GB/T 3914-2008Chemical reagent - The general rules of anodic stripping voltammetry (English PDF)

3.1

The substrate of the working electrode is an inert material having good conductive properties of the finished solid having a certain shape and a certain surface area

Quality, the metal may be used as the working electrode in the form of thin films is fixed on a certain surface area thereof. Fixing methods are applied, pre-electrolysis

Plating and coating methods such as parity.

3.2

Adding a certain concentration in the sample solution as determined For the metal compound film, measured in the pre-electrolysis, is formed on the substrate

Thin film, the film as a working electrode to be measured was the pre-electrolytic enrichment on it, back when freed entirely from the substrate solution.

3.3

Dissolve the sample for measurement of anodic stripping voltammetry solvent.

3.4

In determining the potential and stirring conditions under which a certain time, the part to be measured was enriched to the electrolytic membrane electrode.

3.5

After the pre-electrolysis, stirring for a certain time to stop using potential measurement potential from negative to positive, according to a certain scanning rate changes linearly. this

Determination is the pre-electrolytic enrichment was to be measured to the dissolution of the membrane electrode on record its stripping voltammetry curves.