GB/T 5454-1997Textiles. Burning behaviour. Oxygen index method (English PDF)
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Issued by
State Bureau of Technical Supervision
Level / Type
National · Recommended
Issue date
June 9, 1997
Implementation date
December 1, 1997
Scope
GB/T 5454-1997 (Textiles. Burning behaviour. Oxygen index method) is available as an English-translated PDF.
GB/T 5454-1997 — This standard specifies the test methods for determining the minimum oxygen concentration (also known as limiting oxygen index) required to maintain the burning of the specimen in the mixed flow of oxygen and nitrogen when the specimen is vertical.
This standard applies to the determination of burning behavior of various types of textiles (including single-component or multi-component), such as woven fabrics, knitted fabrics, non-woven fabrics, coated fabrics, laminated fabrics, composite fabrics, carpets (including flame retardant treated and untreated).
This standard is only used to determine the burning behavior of textiles under laboratory conditions and to control the quality of the products. It cannot be used as a basis for assessing the risk of fire under actual conditions of use, or it can only be used to analyze one of the factors when a special purpose material catches fire.
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Document preview — GB/T 5454-1997
National Standard of the People's Republic of China
- ICS
- 59.080.01
- Classification
- W 04
Issued by: State Bureau of Technical Supervision
Contents
- Foreword...3
- 1 Scope...5
- 2 Normative references...5
- 3 Definitions...5
- 4 Principles...6
- 5 Health and safety of testing personnel...6
- 6 Equipment and materials...6
- 7 Specimen and humidity conditioning...8
- 8 Test procedures...9
- 9 Calculation and result representation...10
- 10 Test report...13
- Appendix A (Normative) Calculation of oxygen concentration...14
Foreword
This standard non-equivalently adopted the international standard ISO 4589.
1984 "Plastics - Burning behavior - Oxygen index method". It combined the
characteristics of the textiles to make modification of the national standard GB
5454-85.Its main technical contents and test methods and procedures are
consistent with international standard.
This standard inherits the main technical content of the previous version, makes
supplementary and editorial changes of the name of the standard, the
arrangement of the clauses, and the technical content. It adds the "foreword",
deletes the additional instructions, and incorporates the content into the
foreword
The name of this standard has been changed to "Textiles - Burning behavior -
Oxygen index method".
In clause 1 "Scope", ADD the test methods contents under which conditions as
specified by this standard, in the scope of determination, ADD "including single-
component and multi-component".
In this standard, ADD clause 2 "Normative references", ADD foreign terms
corresponding to 3 nouns and 4 nouns, ADD clause 5 "Testing personnel health
and safety".
In clause 6, MODIFY the "instrument" into "equipment and material", MAKE
editorial changes of the contents, ADD one clause "Gas decompressor".
In clause 7, MODIFY the "specimen" into "specimen and temperature
conditioning". MODIFY the number of specimen cutting into "take at least 15
pieces along warp and weft for general textiles", DELETE the specimen
preparation test method that "It shall sew three 8 ~ 11 Nm glass fiber when
testing the textiles made by fused fiber". MODIFY "The specimen shall be
balanced for over 24 h" into "The specimen is subject to humidity conditioning
for 8 ~ 24 h depending on its thickness to make it reach temperature
equilibrium".
In clause 8, ADD "determination of initial oxygen concentration", "increase -
decrease method", and "determination of limiting oxygen index" to replace
clause 6.7 of the original standard.
In clause 9 of this standard, for the oxygen index calculation, ADD three clauses
"k-value coefficient determination table", "verification of oxygen concentration
interval", and "precision".
In this standard, ADD "Appendix A Calculation of oxygen concentration",
CHANGE the name of "Appendix A References" into "Appendix B", ADD
"Appendix C Calibration of equipment" and "Appendix D Example of typical test
results".
This standard was first published in 1985 and revised in 1995.
Appendix A of this standard is normative.
Appendix B, Appendix C, and Appendix D of this standard are informative.
This standard replaced GB 5454-85 from the effective date.
This standard was proposed by the China Textile Federation.
This standard shall be under the jurisdiction of the China Textile Federation
Standardization Institute.
Drafting organizations of this standard. China Textile Association
Standardization Institute.
1 Scope
This standard specifies the test methods for determining the minimum oxygen
concentration (also known as limiting oxygen index) required to maintain the
burning of the specimen in the mixed flow of oxygen and nitrogen when the
specimen is vertical.
This standard applies to the determination of burning behavior of various types
of textiles (including single-component or multi-component), such as woven
fabrics, knitted fabrics, non-woven fabrics, coated fabrics, laminated fabrics,
composite fabrics, carpets (including flame retardant treated and untreated).
This standard is only used to determine the burning behavior of textiles under
laboratory conditions and to control the quality of the products. It cannot be
used as a basis for assessing the risk of fire under actual conditions of use, or
it can only be used to analyze one of the factors when a special purpose
material catches fire.
2 Normative references
The provisions contained in the following standards constitute the provisions of
this standard through reference in this standard. At the time of publication, the
editions indicated were valid. All standards will be revised and all parties using
this standard shall explore the possibility of using the latest version of the
following standards.
GB 6529-86 Standard atmospheres for textiles conditioning and testing
3 Definitions
This standard uses the following definitions.
3.1
Afterflame time
Under the specified test conditions, the duration during which the material
continues flame burning after moving the fire source away.
