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GB/T 34764-2017Determination of copper,iron,zinc,manganese,boron and molybdenum content in fertilizers - Inductively coupled plasma optical emission spectroscopy (English PDF)

肥料中铜、铁、锰、锌、硼、钼含量的测定 等离子体发射光谱法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

November 1, 2017

Implementation date

May 1, 2018

Scope

GB/T 34764-2017 is the English-translated version of 肥料中铜、铁、锰、锌、硼、钼含量的测定 等离子体发射光谱法.

GB/T 34764-2017 is the Chinese standard "Determination of copper,iron,zinc,manganese,boron and molybdenum content in fertilizers - Inductively coupled plasma optical emission spectroscopy".

Its scope clause reads: This standard specifies the method of determination of copper, iron, manganese, zinc, boron, molybdenum content of fertilizer by plasma emission spectrometry (ICP).

This standard applies to copper, iron, manganese, zinc, boron, molybdenum content <= 1% of the fertilizer. The detection limit of this standard method of copper 0.003µg/mL, iron 0.03µg/mL, manganese 0.004µg/mL, zinc 0.03µg/mL, boron 0.05 µg/mL, molybdenum 0.007 µg/mL. Its clauses include principle; reagents and materials.

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Document preview — GB/T 34764-2017

National Standard of the People's Republic of China

ICS
65.080
Classification
G 20

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • 1 Scope
  • 2 Normative references
  • 3 principle
  • 4 Reagents and materials

1 Scope

This standard specifies the method of determination of copper, iron, manganese, zinc, boron, molybdenum content of fertilizer by plasma emission spectrometry (ICP).

This standard applies to copper, iron, manganese, zinc, boron, molybdenum content <= 1% of the fertilizer.

The detection limit of this standard method of copper 0.003µg/mL, iron 0.03µg/mL, manganese 0.004µg/mL, zinc 0.03µg/mL, boron

0.05 µg/mL, molybdenum 0.007 µg/mL.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version applies to this article

Pieces. For undated references, the latest edition (including all amendments) applies to this document.

GB/T 6682 analytical laboratory water specifications and test methods

Determination of copper, iron, manganese, zinc, boron and molybdenum content in compound fertilizers GB/T 14540-2003

GB/T 17767.3-2010 Determination of organic - inorganic compound fertilizers - Part 3. Total potassium content

3 principle

Copper, iron, manganese, zinc, boron, molybdenum in sample solution atomize in ICP light source and excite to high energy state,

To the ground state has a characteristic wavelength of electromagnetic radiation, radiation intensity and atomic concentration is proportional to.

4 Reagents and materials

Warning --- personnel using this standard should have formal laboratory work experience. This standard does not indicate all possible safety issues question. It is the user's responsibility to take appropriate safety and health measures and to ensure compliance with the requirements of the relevant state laws and regulations.

4.1

Unless otherwise specified, only the reagents identified as analytical grade are used in the analysis. The pH range and conductivity of water should be in accordance with GB/T 6682

Three in the water specifications.

4.2

hydrochloric acid solution .1 1, prepared using excellent grade pure hydrochloric acid.

4.3 Argon

Purity greater than 99.99%.

4.4

copper standard solution .100µg/mL, commercially available certified standard solution or prepared with a certified reference material.

4.5

iron standard solution .100µg/mL, a certified standard solution on the market or with certified reference material preparation.

4.6

Manganese standard solution .100µg/mL, commercially available certified standard solution or prepared with certified reference material.

4.7

Zinc standard solution .100µg/mL, commercially available certified standard solution or certified reference material preparation.

4.8

Boron standard solution .100µg/mL, a commercially available certified standard solution or certified reference material preparation.

4.9

Molybdenum standard solution .100µg/mL, a commercially available certified standard solution or prepared with a certified reference material.

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

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