HG/T 2525-2011Insoluble sulfur for rubber (English PDF)
橡胶用不溶性硫磺
This is a limited preview
Buy now to download the full PDF (20 pages)
Need quotation for your management?
Get a formal quotation for HG/T 2525-2011 in 30 minutes.
Issued by
MIIT
Level / Type
Industry · Recommended
Issue date
December 20, 2011
Implementation date
July 1, 2012
Scope
HG/T 2525-2011 is the English-translated version of 橡胶用不溶性硫磺.
HG/T 2525-2011 is the Chinese chemical industry standard for insoluble sulfur used as a rubber vulcanizing agent, in both non-oil-filled and oil-filled form. It fixes the grade requirements, among them the IS-HS 70-20 and IS-HS 60-33 types introduced in this edition, and the test methods behind each figure: insoluble sulfur content, mass fraction of sieve residue on the 150 µm sieve, acidity titrated with sodium hydroxide against bromothymol blue and reported as sulfuric acid, and heat stability at 105 °C. Inspection rules with re-sampling on a failed indicator, marking, 25 kg woven bags with a plastic liner, transport, storage below 45 °C for at most one year and fire safety complete the text. It replaces HG/T 2525-1993. Issued on 20 December 2011, it has applied since 1 July 2012.
Found what you need?
Document preview — HG/T 2525-2011
National Standard of the People's Republic of China
- Replacing
- HG/T 2525-1993
Issued by: Ministry of Industry and Information Technology of the People's Republic of China
Contents
- FOREWORD3
- 1 SCOPE4
- 2 NORMATIVE REFERENCES4
- 3 REQUIREMENTS5
- 4 TEST METHODS5
- 5 INSPECTION RULES17
- 6 MARKING, PACKAGING, TRANSPORTATION AND STORAGE18
- 7 SAFETY18
Foreword
This Standard is drafted according to the rules specified in GB/T 1.1-2009.
This Standard replaces HG/T 2525-1993 - The Insoluble Sulfur for Rubber. Compared with HG/T 2525-1993, the main technical changes are as follows, in addition to editorial changes.
- - DELETE the requirements to models IS 70-20 and IS 60-33, and ADD the requirements to models IS-HS 70-20 and IS-HS 60-33 (see Chapter 3, and Chapter 4 of Edition 1993);
- - MODIFY the testing items' requirements to different types of products (see Chapter 3, Chapter 4 of Edition 1993)
- - MODIFY the indication value of mass fraction of sieve residue (150µm) in insoluble sulfur for rubber (see Chapter 3, Chapter 4 of Edition 1993);
- - ADD the requirements and test methods for the heat stability (105) of insoluble °C sulfur for rubber (see Chapters 3 and 4.6).
1 Scope
This Standard specifies the requirements, test methods, inspection rules, marking, packaging, transportation, storage and safety of insoluble sulfur for rubber.
This Standard is applicable to rubber vulcanizer - Non-oil-filled and oil-filled insoluble sulfur.
2 Normative references
The articles contained in the following documents have become part of this Standard when they are quoted herein. For the dated documents so quoted, all the modifications (Including all corrections) or revisions made thereafter shall be applicable to this Standard.
For undated document, its newest edition (including all corrigenda) applies to this Standard.
GB 190 Packing symbol of dangerous goods
GB/T 191 Packaging - Pictorial marking for handling of goods
GB/T 601 Chemical reagent - Preparations of standard volumetric solutions
GB/T 603 Chemical reagent - Preparations of reagent solutions for use in test methods
GB/T 6003.1 Test sieves - Technical requirements and testing - Part 1: Test sieves of metal wire cloth
GB/T 6678 General principles for sampling chemical products
GB/T 6679 General rules for sampling solid chemical products
GB/T 6682 Water for analytical laboratory use - Specification and test methods
4 TEST METHODS
4.7.1 Principle
EXTRACT the acidic substances of the specimen with the water containing a small amount of ethanol; USE thymol blue bromide as indicator; USE sodium hydroxide standard titration solution to titrate.
4.7.2 Reagents
4.7.2.1 Anhydrous ethanol.
4.7.2.2 Sodium hydroxide standard titration solution.
4.7.2.3 Sodium hydroxide standard titration solution. c (NaOH) = 0.02 mol/L
DRAW 20.00 mL of sodium hydroxide standard titration solution (4.7.2.2) INTO 100 mL volumetric flask; DILUTE with water to the mark; SHAKE well. PREPARE this solution whenever needed.
4.7.2.4 Indicating solution of thymol blue bromide. 1 g/L.
4.7.3 Analytical steps
WEIGH approximate 10g of sample with accuracy of 0.01g; PLACE in a 400mL beaker;
ADD 15 mL of anhydrous ethanol (4.7.2.1); STIR well; LET the specimen fully wet; ADD additional 200mL of water; STIR fully for 2min - 3min; ADD 10 drops of thymol blue bromide indicating liquid (4.7.2.4) after placing it for 5min; USE sodium hydroxide standard titration solution (4.7.2.3) to titrate until the solution becomes blue green. Blank test shall be conducted simultaneously.
