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GB/T 12532-2008Determination of total ash content in edible mushroom (English PDF)

食用菌灰分测定

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Issued by

Standardization Administration of China

Level / Type

National · Recommended

Issue date

August 7, 2008

Implementation date

December 1, 2008

Scope

GB/T 12532-2008 is the English-translated version of 食用菌灰分测定.

GB/T 12532-2008 — This standard specifies the method for determination of edible fungi and products of ash. This standard applies to edible mushrooms fruiting bodies, mycelium and products measuring ash content.

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Document preview — GB/T 12532-2008

National Standard of the People's Republic of China

ICS
67.080.20
Classification
B 31
Replacing
GB/T 12532-1990

Issued by: Standardization Administration of China

Contents

  • Foreword
  • 1 Scope
  • 2 Terms and definitions
  • 4 Instruments and equipment
  • 5 Measuring step
  • 5.1 Sampling
  • 5.2 Crucible constant weight

Foreword

This standard replaces GB/T 12532-1990 "Edible Determination of ash." this standard and GB/T 12532-1990 compared to major changes are as follows.

--- According to GB/T 1.1-2000 "Standardization Guide Part 1. Standard structure and write rules" of standard text format it has been revised;

--- The standard formerly known by the English name "Determinationofashinediblefungi" to "Determinationofash contentinediblemushroom ";

--- Scope from "Edible" to "edible mushrooms and their products";

--- Remove the "reference standard";

--- Added "sampling" requirement;

--- Modify ashing temperature "600 °C" is 525 °C ± 25 °C;

--- Modify sample weight "2g ~ 10g" to "4.0g ~ 25.0g";

--- Revised the "measurement result calculation method", the "dry, fresh samples of ash determination" are combined, not to distinguish, depending on the properties of the sample is determined Weigh the sample volume. Added "result indicates" revised "allowable difference." the standard proposed by China Federation of Supply and Marketing Cooperatives.

The standard by the China Federation of Supply and Marketing Cooperatives Kunming Institute of Edible Fungus.

This standard is mainly drafted by. China Federation of Supply and Marketing Cooperatives Kunming Institute of Edible Fungus.

1 Scope

This standard specifies the method for determination of edible fungi and products of ash.

This standard applies to edible mushrooms fruiting bodies, mycelium and products measuring ash content.

2 Terms and definitions

The following terms and definitions apply to this standard.

The sample was obtained after high temperature burning residue.

Principle 3

After the sample was carbonized at 525 °C ± 25 °C temperature of ignition to constant weight, saying the quality of the sample residue ash content.

4 Instruments and equipment

4.1 resistance furnace temperature. 1000 °C.

4.2 Crucible. 60mL ~ 90mL silica crucible or a porcelain crucible.

4.3 water bath.

4.4 electric oven.

4.5 dryer. fitted with an efficient desiccant.

4.6 Analysis of balance. a sense of the amount of 0.0001g.

5 Measuring step

5.1 Sampling

5.1.1 Sampling method and number

In the bulk cargo, packaging products sachet on the same goods (boxes, boxes, etc.) as the base, the quality of the same goods in bulk products (Kg) or number of pieces as the base, from different locations the entire consignment of a random sample of the entire consignment the following number of member base.

--- Bulk goods 50 or less, the base sample is 2;

--- Bulk cargo 51 ~ 100, sampling base is 4;

--- Bulk cargo 101 ~ 200, the sampling base 5;

--- Whole lot more than 201, with a minimum of 6 for each additional 50 plus a draw.

Small package when insufficient quality inspection required quality, appropriate to increase the sample size.

5.1.2 Reduced sample and the test sample

When the sample is too large, the sample was mixed and spread evenly into a square, random sampling reduction. Reduced test sample obtained from a sample, according to inspection the required amount of sample test items sampled four times, including one for the test sample, two samples for re-examination, as a kind of deposit.

5.2 Crucible constant weight

Wash crucible transferred to 525 °C ± 25 °C high temperature resistance furnace burning 1h, cooled to below 200 °C removed and transferred to a dryer cold to room temperature and weighed. Repeated burning, cooling, weighing, up to twice the difference between before and after mass not exceeding 0.0002g, is a constant weight.

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 4 pages — is available in the English PDF.

Referenced standards

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