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GB/T 42160-2022Grain boundary diffusion neodymium iron boron permanent magnet materials (English PDF)

晶界扩散钕铁硼永磁材料

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

December 30, 2022

Implementation date

July 1, 2023

Scope

GB/T 42160-2022 is the English-translated version of 晶界扩散钕铁硼永磁材料.

China's national standard for neodymium iron boron permanent magnets made by grain boundary diffusion. The technique addresses the central economic problem of these magnets. A magnet for a traction motor must resist demagnetisation at the temperature the motor runs at, and that coercivity is obtained by substituting dysprosium or terbium for some of the neodymium - heavy rare earths that are scarce, expensive and geographically concentrated even by rare earth standards. But the coercivity is determined at the grain boundaries rather than throughout the grain, so most of the added dysprosium is doing nothing. Grain boundary diffusion applies it to the surface of a finished magnet and diffuses it inward along the boundaries alone, achieving the same coercivity with a fraction of the heavy rare earth. It is the single most consequential process development in permanent magnets in decades, and it is why electric traction motors are affordable.

Document preview — GB/T 42160-2022

National Standard of the People's Republic of China

ICS
77.150.99
Classification
H 65

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • 1 Scope1
  • 2 Normative references1
  • 3 Terms and Definitions1
  • 4 Classification and grade2
  • 4.1 Classification2
  • 4.2 Grade2
  • 4.3 Designation method2
  • 5 Technical requirements2
  • 5.1 Magnetic properties2
  • 5.2 Temperature coefficient of magnetic properties4
  • 5.3 Other physical properties4
  • 5.4 Weightlessness4
  • 5.5 Surface protection4
  • 5.6 Magnetic dipole moment consistency4
  • 5.7 Irreversible loss of magnetic flux at high temperature4
  • 5.8 Appearance quality4
  • 5.9 Size and shape deviation5
  • 6 Test method5
  • 6.1 Magnetic properties5
  • 6.2 Temperature coefficient of magnetic properties5
  • 6.3 Other physical properties5
  • 6.4 Weightlessness5
  • 6.5 Surface protection5
  • 6.6 Consistency of Magnetic Dipole Moment5
  • 6.7 Irreversible loss of magnetic flux at high temperature5
  • 6.8 Appearance quality5
  • 6.9 Size5
  • 6.10 Numerical rounding off6
  • 7 Inspection rules6
  • 7.1 Inspection classification6
  • 7.2 Batch6
  • 7.3 Inspection item6
  • 7.4 Sampling method for product factory inspection6
  • 7.5 Inspection result judgment and repeated inspection rules6
  • 8 Packaging, marking, transportation, storage and accompanying documents6
  • 8.1 Packaging, marking, transportation and storage6
  • 12 Appendix E (informative) Consistency of magnetic dipole moment, size and shape deviation of grain boundary diffused NdFeB permanent magnets13

Foreword

This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for Standardization Work Part

1.Structure and Drafting Rules for Standardization Documents" drafting. Please note that some contents of this document may refer to patents. The issuing agency of this document assumes no responsibility for identifying patents. This document is proposed and managed by the National Rare Earth Standardization Technical Committee (SAC/TC229). This document was drafted by: Ningbo Yunsheng Co., Ltd., Beijing Zhongke Sanhuan High-tech Co., Ltd., Anhui Earth Bear New Materials Co., Ltd., Ningbo Zhaobao Magnetic Industry Co., Ltd., Beijing University of Technology, Baotou Tianhe Magnetic Technology Co., Ltd., Ningbo Permanent Magnetic Industry Co., Ltd., Hangzhou Magnetic Technology Co., Ltd., Youyan Rare Earth New Materials Co., Ltd., Fujian Changting Jinlong Rare Earth Co., Ltd., China Academy of Sciences Ningbo Institute of Materials Technology and Engineering, Baotou Rare Earth Research Institute, Ganzhou Fuerte Electronics Co., Ltd., China North Rare Earth (Group) Group) High Technology Co., Ltd. The main drafters of this document. Lu Xiangke, Shen Guodi, Zhang Min, Zhu Xiaodong, Liang Fengji, Cao Shuohao, Liu Youyou, He Qijun, Yue Ming, Dong Yi, He Ting, Jia Shengli, Luo Yang, Zhang Jiulei, Song Zhenlun, Ding Yong, Fu Jianlong, Qi Zhiqi, Lou Shupu, Liu Feng, Ouyang Xike, Huang Xiulian, Lin Jianqiang, Liu Weiqiang, Wu Shujie, Li Jianzhong, Yan Wenlong, Yang Lijing, Jiang Jianjun, Sun Yingli, Pang Zaisheng. Grain Boundary Diffusion NdFeB Permanent Magnets

1 Scope

China's national standard for neodymium iron boron permanent magnets made by grain boundary diffusion. The technique addresses the central economic problem of these magnets. A magnet for a traction motor must resist demagnetisation at the temperature the motor runs at, and that coercivity is obtained by substituting dysprosium or terbium for some of the neodymium - heavy rare earths that are scarce, expensive and geographically concentrated even by rare earth standards. But the coercivity is determined at the grain boundaries rather than throughout the grain, so most of the added dysprosium is doing nothing. Grain boundary diffusion applies it to the surface of a finished magnet and diffuses it inward along the boundaries alone, achieving the same coercivity with a fraction of the heavy rare earth. It is the single most consequential process development in permanent magnets in decades, and it is why electric traction motors are affordable.

This document specifies the classification and designation, technical requirements, test methods, inspection rules, and packaging, Signage, transport, storage and accompanying documents. This document is applicable to sintered NdFeB permanent magnet materials treated by grain boundary diffusion process.

2 Normative references

The contents of the following documents constitute the essential provisions of this document through normative references in the text. Among them, dated references For documents, only the version corresponding to the date is applicable to this document; for undated reference documents, the latest version (including all amendments) is applicable to this document.

GB/T 2828.1-2012 Counting sampling inspection procedure Part

1.Batch-by-batch inspection sampling retrieved by acceptance quality limit (AQL) plan

GB/T 3217 Magnetic test methods for permanent magnet (hard magnetic) materials

GB/T 3850 Density Determination Method for Dense Sintered Metal Materials and Cemented Carbide

GB/T 4339 Determination of thermal expansion characteristic parameters of metallic materials

GB/T 5167 Determination of resistivity of sintered metal materials and cemented carbide

GB/T 7314 Compression test method for metallic materials at room temperature

GB/T 8170 Numerical rounding off rules and expression and determination of limit values

GB/T 9097 Determination of apparent hardness and microhardness of sintered metal materials (excluding cemented carbide)

GB/T 9637 Electrotechnical Terminology Magnetic Materials and Components

GB/T 13560 Sintered NdFeB permanent magnet materials

GB/T 22315-2008 Test method for elastic modulus and Poisson's ratio of metallic materials

GB/T 22588 Flash method for measuring thermal diffusivity or thermal conductivity

3 Terms and Definitions

The following terms and definitions defined in GB/T 9637 and GB/T 13560 apply to this document.

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 17 pages — is available in the English PDF.

Referenced standards

Normative references

GB/T 3217 · GB/T 3850 · GB/T 4339 · GB/T 9097 · GB/T 9637 · GB/T 29628 · GB/T 38437

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