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GB/T 5195.9-2016Fluorspar - Determination of loss on ignition - Gravimetric method (English PDF)

萤石 灼烧减量的测定 重量法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

December 13, 2016

Implementation date

September 1, 2017

Scope

GB/T 5195.9-2016 is the English-translated version of 萤石 灼烧减量的测定 重量法.

GB/T 5195.9-2016 is the Chinese standard "Fluorspar - Determination of loss on ignition - Gravimetric method". Its scope clause reads: This part of GB/T 5195 specifies the gravimetric determination of the ignition reduction.

This part is applicable to the determination of burning loss in fluorite, the determination range (mass fraction). 0.050% ~ 5.00%. Its clauses include normative reference documents; principle; instruments; samples; analysis steps.

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Document preview — GB/T 5195.9-2016

National Standard of the People's Republic of China

ICS
73.080
Classification
D 52

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • 1 Scope
  • 2 normative reference documents
  • 3 principle
  • 4 instruments
  • 5 samples
  • 6 Analysis steps

1 Scope

This part of GB/T 5195 specifies the gravimetric determination of the ignition reduction.

This part is applicable to the determination of burning loss in fluorite, the determination range (mass fraction). 0.050% ~ 5.00%.

2 normative reference documents

The following documents are indispensable for the application of this document. For dated references, only the dated edition applies to this article

Pieces. For undated references, the latest edition (including all modifications) applies to this document.

GB/T 6379.1 Accuracy of measurement methods and results (accuracy and precision) - Part 1. General and definitions

GB/T 6379.2 Accuracy of measurement methods and results (accuracy and precision) - Part 2. Determination of standard measurement methods

The basic method of sex and reproducibility

Representation and Judgment of Numerical Correction Rule and Limit Value of GB/T 8170

GB/T 22564 fluorite sampling and sample preparation

3 principle

The sample was calcined at 800 ° C to 810 ° C until constant, and the amount of ignition was calculated based on the mass loss.

4 instruments

4.1 Analysis of balance

accurate to 0.1mg.

4.2 muffle furnace

the maximum temperature can reach 1000 °C.

4.3 porcelain crucible

with a lid, the volume of 30mL.

5 samples

The samples were prepared according to the requirements of GB/T 22564, the particle size was less than 150µm, and dried at 105 °C ± 2 °C for 2h,

Room temperature.

6 Analysis steps

6.1 Quantity of sample

Weigh 2,00 g of sample, accurate to 0.0001g.

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

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