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GB/T 34438-2017Determination of cadmium in toy materials—Flame atomic absorption spectrometry (English PDF)

玩具材料中镉的测定 火焰原子吸收光谱法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

October 14, 2017

Implementation date

May 1, 2018

Scope

GB/T 34438-2017 is the English-translated version of 玩具材料中镉的测定 火焰原子吸收光谱法.

GB/T 34438-2017 is the Chinese standard "Determination of cadmium in toy materials—Flame atomic absorption spectrometry". Its scope clause reads: This standard specifies the method of flame atomic absorption spectrometry determination of cadmium content in toy materials.

This standard applies to toys in the coating, plastic (except fluorine plastic), natural or synthetic textiles, paper and cardboard, metal materials, cadmium content Determination. Its clauses include principle; reagents and materials.

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Document preview — GB/T 34438-2017

National Standard of the People's Republic of China

ICS
97.200.50
Classification
Y 57

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • 1 Scope
  • 2 Normative references
  • 3 principle
  • 4 Reagents and materials

1 Scope

This standard specifies the method of flame atomic absorption spectrometry determination of cadmium content in toy materials.

This standard applies to toys in the coating, plastic (except fluorine plastic), natural or synthetic textiles, paper and cardboard, metal materials, cadmium content

Determination.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version applies to this article

Pieces. For undated references, the latest edition (including all amendments) applies to this document.

GB/T 602 chemical reagent impurity standard solution preparation

GB/T 6379.2 accuracy of measurement methods and results (accuracy and precision) Part 2. Determination of standard measurement methods repeated

The basic method of sexuality and reproducibility

GB/T 6682 analytical laboratory water specifications and test methods

3 principle

Sample using electric heating plate digestion or microwave digestion. Digestion solution was determined by flame atomic absorption spectrometry at a wavelength of 228.8nm,

External standard method to determine the concentration of cadmium in the solution, calculate the content of cadmium in the sample.

4 Reagents and materials

Unless otherwise noted, all reagents are superior grade pure.

4.1

water, at least to meet the three water GB/T 6682 requirements.

4.2

nitric acid, the mass fraction is 65% ~ 68%.

4.3

sulfuric acid mass fraction of 95% to 98%.

4.4 Hydrogen peroxide

The mass fraction is 35%.

4.5

hydrochloric acid mass fraction of 35% to 37%.

4.6 Nitric acid

The volume fraction is 10%.

4.7

sulfuric acid volume fraction is 10%.

4.8

Cadmium standard solution (1000mg/L), according to GB/T 602 preparation or direct purchase with traceability certificate of the standard material.

4.9 Cadmium standard working solution 1

Pipette a certain volume of cadmium standard solution (4.8) in 100mL volumetric flask, diluted with nitric acid (4.6) until engraved

Degree, mixing, formulated into a concentration of 0.05mg/L, 0.1mg/L, 0.2mg/L, 0.5mg/L, 1.0mg/L standard solution.

4.10 Cadmium standard working solution 2

Pipette a certain volume of cadmium standard solution (4.8) in 100mL volumetric flask, diluted with sulfuric acid (4.7) until engraved […]

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

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