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GB/T 5518-2008Inspection of grain and oil - Determination of relatively density of grain and oilseeds (English PDF)

粮油检验 粮食、油料相对密度的测定

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

November 4, 2008

Implementation date

January 20, 2009

Scope

GB/T 5518-2008 is the English-translated version of 粮油检验 粮食、油料相对密度的测定.

GB/T 5518-2008 is a grain and oils inspection method for the relative density of grain and oilseeds.

Clause 1 states that the standard specifies the terms and definitions, principle, reagents, apparatus and appliances, sample preparation, analysis steps and calculation of results for the relative density of grain and oilseeds; the sentence that follows, on what the standard applies to, is garbled in the draft version on the page and in the summary alike, and cannot be read with confidence.

Clause 3 carries a single definition whose term name the draft does not print, for the ratio, at a given temperature and under given operating conditions, of the mass of the grain or oilseed to the mass of the same volume of water, taken on its net volume.

The clause printed as Principle 4 adds a weighed quantity of grain or oilseed to a measured volume of liquid, takes the increase in liquid volume as the net volume of the sample and computes the ratio against the mass of an equal volume of water.

Clause 5, Reagents, lists 95% ethanol of analytical grade and a 20% ethanol made up from 21 mL of the 95% ethanol and 79 mL of distilled water, and clause 6, apparatus and appliances, calls for a balance with a division value of 0.01 g, a 25 mL cylinder graduated in 0.1 mL and a long-necked density bottle with a piston, graduated in 0.1 mL over 10 mL with the zero mark low on the neck.

Clause 7 refers sample preparation to GB 5491, with impurities and imperfect pieces removed, and the clause printed as Analysis Step 8 opens with 8.1, the cylinder method, carried out at a room temperature of 22 degrees C plus or minus 5 degrees C on a sample of about 5 g weighed to 0.01 g in 10 mL of the 20% ethanol, the rise in liquid level being read once the surface is still; the draft ends after that subclause.

Clause 2 cites GB 5491.

The foreword records that the two methods of the 1985 edition were combined, that terms and definitions and a principle were added, that the sample and reagent requirements were modified, that requirements on the measurement environment were added and that the repeatability requirement for the calculation of results was changed.

It replaces GB/T 5518-1985, was issued on 2008-11-04 and has applied since 2009-01-20.

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Document preview — GB/T 5518-2008

National Standard of the People's Republic of China

ICS
67.040
Classification
X 10
Replacing
GB/T 5518-1985

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Foreword
  • 1 Scope
  • 2 Normative references
  • 3 Terms and Definitions
  • 4 Principle
  • 5 Reagents
  • 6 Apparatus and appliances
  • 7 Sample Preparation
  • 8 Analysis Step

Foreword

This standard replaces GB/T 5518-1985 "grain and oilseeds for food inspection determination of specific gravity." This standard and GB/T 5518-1985 main technical differences are as follows.

--- Change the standard name is "Inspection of grain and determination of grain and oilseeds relative density";

--- Increasing the terms and definitions and principles;

--- The standard two methods are combined;

--- Modify the sample volume and reagent requirements symmetry like;

--- Increased the determination of environmental requirements;

--- The results of calculation of the repeatability requirement has been modified.

The standard proposed by the National Food Authority.

1 Scope

This standard specifies the grain and oilseeds relative density of terms and definitions, principle, reagents, apparatus and appliances, sample preparation, analysis step And the results of calculations.

This standard applies to food, the relative density measured fuel.

2 Normative references

The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.

GB 5491 grain and oilseeds testing for sampling, and sample method

3 Terms and Definitions

The following terms and definitions apply to this standard.

3.1

At a predetermined temperature and operating conditions, than the quality of the food, the quality of oil net volume with the same volume of water.

4 Principle

Grain, oil is added to a sample of a certain quality, a predetermined liquid volume, resulting in increase in the volume of the liquid, the increased volume is again Like net volume. Than the quality of the sample with the same volume of water is calculated.

5 Reagents

5.1 95% ethanol. AR.

5.2 20% ethanol. 95% ethanol (5.1) 21mL distilled water 79mL.

6 Apparatus and appliances

6.1 Balance. dividing the value of 0.01g.

6.2 Cylinder. 25mL, dividing the value of 0.1mL.

6.3 Density bottle. long-necked bottle with the piston. There 0.1mL neck scale, count 10mL, zero-scale at the lower long-necked, under zero Adjust the liquid volume of the piston.

7 Sample Preparation

GB 5491 by decimation, to remove impurities and imperfections tablets.

8 Analysis Step

8.1 Cylinder method

At room temperature (22 °C ± 5 °C) under the graduated cylinder (6.2) poured into 20% ethanol (5.2) 10mL, and then placed in a sample of about 5g (m1, accurate to 0.01g), a little shaken, expelled bubbles, until after the smooth surface, immediately reads the volume of liquid rises (Vp).

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

Referenced standards

Similar standards

Editions of GB/T 5518

EditionTitleRevisionStatus
GB/T 5518-2008Inspection of grain and oil - Determination of relatively density of grain and oilseedscurrent editionCurrent
GB/T 5518-1985Inspection of grain and oil - Determination of relatively density of grain and oilseedsprevious editionSuperseded

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