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GB/T 36058-2018Method for analysis of forestry biomas—Determination of insoluble saccharides content (English PDF)

林业生物质原料分析方法 不可溶性糖测定

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

March 15, 2018

Implementation date

October 1, 2018

Scope

GB/T 36058-2018 is the English-translated version of 林业生物质原料分析方法 不可溶性糖测定.

GB/T 36058-2018 gives a method for determining the insoluble saccharides content of forestry biomass raw materials, meaning the water-insoluble carbohydrates such as cellulose and most hemicelluloses.

The insoluble sugars are converted to monosaccharides by a two-stage sulfuric acid hydrolysis, the monosaccharides are measured by high performance liquid chromatography (HPLC), and the insoluble sugar content is calculated from them.

The standard covers the reagents and materials, instruments, sample preparation, test procedure, data processing, precision and test report. With a 20 µL injection, the detection limits are 8 mg/L for glucose, 14 mg/L for xylose, 28 mg/L for arabinose, 10 mg/L for galactose and 16 mg/L for mannose.

It relies on the national methods for sampling forestry biomass, preparing samples and determining moisture. It was issued on 15 March 2018 and has applied since 1 October 2018.

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Document preview — GB/T 36058-2018

National Standard of the People's Republic of China

ICS
79.010
Classification
B 60

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Foreword
  • 1 Scope
  • 2 Normative references
  • 3 Terms and definitions
  • 4 Principle

Foreword

This standard was drafted in accordance with the rules given in GB/T 1.1-2009.

1 Scope

This standard specifies the terms and definitions, principles, reagents and materials, instruments and equipment for the determination of insoluble sugar content in forestry biomass raw materials. Sample preparation, test procedures, test data processing, precision requirements, and test reports.

This standard applies to the determination of insoluble sugar content in forestry biomass raw materials.

When the injection volume was 20 µL, the detection limit (S/N >= 3) of the method was. glucose 8 mg/L, xylose 14 mg/L, Arabinose 28 mg/L, galactose 10 mg/L, and mannose 16 mg/L.

2 Normative references

The following documents are indispensable for the application of this document. For dated references, only dated versions apply to this document. For undated references, the latest version (including all amendments) applies to this document.

GB/T 2677.6-1994 Determination of extractables content of organic solvent in papermaking raw materials

GB/T 30366-2013 biomass terminology

GB/T 35814-2018 Analysis of forestry biomass feedstock sample processing methods

GB/T 35820-2018 forestry biomass raw material analysis method sampling method

GB/T 36055-2018 Analysis method of forestry biomass feedstock moisture content determination

3 Terms and definitions

The terms and definitions defined in GB/T 30336-2013 and the following apply to this document. For ease of use, the following is repeated Some terms and definitions in GB/T 30366-2013.

3.1 Forestry biomass

Biomass produced during forestry production and processing. Mainly include forest products (such as wood, bamboo, rattan, etc.) and forestry residues (such as branches Slag, sawdust, sawdust, shoots, slats and truncated, husks and kernels and other processing residues and processing residues, paper-making waste, and waste wood), Energy forest and so on. [GB/T 30336-2013, definition 2.1.3]

3.2 Insoluble sugars

The (heat) water-insoluble carbohydrates in forestry biomass feedstocks include cellulose and most hemicelluloses.

4 Principle

The insoluble sugars in the forestry biomass feedstock can be converted to the corresponding monosaccharides by two stages of sulfuric acid hydrolysis. High performance liquid chromatography (HPLC) After the monosaccharide content was measured, the insoluble sugar content in the forestry biomass material was calculated.

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This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

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