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GB/T 10512-2008Determination of phosphorus content for nitrophosphate - Quinoline phosphomolybdate gravimetric method (English PDF)

硝酸磷肥中磷含量的测定 磷钼酸喹啉重量法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

June 17, 2008

Implementation date

September 1, 2008

Scope

GB/T 10512-2008 is the English-translated version of 硝酸磷肥中磷含量的测定 磷钼酸喹啉重量法.

GB/T 10512-2008 is the Chinese standard "Determination of phosphorus content for nitrophosphate - Quinoline phosphomolybdate gravimetric method". Its scope clause reads: This standard specifies the determination of quinoline phosphomolybdate gravimetric method nitrate fertilizer, the phosphorus content of phosphorus and potassium nitrate.

This standard applies to all kinds of technology, the nitrate fertilizer, water solubility of phosphorus and phosphorus content of phosphorus and potassium nitrate. Its clauses include reagents and materials; instruments.

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Document preview — GB/T 10512-2008

National Standard of the People's Republic of China

ICS
65.080
Classification
G 20
Replacing
GB/T 10512-1989

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Foreword
  • 1 Scope
  • 2 Normative references

1 Scope

This standard specifies the determination of quinoline phosphomolybdate gravimetric method nitrate fertilizer, the phosphorus content of phosphorus and potassium nitrate.

This standard applies to all kinds of technology, the nitrate fertilizer, water solubility of phosphorus and phosphorus content of phosphorus and potassium nitrate.

2 Normative references

The following documents contain provisions which, through reference in this standard and become the standard terms. For dated references, subsequent

Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to the agreement are based on research

Whether the latest versions of these documents. For undated reference documents, the latest versions apply to this standard.

GB/T 10511-2008 nitrophosphate total nitrogen content after distillation titration

HG/T 2843 fertilizer products chemical analysis commonly used in standard titration solution, standard solution, reagent solution and indicator solution

Principle 3

Water and disodium EDTA solution was extracted nitrate fertilizer, water-soluble phosphorus Phosphorus Potassium nitrate and phosphorus, phosphate extracts CKS Ion in acidic medium to form a yellow phosphomolybdic acid reagent and Quimociac quinoline precipitation, determination of phosphorus using quinoline phosphomolybdate gravimetric method.

4 Reagents and materials

The following part-corrosive reagents and solutions, the operator should be careful! If splashed on skin, immediately wash with water, severe cases should

Immediate treatment.

The standard reagent preparation, and water solution used in the method of preparation and specifications are not specified, shall comply with HG/T 2843 stipulated.

4.1

Disodium ethylenediaminetetraacetate (EDTA) solution, 37.5g/L;

Weigh 37.5gEDTA in 1000mL beaker, add a small amount of water dissolved, diluted with water to 1000mL, and mix.

4.2

Quimociac reagent;

Nitric acid solution was 4.3, 1 + 1.

5 Instruments

5.1

usually laboratory instruments;

5.2

Ovens can be controlled (180 ± 2) °C;

5.3 Glass filter crucible, No

4, volume 30mL;

5.4

constant temperature water bath oscillator, to control the temperature (60 ± 2) °C or roundabout reciprocating oscillator oscillator.

Step 6 Analysis

Do two parallel determination of sample.

6.1 Sample Weighing

Weigh phosphorus pentoxide containing 100mg ~ 180mg samples (sample preparation see GB/T 10511-2008 6.1) to the nearest

0.0002g.

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

Referenced standards

Similar standards

Editions of GB/T 10512

EditionTitleRevisionStatus
GB/T 10512-2008Determination of phosphorus content for nitrophosphate - Quinoline phosphomolybdate gravimetric methodcurrent editionCurrent
GB/T 10512-1989Determination of phosphorus content for nitrophosphate - Quinoline phosphomolybdate gravimetric methodprevious editionSuperseded

This page sells the current edition, GB/T 10512-2008. Earlier editions are listed for reference only.

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