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GB/T 40906-2021Methods for the determination of prohibited substances in furniture products and related materials—Certain phthalate esters (English PDF)

家具产品及其材料中禁限用物质测定方法 邻苯二甲酸酯增塑剂

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

October 11, 2021

Implementation date

May 1, 2022

Scope

GB/T 40906-2021 is the English-translated version of 家具产品及其材料中禁限用物质测定方法 邻苯二甲酸酯增塑剂.

GB/T 40906-2021 is a Chinese national test method for six phthalate plasticizers treated as prohibited or restricted substances in furniture products and the materials they are made of.

The phthalates are extracted from the sample with dichloromethane in a Soxhlet extractor or an ultrasonic generator, and the extract is brought to volume and analysed by gas chromatography/mass spectrometry.

The document defines phthalates, lists the six compounds in a table and sets out the reagents, including dichloromethane and reference materials of at least 95% purity, with grade three water to GB/T 6682.

Other phthalate plasticizers can also be tested following the same method once it has been verified for them. It was issued on 11 October 2021 and has applied since 1 May 2022.

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Document preview — GB/T 40906-2021

National Standard of the People's Republic of China

ICS
97.140
Classification
Y 80

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Foreword
  • 1 Scope
  • 2 Normative references
  • 3 Terms and definitions
  • 4 Principle
  • 5 Reagents or materials

Foreword

This document is in accordance with the provisions of GB/T 1.1-2020 "Guidelines for Standardization Work Part 1: Structure and Drafting Rules of Standardization Documents" Drafting.

1 Scope

This document describes the gas chromatography/mass spectrometry method for the determination of six phthalate plasticizers in furniture products and their materials.

The test of diformate plasticizer can also be carried out with reference to this document after verification.

This document is applicable to the determination of 6 phthalate plasticizers in furniture products and their materials.

2 Normative references

The contents of the following documents constitute the indispensable clauses of this document through normative references in the text. Among them, dated quotations Only the version corresponding to that date is applicable to this document; for undated reference documents, the latest version (including all amendments) is applicable to this document.

GB/T 6682 Analytical laboratory water specifications and test methods

3 Terms and definitions

The following terms and definitions apply to this document.

3.1 Phthalates

The general term for esters formed by the reaction of phthalic acid and alcohol. Its chemical structure is characterized by two symmetrical or asymmetric methyl esters at the ortho position of the benzene ring. Acid hydrocarbon ester.

Note: The 6 phthalates in this document are shown in Table 1.

4 Principle

Use methylene chloride to extract the phthalates in the sample in a Soxhlet extractor or ultrasonic generator, and extract After the liquid is constant volume, use gas chromatography/mass spectrometry for analysis and determination.

5 Reagents or materials

The test water should conform to the third grade water specified in GB/T 6682.

5.1 Dichloromethane

Analytical or chromatographically pure.

5.2 Phthalates standard materials

The purity is not less than 95%, see Table 1.

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

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