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JC/T 620-2021Sampling method for lime (English PDF)

石灰取样方法

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Issued by

Ministry of Industry and Information Technology of PRC

Level / Type

National · Recommended

Issue date

March 5, 2021

Implementation date

July 1, 2021

Scope

JC/T 620-2021 is the English-translated version of 石灰取样方法.

JC/T 620-2021 — This document specifies the terms and definitions, sampling tools, sampling sites and locations, total sampling size, sampling procedures, sample preparation, packaging and storage, sampling sheets, of lime sampling.

This document is applicable to the inspection sampling of the production and use of quicklime, quicklime powder, slaked lime powder.

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Document preview — JC/T 620-2021

National Standard of the People's Republic of China

ICS
91.100.10

Issued by: Ministry of Industry and Information Technology of PRC

Contents

  • Foreword...3
  • 1 Scope...5
  • 2 Normative references...5
  • 3 Terms and definitions...5
  • 4 Sampling tools...6
  • 5 Sampling site and sampling location...6
  • 6 Total sampling...7
  • 7 Sampling steps...7
  • 8 Sample preparation...9
  • 9 Packaging and storage...9
  • 10 Sampling sheet...9
  • Appendix A (Informative) Lime sampler...10

Foreword

This document was drafted in accordance with the rules given in GB/T 1.1-2020

"Directives for standardization - Part 1.Rules for the structure and drafting of

standardizing documents"

This document replaces JC/T 620-2009.Compared with JC/T 620-2009, in

addition to structural adjustments and editorial changes, the main technical

changes are as follows.

a) ADD the scope (see Chapter 1);

b) In terms and definitions, CANCEL the "batch", "batch size", "number";

ADD the "automatic sampling" (see Chapter 2);

c) CANCEL the "batch size" (Chapter 4 of the 2009 edition);

d) In the sampling tools, ADD the automatic sampler; MOVE the lime

sampling tube and diagram of sampling shovel into the informative

appendix A; MODIFY the diameter of sampling tube (see Chapter 4; 5.1

of the 2009 edition);

e) COMBINE the sampling site and sampling location; MODIFY the

requirements for sampling location (see Chapter 5; 5.2 and 5.3 of the 2009

edition);

f) MODIFY the "sampling method" into "sampling procedure"; MODIFY the

classification of sampling locations (see Chapter 7; 5.5 of the 2009 edition);

g) MODIFY the packaging and storage (see Chapter 9; 5.7 of the 2009

edition);

h) ADD the Appendix A.

1 Scope

This document specifies the terms and definitions, sampling tools, sampling

sites and locations, total sampling size, sampling procedures, sample

preparation, packaging and storage, sampling sheets, of lime sampling.

This document is applicable to the inspection sampling of the production and

use of quicklime, quicklime powder, slaked lime powder.

2 Normative references

The provisions in following documents become the provisions of this Standard

through reference in this Standard. For the dated documents, only the versions

with the dates indicated are applicable to this document; for the undated

documents, only the latest version (including all the amendments) is applicable

to this standard.

JC/T 619 Terms for lime

3 Terms and definitions

The terms and definitions as defined in JC/T 619, as well as the following terms

and definitions, apply to this document.

3.1

Manual sampling

Collection of lime samples by the use of manual sampling tools.

3.2

Automatic sampling

Collection of lime samples by the use of an autosampler.

3.3

Unit sample

A lime sample, which is taken from a point or part of each inspection lot,

according to the specified amount.

3.4

Composite sample

A sample, which is obtained by taking the specified volume of all the unit

lime samples, that are obtained from an inspection lot, after uniformly and

thoroughly mixing them.

4 Sampling tools

4.1 Material of sampling tool

The sampling tools shall be made of materials, that do not chemically react with

lime, such as stainless steel.

4.4 Autosampler

Used for automatic sampling of powdered lime. Refer to Appendix A.3 for

commonly used autosamplers.

5 Sampling site and sampling location

5.1 The sampling site shall be representative. The sampling shall not be carried

out in rainwater OR in a heavily polluted environment.

