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GB/T 30740-2014Determination of total organic carbon in marine sediment—Nondispersive infrared absorption (English PDF)

海洋沉积物中总有机碳的测定 非色散红外吸收法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

March 27, 2014

Implementation date

October 1, 2014

Scope

GB/T 30740-2014 is the English-translated version of 海洋沉积物中总有机碳的测定 非色散红外吸收法.

GB/T 30740-2014 is the Chinese national method for determining the total organic carbon of marine sediment by non-dispersive infrared absorption.

It specifies the principle, the reagents and apparatus, the collection and preparation of the sample - including the removal of inorganic carbon - the combustion and measurement procedure, and the calculation, precision and test report.

It applies to sediments from estuaries, bays, coastal waters and the open sea. Marine monitoring institutes and environmental laboratories use it, since organic carbon is one of the indicators that describe the state of the sea bed. Issued on 27 March 2014, it has applied since 1 October 2014.

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Document preview — GB/T 30740-2014

National Standard of the People's Republic of China

ICS
07.060; 13.060
Classification
Z 17

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Foreword
  • 1 Scope
  • 2 Normative references
  • 3 Terms and Definitions
  • 4 Principle of the method

Foreword

This standard was drafted in accordance with GB/T 1.1-2009 given rules.

1 Scope

This standard specifies the method for the determination of total organic carbon in marine sediments with a non-dispersive infrared absorption.

This standard applies to the determination of estuaries, bays, coastal and ocean sediments TOC.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein Member. For undated references, the latest edition (including any amendments) applies to this document.

GB 17378.5-2007 marine monitoring Part 5. Sediment analysis

3 Terms and Definitions

The following terms and definitions apply to this document.

3.1 Marine sediments

General term for various marine seabed sediment formed by deposition.

3.2 Total carbon totalcarbon; TC

Carbon in general, including organic carbon and inorganic carbon.

3.3 Total inorganic carbon totalinorganiccarbon; TIC

Inorganic carbon in general, including the carbonate or bicarbonate of carbon present in the form.

3.4 TOC totalorganiccarbon; TOC

Organic general form of the element carbon.

4 Principle of the method

The samples were high temperature combustion or acid treatment, the appropriate form of carbon is converted to carbon dioxide, generated by the sample and the sample of Proportional to the carbon content. An oxygen carrier, the content of carbon dioxide to form carbon content is calculated corresponding measured by an infrared detector.

TOC can be used directly or subtraction method was measured.

4.1 Determination of total organic carbon subtraction

4.1.1 Determination of total carbon

Samples from the injector into the combustion temperature, which leads to high purity oxygen in the sample of all carbonaceous material is oxidized to carbon dioxide, produced by

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 20 pages — is available in the English PDF.

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