3.2
Afterglow time
Under the specified test conditions, the duration during which the material
continues to flameless burning after the flame burning is terminated or after
the (point) source of ignition is removed.
4 Principles
The specimen is vertically clamped on the specimen holder and placed in the
combustion cylinder. In the upflowing oxygen-nitrogen gas stream, the upper
end of the specimen is ignited, to observe the combustion characteristics, and
to compare the afterflame time or the damaged length with the specified limiting
value.
5 Health and safety of testing personnel
Smoke and gases from the burning of textile materials are toxic and can affect
the health of workers. The test equipment can be installed in a fume hood.
6 Equipment and materials
6.1 Oxygen index instrument (see Figure 1). Equally effective instruments can
also be used.
6.1.1 Combustion cylinder. It consists of a heat-resistant glass tube with an
inner diameter of at least 75 mm and a height of at least 450 mm. The bottom
of the cylinder is connected to the inlet pipe and filled with glass beads with a
diameter of 3 ~ 5 mm, the height is 80 ~ 100 mm. A metal mesh is placed above
the glass beads to withstand possible dripping during combustion and keep the
bottom of the cylinder clean.
6.2 Gas source. Industrial oxygen and nitrogen.
6.3 Gas decompressor. It can indicate the high pressure in the cylinder of not
less than 15 MPa and ensure the gas supply pressure 0.1 ~ 0.5 MPa.
6.4 Igniter. A tube with an internal diameter of 2 mm ± 1 mm is charged with
propane or butane gas, one end of the tube is fired, the flame height can be
regulated by gas valve, to ensure that it can reach above the combustion
cylinder to ignite the specimen, the flame height is 15 ~ 20 mm.
7 Specimen and humidity conditioning
7.1 Specimen shall be cut from the part away from the textile at a distance 1/10
breadth, the size of each specimen is 150 mm x 58 mm. For general fabrics,
take at least 15 pieces each in the warp (longitudinal) weft (transverse) direction,
respectively.
8 Test procedures
8.1 Test device inspection. OPEN the valves of gas supply part, arbitrarily
SELECT the mixed gas concentration, at the flow rate around 10 L/min, CLOSE
the outlet and inlet valve, RECORD the pressure and flow of oxygen, nitrogen,
and mixed gas. LET it be standing for 30 min, then OBSERVE the values
indicated on each pressure gauge and flow meter, COMPARE with the values
recorded before, it indicates that there is no gas leakage of the device if there
is no deviation.
8.2 Test temperature and humidity. The tests are carried out in the atmosphere
at a temperature of 10 ~ 30 °C and a relative humidity of 30% ~ 80%.
8.3 Initial selection of specimen oxygen concentration.
8.4 INSTALL the specimen in the middle of the specimen holder and fix it. Then
INSERT the specimen holder with the specimen vertically in the specimen
holder in the combustion glass cylinder.
8.5 Open the oxygen and nitrogen valves, to regulate the corresponding oxygen
and nitrogen flow as found from Appendix B, to let the regulated gas flow and
flush the combustion cylinder for at least 30 s before the ignition of specimen,
this flow rate is maintained unchanged in the ignition and combustion process.
8.6 Ignite the igniter.
8.7 Determination of initial oxygen concentration. USE any interval as a variable,
USE the "increase - decrease method" to perform test in accordance with
clause 8.7.1 ~ 8.7.3".
8.7.1 When the specimen is self-extinguishing immediately after ignition, when
the afterflame time or afterglow time is less than 2 min, or when the damaged
length is not reaching 40 mm, it indicates that the oxygen concentration is too
low, the reaction symbol is recorded as "O", and it must increase the oxygen
concentration.
8.8 Determination of limiting oxygen concentration.
8.8.1 USE the initial oxygen concentration co, while maintaining the oxygen
concentration interval of d = 0.2% to repeat the operations of clause 8.7.1 ~
8.7.2, to determine a series of oxygen concentration value and the
corresponding symbol, wherein the last reaction symbol "O" or "X" is the first
data in 8.8.2 in NL series determination by oxygen index (see Appendix D).
9 Calculation and result representation
9.1 Calculation of limiting oxygen index
The limiting oxygen index LOI is expressed in volume percentage and is
calculated in accordance with formula (1).
9.2.2 If the last five oxygen index values are determined by the test in 8.8.1, the
first reaction symbol is "O", find the corresponding reaction symbol of the last
five determinations from the column 6 of Table 1, and find the K value factor
corresponding to the "X" number from Table 1 (b), but the symbol of K value is
contrary to the signs of positive and negative numbers in the table.
9.3 Verification of oxygen concentration interval
Oxygen concentration interval verification is calculated in accordance with
9.4 Precision
For easily ignited and flammable materials, this method has the accuracy
shown in Table 2.
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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 14 pages — is available in the English PDF.
Referenced standards
Normative references
GB 6529
Cited by
- GB 8624-2025Classification for burning behavior of building materials and products
- JT/T 1095-2022Flame resistance of commercial bus interior materials
- GB 38262-2019Flammability of interior materials for buses
- TB/T 3138-2018Technical specification of flame retardant materials for railway locomotive and vehicle
- JB/T 12165-2015Halogen-free low-smoke flame-retardant glass fibre tapes for electrical insulation
- GB 24407-2012The safety technique specifications of special school
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