5.2 The sampling of lime production inspection should be at the following

locations.

5.3 Sampling for lime use inspection should be at the following locations.

6 Total sampling

The total amount of quicklime, which is sampled for each inspected lime

inspection lot, shall not be less than 24 kg; the total amount of quicklime powder

and slaked lime powder sampled shall not be less than 5 kg.

7 Sampling steps

7.1 Sampling from storage yards, warehouses, vehicles (ships)

Use ordinary pointed steel shovel or I-type manual sampling shovel for

sampling. Randomly select 12 sampling points, from different parts of each

inspection lot.

7.2 Sampling at the inlet and outlet of conveyor belts, lime silos, bulk

trucks

For lumpy lime, use I-type manual sampling shovel or ordinary pointed steel

shovel to take sample. From the flowing quicklime of each inspection lot, take

12 unit samples at regular intervals; each sample is not less than 2 kg. If there

is a large block, which has the largest size greater than 100 mm, in the sampling

point, it shall be processed in accordance with 7.1.

7.3 Sampling at the outlet of the lime kiln

Select the appropriate sampling location, according to the discharge method of

the lime kiln's discharge port AND the lime temperature; proceed according to

7.2.

7.4 Sampling in bags

For bags of lime not more than 100 kg, randomly take 10 bags from each

inspection lot (the bags shall be intact). Use the manual sampling tubes for

sampling. Insert the sampling tube, obliquely from the opening of the bag, to an

appropriate depth, in the bag. Take out a tube of lime. The sampling volume of

each bag of lime shall not be less than 0.5 kg.

8 Sample preparation

8.1 Composite sample

The unit samples, which are obtained from each inspection lot, shall be

uniformly mixed, immediately after unpacking. Use the quartering method to

reduce it.

8.2 Test sample and retained sample

Divide the reduced mixed sample equally, one is the test sample AND the other

is the retained sample.

9 Packaging and storage

9.1 The obtained test sample and retained sample shall be stored immediately

in a clean, dry, moisture-proof container, that does not affect the performance

of lime, AND sealed.

10 Sampling sheet

After the sample is obtained, the person in charge of sampling shall fill in the

sampling sheet. The sampling sheet shall include at least the following.

JC/T 620-2021

JC

BUILDING INDUSTRY STANDARD OF

THE PEOPLE'S REPUBLIC OF CHINA

ICS 91.100.10

CCS Q 27

Replacing JC/T 620-2009

Sampling method for lime

Issued on. MARCH 05, 2021

Implemented on. JULY 01, 2021

Issued by. Ministry of Industry and Information Technology of PRC

Table of Contents

Foreword... 3

1 Scope... 5

2 Normative references... 5

3 Terms and definitions... 5

4 Sampling tools... 6

5 Sampling site and sampling location... 6

6 Total sampling... 7

7 Sampling steps... 7

8 Sample preparation... 9

9 Packaging and storage... 9

10 Sampling sheet... 9

Appendix A (Informative) Lime sampler... 10

Foreword

This document was drafted in accordance with the rules given in GB/T 1.1-2020

"Directives for standardization - Part 1.Rules for the structure and drafting of

standardizing documents"

This document replaces JC/T 620-2009.Compared with JC/T 620-2009, in

addition to structural adjustments and editorial changes, the main technical

changes are as follows.

a) ADD the scope (see Chapter 1);

b) In terms and definitions, CANCEL the "batch", "batch size", "number";

ADD the "automatic sampling" (see Chapter 2);

c) CANCEL the "batch size" (Chapter 4 of the 2009 edition);

d) In the sampling tools, ADD the automatic sampler; MOVE the lime

sampling tube and diagram of sampling shovel into the informative

appendix A; MODIFY the diameter of sampling tube (see Chapter 4; 5.1

of the 2009 edition);

e) COMBINE the sampling site and sampling location; MODIFY the

requirements for sampling location (see Chapter 5; 5.2 and 5.3 of the 2009

edition);

f) MODIFY the "sampling method" into "sampling procedure"; MODIFY the

classification of sampling locations (see Chapter 7; 5.5 of the 2009 edition);

g) MODIFY the packaging and storage (see Chapter 9; 5.7 of the 2009

edition);

h) ADD the Appendix A.

