GB 2466-1981Pyrites and concentrate -- Determination of copper content -- Flame atomic absorption spectrometric and spectrophotometric methods (English PDF)
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Issued by
General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Level / Type
National · Mandatory
Issue date
May 14, 2008
Implementation date
October 1, 2008
Scope
GB 2466-1981 (Pyrites and concentrate -- Determination of copper content -- Flame atomic absorption spectrometric and spectrophotometric methods) is available as an English-translated PDF.
GB 2466-1981 — This standard specifies the flame atomic absorption spectrometry and spectrophotometric determination of pyrite and sulfur concentrate copper content.
This standard applies to pyrite and sulfur concentrate products in the determination of copper content of 0.01% to 1%.
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Document preview — GB 2466-1981
National Standard of the People's Republic of China
- ICS
- 73.060.01
- Classification
- D 51
- Replacing
- GB/T 2466.1-1996; GB/T 2466.3-1996
Issued by: General Administration of Quality Supervision, Inspection and Quarantine of the People's Republic of China, Standardization Administration of the People's Republic of China
Contents
- Foreword
- 1 Scope
- 2 Normative references
- 3 Sample
- 4 General provisions
- 5 Analytical methods
- 5.1 Flame atomic absorption spectrometry
Foreword
This standard replaces GB/T 2466.1-1996 "Determination of copper content in pyrite and concentrate - Part 1. Flame atomic absorption spectrometry Act "and GB/T 2466.3-1996" Determination of copper content in pyrite and concentrate - Part 3. BOC spectrophotometry, "the two Standard merged into a standard, divided into two methods.
This standard is proposed by China Petroleum and Chemical Industry Association.
This standard by the Chemical Industry Standardization Technical Committee of mineral ore centralized.
This standard was drafted. Blue Blue Sea Design Institute.
1 Scope
This standard specifies the flame atomic absorption spectrometry and spectrophotometric determination of pyrite and sulfur concentrate copper content.
This standard applies to pyrite and sulfur concentrate products in the determination of copper content of 0.01% to 1%.
2 Normative references
The following documents contain provisions which, through reference in this standard and become the standard terms. All dated references, which are subsequently owned Amendments (not including errata content) or revisions do not apply to this standard, however, encourage the parties to reach an agreement based on this standard research Whether you can use the latest versions of these files. For undated references, the latest version applies to this standard.
GB/T 6003.1 woven wire mesh test sieve (GB/T 6003.1-1997, eqv ISO 3310-1.:1990) GB/T 6682 analytical laboratory water specifications and test methods (GB/T 6682-1992, neq ISO 3696. 1987) GB/T 9721 chemical reagent molecular absorption spectrophotometry (UV and visible light part) GB/T 9723 chemical reagent flame atomic absorption spectrometric method
3 Sample
The sample was passed 150µm test sieve (GB/T 6003.1), dried at 100 °C ~ 105 °C to constant weight, placed in a desiccator, cooled to Room temperature.
4 General provisions
The water used in this standard should be consistent with the three water GB/T 6682 specifications; listed reagents except for special provisions, are analytically pure reagents.
5 Analytical methods
5.1 Flame atomic absorption spectrometry
5.1.1 Method summary
The sample was dissolved with hydrochloric acid-nitric acid, air-acetylene flame was used in a dilute hydrochloric acid medium, at a wavelength of 324.8 nm of an atomic absorption spectrometer Absorbance was measured to determine the copper content by the working curve method.
5.1.2 Reagents and solutions
5.1.2.1 Hydrochloric acid.
5.1.2.2 hydrochloric acid solution. 1 +1.
5.1.2.3 Nitric acid.
5.1.2.4 Copper standard solution. 1.00mg/mL. Weigh 1.0000g of high-purity metallic copper in 250mL beaker, add 40mL nitric acid Solution (1 + 1), cover the watch glass, heated to dissolve completely, cooled, transferred to 1000mL volumetric flask, diluted with water to the mark, shake. This solution Liquid copper (Cu) content of 1.00mg/mL.
5.1.2.5 copper standard solution. 100µg/mL. Pipette 50.0mL copper standard solution (5.1.2.4) in 500mL volumetric flask, diluted with water Release to the mark, shake well. This solution contains copper (Cu) amount 100µg/mL.
5.1.3 Instruments
Flame atomic absorption spectrometer. should be consistent with the provisions of GB/T 9723.
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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 5 pages — is available in the English PDF.
Referenced standards
Normative references
- GB/T 6003.1Test sieves—Technical requirements and testing—Part 1:Test sieves of metal wire cloth
- GB/T 6003.1-1997Test sieves—Technical requirements and testing—Part 1:Test sieves of metal wire cloth
- GB/T 6682Water for analytical laboratory use - Specification and test methods
- GB/T 6682-1992Water for analytical laboratory use - Specification and test methods
- GB/T 9721Chemical reagent - General rules for the molecular absorption spectrophotometry (ultraviolet and visible)
- GB/T 9723Chemical Reagent - General rule for flame atomic absorption spectrometric analysis
ISO 3310 · ISO 3696
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Related Standards
GB/T 6003.1-2022 — Test sieves—Technical requirements and testing—Part 1:Test sieves of metal wire cloth
GB/T 6682-2008 — Water for analytical laboratory use - Specification and test methods
GB/T 9721-2006 — Chemical reagent - General rules for the molecular absorption spectrophotometry (ultraviolet and visible)
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