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GB/T 15926-2010Method for chemical analysis of bismuth ores - Determination of bismuth content (English PDF)

铋矿石化学分析方法 铋量测定

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

November 10, 2010

Implementation date

February 1, 2011

Scope

GB/T 15926-2010 is the English-translated version of 铋矿石化学分析方法 铋量测定.

GB/T 15926-2010 is the Chinese standard "Method for chemical analysis of bismuth ores - Determination of bismuth content". Its scope clause reads: This standard specifies the method for the determination of bismuth ores of bismuth content.

This standard applies to the determination of bismuth content of bismuth ore. Measuring range. 0.1% or more of bismuth. Its clauses include reagents.

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Document preview — GB/T 15926-2010

National Standard of the People's Republic of China

ICS
73.060
Classification
D 42
Replacing
GB/T 15926-1995

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • 1 Scope
  • 2 Normative references
  • 4 Reagents
  • 4.12 Bismuth standard stock solution

1 Scope

This standard specifies the method for the determination of bismuth ores of bismuth content.

This standard applies to the determination of bismuth content of bismuth ore.

Measuring range. 0.1% or more of bismuth.

2 Normative references

The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent

Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research

Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.

Laboratory use specifications and test methods GB/T 6682 Analysis

Principle 3

Samples with hydrochloric acid, nitric acid, perchloric acid decomposition, nitric acid medium at pH 1.5 to 2.0, and ascorbic acid with vanadium (V) and iron (III), thiourea, tartaric acid masking interference copper, antimony, tin, thorium, zirconium, niobium, with the xylenol orange indicator, with EDTA standard solution drops

Set by the amount of consumption of EDTA standard solution, calculate the amount of bismuth.

4 Reagents

Unless otherwise indicated in the analysis are consistent with the use of analytical reagents and GB/T 6682 water analytical laboratory.

4.1

ascorbic acid.

4.2

hydrochloride (rho1.19g/mL).

Nitrate 4.3 (rho1.40g/mL).

4.4

perchloric acid (rho1.67g/mL). Warning. explosive materials, careful 4.5 nitric acid (11).

4.6

nitric acid (199).

4.7

Aqueous ammonia (11).

4.8

ammonia (298).

4.9

thiourea solution (60g/L).

4.10

tartaric acid solution (100g/L).

4.11

sodium acetate solution (200g/L).

4.12 Bismuth standard stock solution

Weigh 1.0000g bismuth (mass fraction >=99.99%), placed in 250mL beaker, add 20mL

Nitric acid (4.5), cover the surface of the pan, over low heat until completely dissolved, boil rush to make nitrogen oxides, remove the cooled to room temperature, the solution is transferred

1000mL volumetric flask, with nitric acid (4.6) and Beibi purged dish surface, and dilute to the mark. The concentration of the solution is bismuth

1.0mg/mL.

4.13

edetate disodium (EDTA) titration standard solution (0.005mol/L).

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

Similar standards

Editions of GB/T 15926

EditionTitleRevisionStatus
GB/T 15926-2010Method for chemical analysis of bismuth ores - Determination of bismuth contentcurrent editionCurrent
GB/T 15926-1995Method for chemical analysis of bismuth ores - Determination of bismuth contentprevious editionSuperseded

This page sells the current edition, GB/T 15926-2010. Earlier editions are listed for reference only.

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