GB/T 34438-2017Determination of cadmium in toy materials—Flame atomic absorption spectrometry (English PDF)
玩具材料中镉的测定 火焰原子吸收光谱法
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Issued by
SAMR; SAC
Level / Type
National · Recommended
Issue date
October 14, 2017
Implementation date
May 1, 2018
Scope
GB/T 34438-2017 is the English-translated version of 玩具材料中镉的测定 火焰原子吸收光谱法.
GB/T 34438-2017 is the Chinese standard "Determination of cadmium in toy materials—Flame atomic absorption spectrometry". Its scope clause reads: This standard specifies the method of flame atomic absorption spectrometry determination of cadmium content in toy materials.
This standard applies to toys in the coating, plastic (except fluorine plastic), natural or synthetic textiles, paper and cardboard, metal materials, cadmium content Determination. Its clauses include principle; reagents and materials.
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Document preview — GB/T 34438-2017
National Standard of the People's Republic of China
- ICS
- 97.200.50
- Classification
- Y 57
Issued by: State Administration for Market Regulation; Standardization Administration of the PRC
Contents
- 1 Scope
- 2 Normative references
- 3 principle
- 4 Reagents and materials
1 Scope
This standard specifies the method of flame atomic absorption spectrometry determination of cadmium content in toy materials.
This standard applies to toys in the coating, plastic (except fluorine plastic), natural or synthetic textiles, paper and cardboard, metal materials, cadmium content
Determination.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version applies to this article
Pieces. For undated references, the latest edition (including all amendments) applies to this document.
GB/T 602 chemical reagent impurity standard solution preparation
GB/T 6379.2 accuracy of measurement methods and results (accuracy and precision) Part 2. Determination of standard measurement methods repeated
The basic method of sexuality and reproducibility
GB/T 6682 analytical laboratory water specifications and test methods
3 principle
Sample using electric heating plate digestion or microwave digestion. Digestion solution was determined by flame atomic absorption spectrometry at a wavelength of 228.8nm,
External standard method to determine the concentration of cadmium in the solution, calculate the content of cadmium in the sample.
4 Reagents and materials
Unless otherwise noted, all reagents are superior grade pure.
4.1
water, at least to meet the three water GB/T 6682 requirements.
4.2
nitric acid, the mass fraction is 65% ~ 68%.
4.3
sulfuric acid mass fraction of 95% to 98%.
4.4 Hydrogen peroxide
The mass fraction is 35%.
4.5
hydrochloric acid mass fraction of 35% to 37%.
4.6 Nitric acid
The volume fraction is 10%.
4.7
sulfuric acid volume fraction is 10%.
4.8
Cadmium standard solution (1000mg/L), according to GB/T 602 preparation or direct purchase with traceability certificate of the standard material.
4.9 Cadmium standard working solution 1
Pipette a certain volume of cadmium standard solution (4.8) in 100mL volumetric flask, diluted with nitric acid (4.6) until engraved
Degree, mixing, formulated into a concentration of 0.05mg/L, 0.1mg/L, 0.2mg/L, 0.5mg/L, 1.0mg/L standard solution.
4.10 Cadmium standard working solution 2
Pipette a certain volume of cadmium standard solution (4.8) in 100mL volumetric flask, diluted with sulfuric acid (4.7) until engraved […]
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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.
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