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GB/T 39145-2020Test method for the content of surface metal elements on silicon wafers—Inductively coupled plasma mass spectrometry (English PDF)

硅片表面金属元素含量的测定 电感耦合等离子体质谱法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

October 11, 2020

Implementation date

September 1, 2021

Scope

GB/T 39145-2020 is the English-translated version of 硅片表面金属元素含量的测定 电感耦合等离子体质谱法.

GB/T 39145-2020 is the Chinese standard "Test method for the content of surface metal elements on silicon wafers—Inductively coupled plasma mass spectrometry". Its scope clause reads: This standard specifies the method for determining the content of metal elements on the surface of silicon wafers by inductively coupled plasma mass spectrometry.

This standard is applicable to the trace metal sodium, magnesium, aluminum, potassium, calcium, chromium, manganese, iron, cobalt, nickel, copper and zinc on the surface of polished silicon single crystal wafers and silicon epitaxial wafers.

The determination of the element content is in the range of 108cm-2~1013cm-2.This standard also applies to non-patterned silicon annealing wafers, silicon diffusion wafers, etc. Determination of trace metal element content on silicon wafer surface.

Note. The metal element content on the surface of the silicon wafer is calculated in the number of atoms per square centimeter. Its clauses include terms and definitions.

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Document preview — GB/T 39145-2020

National Standard of the People's Republic of China

ICS
77.040
Classification
H 17

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • 1 Scope
  • 2 Normative references
  • 3 Terms and definitions
  • 3.1 Scan solution
  • 3.2 Direct acid drop decomposition
  • 3.3 Gas phase decomposition

1 Scope

This standard specifies the method for determining the content of metal elements on the surface of silicon wafers by inductively coupled plasma mass spectrometry.

This standard is applicable to the trace metal sodium, magnesium, aluminum, potassium, calcium, chromium, manganese, iron, cobalt, nickel, copper and zinc on the surface of polished silicon single crystal wafers and silicon epitaxial wafers.

The determination of the element content is in the range of 108cm-2~1013cm-2.This standard also applies to non-patterned silicon annealing wafers, silicon diffusion wafers, etc.

Determination of trace metal element content on silicon wafer surface.

Note. The metal element content on the surface of the silicon wafer is calculated in the number of atoms per square centimeter.

2 Normative references

The following documents are indispensable for the application of this document. For dated reference documents, only the dated version applies to this article

Pieces. For undated references, the latest version (including all amendments) applies to this document.

GB/T 6624 Visual inspection method for surface quality of polished silicon wafer

GB/T 14264 Terminology of Semiconductor Materials

GB/T 17433 Basic terms for chemical analysis of metallurgical products

GB/T 19921 Test method for surface particles of polished silicon wafers

GB/T 25915.1-2010 Clean room and related controlled environment Part 1.Air cleanliness grade

GB/T 37837 Quadrupole Inductively Coupled Plasma Mass Spectrometry Method General

JJF1159 Quadrupole Inductively Coupled Plasma Mass Spectrometer Calibration Specification

SEMIF63 Ultrapure Water Guide for Semiconductor Processing

3 Terms and definitions

The following terms and definitions defined in GB/T 14264, GB/T 17433, GB/T 37837 and JJF1159 apply to this document.

3.1 Scan solution

A solution containing trace metal elements on the surface of a silicon wafer collected by scanning.

3.2 Direct acid drop decomposition

Decompose the oxide layer on the surface of the silicon wafer with an extraction solution containing hydrofluoric acid to form a hydrophobic surface, so that trace metals on the surface of the silicon wafer are collected

A scanning solution is formed in the extraction solution.

3.3 Gas phase decomposition

Use hydrofluoric acid vapor to decompose the oxide layer on the surface of the silicon wafer to form a hydrophobic surface, and then use an extraction solution containing hydrofluoric acid to extract the surface of the silicon wafer.

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

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