4.7.4 Result calculation
The mass fraction of acidity shall be measured by mass fraction w6 of sulfuric acid (H2SO4), the value shall be represented by % and calculated according to Formula (6). Where.
V - The value of the volume of sodium hydroxide standard titration solution (4.7.2.3) consumed in the measurement, the unit is in mL;
V0 - The value of the volume of sodium hydroxide standard titration solution consumed in blank test, the unit is in mL;
C - The exact value of actual concentration of sodium hydroxide standard titration result shall be judged if it complies with this Standard. If there is 1 indicator in the inspection result not meeting the requirement of this Standard, it shall repeat the sampling and take double amount of samples for re-inspection. If there is still 1 or more indicator in the re-inspection result not meeting the requirements of this Standard, the whole batch of products is deemed unqualified.
6 Marking, packaging, transportation and storage
6.1 Distinct and reliable marks shall be available on the packaging bags of insoluble sulfur products for rubbers, which shall include. product name, product model, manufacturer's name, manufacturer's address, trademark, batch number, production date, net content, number of this Standard and the mark "Vulnerable to Rain" as specified in GB/T 191; the packaging bags of insoluble sulfurs for the non-oil-extended rubbers shall also be with the mark "Inflammable Solid" as specified in GB 190.
6.2 The insoluble sulfur for rubber shall be packed by plastic woven bag of liner plastic pouch; and the plastic woven bag shall comply with the requirements of GB/T 8946. The thickness of liner plastic bag shall be between 0.18 mm and 0.25 mm; and the volume shall be larger than external packing. TIE both side of the inner bag; SEW the outer bag with machines after folding; and the needle pitch shall be no greater than 10 mm. The net content of each bag shall be 25 kg or other packing amount confirmed by the user.
6.3 The insoluble sulfur for rubber shall be covered with awnings during transport; it must not be mixed with alkaline materials; it shall pay attention to fire prevention, heat-proof, and moisture proof to avoid product deterioration.
6.4 The insoluble sulfur for rubber shall be stored in dry, ventilated and shady warehouse; the storage space shall be kept fire-proof, heat-proof and moisture-proof; the storage temperature shall not be higher than 45.°C The insoluble sulfur for rubber shall not be placed too close to alkaline substances; and it shall be prevented from pressurized and caking. From the date of production, the storage period shall not exceed one year.
7 Safety
7.1 Insoluble sulfur for rubber is non-toxic and combustible; special fire-fighting equipment shall be set up at stacking places and warehouses; and it's forbidden to use open flame.
7.2 The staff engaged in the production, transportation, storage, and processing of insoluble sulfur for rubber shall use the necessary protective articles during the operation.
Translation References and Original Chinese Documents [1] HG/T 2525-2011 Insoluble sulfur for rubber. […]
......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 20 pages — is available in the English PDF.
Referenced standards
Normative references
- GB/T 191Graphical symbols marking for handling and storage of packages
- GB/T 601Chemical Reagent - Preparations of Standard Volumetric Solutions
- GB/T 603Chemical reagent - Preparations of reagent solutions for use in test methods
- GB/T 6003.1Test sieves—Technical requirements and testing—Part 1:Test sieves of metal wire cloth
- GB/T 6678General principles for sampling chemical products
- GB/T 6679General rules for sampling solid chemical products
GB 190
Similar standards
Editions of HG/T 2525
| Edition | Title | Revision | Status |
|---|---|---|---|
| HG/T 2525-2011 | Insoluble sulfur for rubber | current edition | Current |
| HG/T 2525-1993 | Insoluble sulfur for rubber | previous edition | Superseded |
This page sells the current edition, HG/T 2525-2011. Earlier editions are listed for reference only.
How to Download HG/T 2525-2011
- 1
Add to cart
Click "Download PDF" on this page and choose "Buy this standard". You can add more standards before checkout.
- 2
Checkout
Enter your email and billing details. Payment is processed securely by Stripe (cards or bank transfer). Prefer bank details? Request a quotation (min. order $300).
- 3
Instant delivery (0–9 sec)
Delivery is automatic: within seconds of payment you'll receive an email with a secure download link. The link stays valid for 72 hours.
- 4
Invoice included
A tax invoice is attached to the confirmation email. Need a custom invoice? Contact us.
Related Standards
GB 1903.24-2016 — Food Safety National Standard Food Nutrition Enhancer -- Vitamin C Phosphate Magnesium
GB 1903.26-2022 — National food safety standard - Food nutritional fortification substance - Docosahexaenoic Acid (Tuna oil)
GB 1903.28-2018 — National food safety standard -- Food nutrition enhancer selenoprotein
Secure payment via Stripe
Payments accepted
HG/T 2525-2011
$120.00