1 Scope

This document specifies the terms and definitions, sampling tools, sampling

sites and locations, total sampling size, sampling procedures, sample

preparation, packaging and storage, sampling sheets, of lime sampling.

This document is applicable to the inspection sampling of the production and

use of quicklime, quicklime powder, slaked lime powder.

2 Normative references

The provisions in following documents become the provisions of this Standard

through reference in this Standard. For the dated documents, only the versions

with the dates indicated are applicable to this document; for the undated

documents, only the latest version (including all the amendments) is applicable

to this standard.

JC/T 619 Terms for lime

3 Terms and definitions

The terms and definitions as defined in JC/T 619, as well as the following terms

and definitions, apply to this document.

3.1

Manual sampling

Collection of lime samples by the use of manual sampling tools.

3.2

Automatic sampling

Collection of lime samples by the use of an autosampler.

3.3

Unit sample

A lime sample, which is taken from a point or part of each inspection lot,

according to the specified amount.

3.4

Composite sample

A sample, which is obtained by taking the specified volume of all the unit

lime samples, that are obtained from an inspection lot, after uniformly and

thoroughly mixing them.

4 Sampling tools

4.1 Material of sampling tool

The sampling tools shall be made of materials, that do not chemically react with

lime, such as stainless steel.

4.4 Autosampler

Used for automatic sampling of powdered lime. Refer to Appendix A.3 for

commonly used autosamplers.

5 Sampling site and sampling location

5.1 The sampling site shall be representative. The sampling shall not be carried

out in rainwater OR in a heavily polluted environment.

5.2 The sampling of lime production inspection should be at the following

locations.

5.3 Sampling for lime use inspection should be at the following locations.

6 Total sampling

The total amount of quicklime, which is sampled for each inspected lime

inspection lot, shall not be less than 24 kg; the total amount of quicklime powder

and slaked lime powder sampled shall not be less than 5 kg.

7 Sampling steps

7.1 Sampling from storage yards, warehouses, vehicles (ships)

Use ordinary pointed steel shovel or I-type manual sampling shovel for

sampling. Randomly select 12 sampling points, from different parts of each

inspection lot.

7.2 Sampling at the inlet and outlet of conveyor belts, lime silos, bulk

trucks

For lumpy lime, use I-type manual sampling shovel or ordinary pointed steel

shovel to take sample. From the flowing quicklime of each inspection lot, take

12 unit samples at regular intervals; each sample is not less than 2 kg. If there

is a large block, which has the largest size greater than 100 mm, in the sampling

point, it shall be processed in accordance with 7.1.

7.3 Sampling at the outlet of the lime kiln

Select the appropriate sampling location, according to the discharge method of

the lime kiln's discharge port AND the lime temperature; proceed according to

7.2.

7.4 Sampling in bags

For bags of lime not more than 100 kg, randomly take 10 bags from each

inspection lot (the bags shall be intact). Use the manual sampling tubes for

sampling. Insert the sampling tube, obliquely from the opening of the bag, to an

appropriate depth, in the bag. Take out a tube of lime. The sampling volume of

each bag of lime shall not be less than 0.5 kg.

8 Sample preparation

8.1 Composite sample

The unit samples, which are obtained from each inspection lot, shall be

uniformly mixed, immediately after unpacking. Use the quartering method to

reduce it.

8.2 Test sample and retained sample

Divide the reduced mixed sample equally, one is the test sample AND the other

is the retained sample.

9 Packaging and storage

9.1 The obtained test sample and retained sample shall be stored immediately

in a clean, dry, moisture-proof container, that does not affect the performance

of lime, AND sealed.

10 Sampling sheet

After the sample is obtained, the person in charge of sampling shall fill in the

sampling sheet. The sampling sheet shall include at least the following.

......

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 10 pages — is available in the English PDF.

Referenced standards

Normative references

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