GB/T 5195.9-2016Fluorspar - Determination of loss on ignition - Gravimetric method (English PDF)
萤石 灼烧减量的测定 重量法
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Issued by
SAMR; SAC
Level / Type
National · Recommended
Issue date
December 13, 2016
Implementation date
September 1, 2017
Scope
GB/T 5195.9-2016 is the English-translated version of 萤石 灼烧减量的测定 重量法.
GB/T 5195.9-2016 is the Chinese standard "Fluorspar - Determination of loss on ignition - Gravimetric method". Its scope clause reads: This part of GB/T 5195 specifies the gravimetric determination of the ignition reduction.
This part is applicable to the determination of burning loss in fluorite, the determination range (mass fraction). 0.050% ~ 5.00%. Its clauses include normative reference documents; principle; instruments; samples; analysis steps.
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Document preview — GB/T 5195.9-2016
National Standard of the People's Republic of China
- ICS
- 73.080
- Classification
- D 52
Issued by: State Administration for Market Regulation; Standardization Administration of the PRC
Contents
- 1 Scope
- 2 normative reference documents
- 3 principle
- 4 instruments
- 5 samples
- 6 Analysis steps
1 Scope
This part of GB/T 5195 specifies the gravimetric determination of the ignition reduction.
This part is applicable to the determination of burning loss in fluorite, the determination range (mass fraction). 0.050% ~ 5.00%.
2 normative reference documents
The following documents are indispensable for the application of this document. For dated references, only the dated edition applies to this article
Pieces. For undated references, the latest edition (including all modifications) applies to this document.
GB/T 6379.1 Accuracy of measurement methods and results (accuracy and precision) - Part 1. General and definitions
GB/T 6379.2 Accuracy of measurement methods and results (accuracy and precision) - Part 2. Determination of standard measurement methods
The basic method of sex and reproducibility
Representation and Judgment of Numerical Correction Rule and Limit Value of GB/T 8170
GB/T 22564 fluorite sampling and sample preparation
3 principle
The sample was calcined at 800 ° C to 810 ° C until constant, and the amount of ignition was calculated based on the mass loss.
4 instruments
4.1 Analysis of balance
accurate to 0.1mg.
4.2 muffle furnace
the maximum temperature can reach 1000 °C.
4.3 porcelain crucible
with a lid, the volume of 30mL.
5 samples
The samples were prepared according to the requirements of GB/T 22564, the particle size was less than 150µm, and dried at 105 °C ± 2 °C for 2h,
Room temperature.
6 Analysis steps
6.1 Quantity of sample
Weigh 2,00 g of sample, accurate to 0.0001g.
......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.
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