GB/T 34609.1-2017Method for chemical analysis of rhodium compounds - Part 1: Determination of rhodium content - Gravimetric method with hexaammine cobalt nitrate (English PDF)
铑化合物化学分析方法 第1部分：铑量的测定 硝酸六氨合钴重量法
This is a limited preview
Buy now to download the full PDF (15 pages)
Need quotation for your management?
Get a formal quotation for GB/T 34609.1-2017 in 30 minutes.
Issued by
SAMR; SAC
Level / Type
National · Recommended
Issue date
October 14, 2017
Implementation date
May 1, 2018
Scope
GB/T 34609.1-2017 is the English-translated version of 铑化合物化学分析方法 第1部分：铑量的测定 硝酸六氨合钴重量法.
GB/T 34609.1-2017 is the Chinese standard "Method for chemical analysis of rhodium compounds - Part 1: Determination of rhodium content - Gravimetric method with hexaammine cobalt nitrate".
Its scope clause reads: GB/T 34609 provisions of this part of the determination of rhodium rhodium compounds.
This section applies to rhodium nitrate (Rh (NO3) 3), rhodium sulfate (Rh2 (SO4) 3), rhodium trichloride (RhCl3), rhodium iodide (RhI3), rhodium acetate Rhodium octylate ([Rh (CH3 (CH2) 6CO2) 2] 2), rhodium acetylacetonate (C15H21O6Rh) Determination of rhodium content in triphenylphosphine rhodium chloride ([(C6H5) 3P] 3RhCl).
Measurement range .5% ~ 50%. Its clauses include method principle; reagent; device; sample.
Found what you need?
Document preview — GB/T 34609.1-2017
National Standard of the People's Republic of China
- ICS
- 77.120.99
- Classification
- H 15
Issued by: State Administration for Market Regulation; Standardization Administration of the PRC
Contents
- 1 Scope
- 2 method principle
- 3 reagent
- 4 device
- 5 sample
1 Scope
GB/T 34609 provisions of this part of the determination of rhodium rhodium compounds.
This section applies to rhodium nitrate (Rh (NO3) 3), rhodium sulfate (Rh2 (SO4) 3), rhodium trichloride (RhCl3), rhodium iodide (RhI3), rhodium acetate
Rhodium octylate ([Rh (CH3 (CH2) 6CO2) 2] 2), rhodium acetylacetonate (C15H21O6Rh)
Determination of rhodium content in triphenylphosphine rhodium chloride ([(C6H5) 3P] 3RhCl). Measurement range .5% ~ 50%.
2 method principle
The sample was pretreated with nitric acid, hydrochloric acid and perchloric acid, then digested in polytetrafluoroethylene tank and hydrochloric acid-hydrogen peroxide was digested under high temperature and high pressure,
Chlorine complex slightly acidic solution, with rhodium nitrate hexamine cobalt complex precipitation, gravimetric determination of rhodium.
3 reagent
Unless otherwise specified, only reagents that are identified as analytically pure and secondary water are used in the analysis.
3.1
sodium nitrite.
3.2
Nitric acid (p = 1.42 g/mL).
3.3
Hydrochloric acid (p = 1.19 g/mL).
3.4
Absolute ethanol (rho = 0.79g/mL).
3.5
ether (p = 1.19 g/mL).
3.6
perchloric acid (70.0% ~ 72.0%).
3.7
Hydrogen peroxide (30%, volume fraction).
3.8
Ammonium hexamine cobalt saturation solution Weigh 17g crystalline hexamine cobalt, add 300mL of water, heated to dissolve, with fast qualitative filter paper
After filtration, dilute to 1000 mL.
3.9
Ammonium hexamine cobalt lotion Take 15mL hexamine cobalt saturated solution, diluted with water to 500mL.
Note Preparation of hexamine cobalt nitrate in Appendix A.
4 device
Balance. Sense of 0.01mg.
5 sample
Samples stored in a closed container, the time is now.
......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.
Referenced standards
Similar standards
How to Download GB/T 34609.1-2017
- 1
Add to cart
Click "Download PDF" on this page and choose "Buy this standard". You can add more standards before checkout.
- 2
Checkout
Enter your email and billing details. Payment is processed securely by Stripe (cards or bank transfer). Prefer bank details? Request a quotation (min. order $300).
- 3
Instant delivery (0–9 sec)
Delivery is automatic: within seconds of payment you'll receive an email with a secure download link. The link stays valid for 72 hours.
- 4
Invoice included
A tax invoice is attached to the confirmation email. Need a custom invoice? Contact us.
Related Standards
GB/T 34609.2-2020 — Method for chemical analysis of rhodium compounds - Part 2: Determination of silver,gold,platinum,palladium,iridium,ruthenium,lead,nickel,copper,iron,tin,zinc,magnesium,manganese,aluminium,calcium,sodium,potassium,chromium and silicon contents - Inductively c
GB/T 10003-2026 — Biaxially oriented polypropylene (BOPP) film
GB/T 10004-2026 — Plastic/Plastic laminated films and pouches for packaging
Secure payment via Stripe
Payments accepted
GB/T 34609.1-2017
$145.00