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GB/T 19144-2010Isolation method for kerogen from sedimentary rock (English PDF)

沉积岩中干酪根分离方法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

September 2, 2010

Implementation date

December 1, 2010

Scope

GB/T 19144-2010 is the English-translated version of 沉积岩中干酪根分离方法.

GB/T 19144-2010 is the Chinese standard "Isolation method for kerogen from sedimentary rock". Its scope clause reads: This standard specifies the preparation, separation procedures and quality requirements for kerogen separation equipment, equipment, reagents, samples.

This standard applies to the kerogen separation of sedimentary rock samples and also to the separation of insoluble organic matter in modern sediments. Its clauses include principle; instruments and equipment; reagents and materials; sample preparation.

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Document preview — GB/T 19144-2010

National Standard of the People's Republic of China

Classification
E 11
Replacing
GB/T 19144-2003

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • 1 Scope
  • 2 principle
  • 3 instruments and equipment
  • 4 reagents and materials
  • 5 sample preparation

1 Scope

This standard specifies the preparation, separation procedures and quality requirements for kerogen separation equipment, equipment, reagents, samples.

This standard applies to the kerogen separation of sedimentary rock samples and also to the separation of insoluble organic matter in modern sediments.

2 principle

The kerogen separation uses chemical and physical methods to remove inorganic minerals and chloroform soluble organic matter in the rock, allowing other organic matter to be enriched.

3 instruments and equipment

3.1 acid reaction device

made of hydrofluoric acid corrosion material.

3.2 heating mixing device

can be heated to about 90 °C, adjustable speed.

3.3 Centrifuge

the maximum speed of not less than 4000r/min, with a volume of about 400mL, 50mL, 10mL of the centrifuge tube.

3.4 electric drying oven

the maximum temperature of not less than.200 °C.

3.5 refrigerator

freezing temperature below -5 °C.

3.6 Ultrasonic cleaner or oscillator

Output power 250W.

3.7 high temperature furnace

temperature control 1000 °C ± 20 °C.

3.8 Analysis of balance

resolution 0.1mg.

3.9 agate mortar

about 8cm in diameter.

3.10 Crucible

resistant to high temperature of 1000 °C.

3.11

sealed test sample grinder.

3.12 standard test sieve

0.18mm, 0.5mm, 1.0mm.

3.13 balance

resolution 0.5g, the maximum weighing 500g.

3.14 Density meter

relative density measurement range of 1.00g/mL ~ 2.50g/mL.

4 reagents and materials

4.1 hydrochloric acid

chemical pure, dubbed about 1mol/L, 6mol/L, 8mol/L solution.

4.2 hydrofluoric acid

chemically pure.

4.3 glacial acetic acid

chemically pure

4.4 Arsenic free zinc particles

analytical grade.

4.5 chloroform

analytical grade.

4.6 silver nitrate

analysis of pure, dubbed 1% solution.

4.7 sodium hydroxide

analysis of pure, dubbed 0.5mol/L solution.

4.8 heavy liquid

relative density d204 2.0g/mL ~ 2.1g/mL of the relevant solution, the specific preparation method see Appendix A.

4.9 pH test paper

pH1 ~ pH12.

5 sample preparation

5.1 rock samples

Separate kerogen rock samples, the organic carbon content should be consistent with the provisions of Table 1.

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

Referenced standards

Similar standards

Editions of GB/T 19144

EditionTitleRevisionStatus
GB/T 19144-2010Isolation method for kerogen from sedimentary rockcurrent editionCurrent
GB/T 19144-2003Isolation method for kerogen from sedimentary rockprevious editionSuperseded

This page sells the current edition, GB/T 19144-2010. Earlier editions are listed for reference only.

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