SN/T 3056.4-2011Determination of essential parameers of chemical raw materials for use in fireworks and firecrackers. Part 4: Basic cupric carbonate (English PDF)
烟花爆竹用化工原材料关键指标的测定 第4部分:碱式碳酸铜
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Issued by
General Administration of Customs
Level / Type
National · Recommended
Issue date
September 9, 2011
Implementation date
April 1, 2012
Scope
SN/T 3056.4-2011 is the English-translated version of 烟花爆竹用化工原材料关键指标的测定 第4部分:碱式碳酸铜.
SN/T 3056.4-2011 — SN/T 3056 provisions of this part of the fireworks with the determination of basic copper carbonate copper content, the determination of iron content, salt Determination of acid insoluble content, determination of sulphate content determination method and moisture content.
This section applies to fireworks measuring basic copper carbonate copper content, Determination of iron content, measured hydrochloric acid insoluble content of sulfur Determination of salt content and moisture content determination.
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Document preview — SN/T 3056.4-2011
National Standard of the People's Republic of China
- Classification
- Y 88
Issued by: General Administration of Customs
Contents
- Foreword
- 1 Scope
- 2 Normative references
- 3 Determination
- 3.1 Drying the sample
- 3.2 Determination of hydrochloric acid insoluble content
Foreword
"Determination of fireworks with chemical raw materials key indicators" SN/T 3056 series of standards is divided into 15 parts.
--- Part 1. potassium hydrogen phthalate;
--- Part 2. sodium fluoride;
--- Part 3. Red Lead;
--- Part 4. basic copper carbonate;
--- Part 5. sulfur;
--- Part 6. strontium sulfate;
--- Part 7. copper sulfate;
--- Part 8. potassium chlorate;
--- Part 9. sodium bicarbonate;
--- Part 10. strontium carbonate;
--- Part 11. iron;
--- Part 12. barium nitrate;
--- Part 13. Silver nitrate;
--- Part 14. bismuth oxide;
--- Part 15. potassium dichromate.
This section SN/T 3056 Part 4.
This section drafted in accordance with GB/T 1.1-2009 given rules.
This section proposed and managed by the National Certification and Accreditation Administration Committee.
1 Scope
SN/T 3056 provisions of this part of the fireworks with the determination of basic copper carbonate copper content, the determination of iron content, salt Determination of acid insoluble content, determination of sulphate content determination method and moisture content.
This section applies to fireworks measuring basic copper carbonate copper content, Determination of iron content, measured hydrochloric acid insoluble content of sulfur Determination of salt content and moisture content determination.
2 Normative references
The following documents for the application of this document is essential. For dated references, only the dated version suitable for use herein Member. For undated references, the latest edition (including any amendments) applies to this document.
Preparation of GB/T 601 chemical reagent standard titration solution General Method GB/T 3049 Industrial chemicals determination of iron content 1,10 phenanthroline spectrophotometry Lynn GB/T 6003.1 Test sieves of metal wire cloth Laboratory use specifications and test methods GB/T 6682 Analysis GB/T 8170 repair value expressed about the rules and limit values and judgment HG/T 3696.1 ~ 3696.3 inorganic chemical products, chemical analysis using standard titration solution, impurity standard solution, preparations and articles Preparation
3 Determination
3.1 Drying the sample
Sample at 105 °C ± 2 °C dried 3h, into the dryer to cool reserve. After drying the sample project to detect water points outside use.
3.2 Determination of hydrochloric acid insoluble content
3.2.1 Principle
After the sample is dissolved hydrochloric acid by filtration, dried insolubles, call quality.
3.2.2 Reagents
Unless otherwise indicated in the analysis using only confirm at least three water analytical grade reagents and GB/T 6682 stipulated.
Hydrochloric acid (11).
3.2.3 Instruments
3.2.3.1 Drying oven. Controlled temperature 105 °C ± 2 °C.
3.2.3.2 Analytical balance. accuracy of 0.1mg.
......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 7 pages — is available in the English PDF.
Referenced standards
Normative references
- GB/T 601Chemical Reagent - Preparations of Standard Volumetric Solutions
- GB/T 3049Chemical products for industrial use - General method for determination of iron content. 1, 10-Phenanthroline spectrophotometric method
- GB/T 6003.1Test sieves—Technical requirements and testing—Part 1:Test sieves of metal wire cloth
- GB/T 6682Water for analytical laboratory use - Specification and test methods
- GB/T 8170Rules of rounding off for numerical values & expression and judgement of limiting values
- HG/T 3696.1Inorganic chemical products - Preparation of standard solutions, reagent solutions and products for chemical analysis - Part 1: Preparation of standard volumetric solutions
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