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GB/T 41442-2022Test method for pure cashmere content of cashmere—Near infrared spectrometer method (English PDF)

山羊绒净绒率试验方法 近红外光谱法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

April 15, 2022

Implementation date

November 1, 2022

Scope

GB/T 41442-2022 is the English-translated version of 山羊绒净绒率试验方法 近红外光谱法.

GB/T 41442-2022 is the Chinese national method for measuring the pure cashmere content of cashmere by near infrared spectrometry. It describes the principle, the instrument and its calibration model, the preparation of the sample, the measurement, the reading of the result and its precision, with the test report.

It applies to the rapid determination of the net cashmere yield of raw and washed cashmere, the figure on which a lot is bought. Cashmere traders, scourers and testing laboratories use it. Issued on 15 April 2022, it has applied since 1 November 2022.

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Document preview — GB/T 41442-2022

National Standard of the People's Republic of China

ICS
59.060
Classification
W 20

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Foreword
  • 1 Scope
  • 2 Normative references
  • 3 Terms and Definitions
  • 4 Principles

Foreword

This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for Standardization Work Part 1: Structure and Drafting Rules of Standardization Documents" drafted.

1 Scope

This document describes a test method for the detection of cashmere net cashmere by near-infrared spectroscopy.

This document is suitable for the rapid detection of the net cashmere rate of raw cashmere and washed cashmere.

2 Normative references

The contents of the following documents constitute essential provisions of this document through normative references in the text. Among them, dated citations documents, only the version corresponding to that date applies to this document; for undated references, the latest edition (including all amendments) applies to this document.

GB/T 8170 Numerical Rounding Rules and Representation and Judgment of Limit Values

GB 18267 Cashmere

3 Terms and Definitions

The following terms and definitions apply to this document.

3.1 Calibration database

A database consisting of a set of near-infrared spectra and calibration values of cashmere samples involved in calibration.

3.2 Calibrated sample

Samples that pass verification during the calibration process.

Note: The calibration sample is used as the verification material for calibration in this document.

3.3 Sampleoutsidelibrary

The standard deviation of the spectrum does not exceed the set threshold and the error of the property value is less than the maximum allowable value of the reproducibility of the calibration method, and the spectral similarity is greater than the set value. Samples that mark the boundaries of the database.

3.4 Outliersample

Samples that failed verification during calibration.

Note: Include samples whose spectral standard deviation exceeds the set threshold or whose property value error is greater than the reproducibility of the calibration method.

4 Principles

Based on the correlation between the change of the net cashmere rate of the sample and the change of its molecular spectrum, a multivariate analysis method was used to establish a spectroscopic determination of net According to the calibration curve of the cashmere ratio, measure the spectrum of the sample to be tested to obtain the net cashmere ratio.

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 18 pages — is available in the English PDF.

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