemical composition of wrought copper and copper alloys
- GB/T 11143-2008Test method for rust-preventing characteristics of inhibited mineral oil in the presence of water
GB 265-1988 · ISO 2592.2000 · GB/T 4756 · GB/T 4756-1998 · ISO 3170.1988 · GB/T 7631.2
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