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GB/T 34723-2017Residual styrene monomer content determination in unsaturated polyester decorative wood-based panels by gas chromatography (English PDF)

不饱和聚酯树脂装饰人造板残留苯乙烯单体含量测定 气相色谱法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

November 1, 2017

Implementation date

May 1, 2018

Scope

GB/T 34723-2017 is the English-translated version of 不饱和聚酯树脂装饰人造板残留苯乙烯单体含量测定 气相色谱法.

GB/T 34723-2017 gives the gas chromatographic method for determining the residual styrene monomer content of unsaturated polyester decorative wood-based panels.

Clause 1 states that the standard specifies that determination and that it applies to the determination of residual styrene monomer content in unsaturated polyester resin decorative panels used in interior decoration, furniture, doors and musical instruments.

The title page and the foreword record that the standard was prepared with reference to ISO 4901-2011, on the determination by gas chromatography of the residual styrene monomer content as well as the content of other volatile aromatic hydrocarbons in reinforced plastics, and that its consistency with ISO 4901-2011 is not equivalent.

Clause 3 takes its terms from GB/T 4946 and adds the unsaturated polyester resin decorative wood-based panel, taken from definition 3.1 of LY/T 1070-2013 as a panel made by coating a wood-based substrate, such as plywood, fibreboard, particleboard or blockboard, with decorative paper or veneer on one or both sides and then with unsaturated polyester resin which is cured, and the residual styrene monomer content, meaning the styrene monomer left unreacted during processing.

Clause 4 states the principle: the residual styrene monomer is extracted from the unsaturated polyester resin polymer with methylene chloride, and the styrene monomer content of the extract is determined by gas chromatography using the internal standard method and the standard curve method.

Clause 5 opens with a warning on the toxicity of dichloromethane, requires the reagents to be given a blank test before use to confirm that no interfering peaks appear in the retention time interval of the target, and specifies nitrogen or helium of purity not less than 99.995 % as the carrier gas and hydrogen of the same purity.

The draft breaks off there and the page gives no table of contents, so the apparatus, the procedure and the calculation clauses are not shown. The standard carries ICS 79.060.01 and Chinese classification B70, was proposed by the State Forestry Administration and is kept by the National Panel Standardization Technical Committee (SAC/TC198). It was issued on 1 November 2017 and has applied since 1 May 2018.

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Document preview — GB/T 34723-2017

National Standard of the People's Republic of China

ICS
79.060.01
Classification
B 70

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Foreword
  • 1 Scope
  • 2 Normative references
  • 3 Terms and definitions GB/T 4946 defined and the following
  • 4 Principle
  • 5 Reagent

Foreword

This standard was drafted in accordance with the rules given in GB/T 1.1-2009.

This standard reference ISO 4901-2011 "Unsaturated polyester resin reinforced plastics by gas chromatography analysis of residual styrene monomer Content and other volatile aromatic content "preparation. Consistency with ISO 4901-2011 is not equivalent.

1 Scope

This standard specifies the content of residual styrene monomer in unsaturated polyester resin decorative man-made board finishes by gas chromatography.

This standard applies to interior decoration, furniture, doors and musical instruments such as the use of unsaturated polyester resin decorative plywood residue in benzene Determination of vinyl monomer content.

2 Normative references

The following documents for the application of this document is essential. For dated references, only the dated version applies to this document. For undated references, the latest edition (including all amendments) applies to this document.

GB/T 4946 gas chromatography terminology

LY/T 1070-2013 Unsaturated polyester resin decorative panel

3 Terms and definitions

GB/T 4946 defined and the following terms and definitions apply to this document.

3.1 Unsaturated polyester resin decorative plywood

To plywood (plywood, fiberboard, particleboard, blockboard, etc.) as the substrate, the substrate coated with decorative paper or single or double-sided After the board (veneer), and then coated with unsaturated polyester resin, the cured (ie, coating) made of sheet. [LY/T 1070-2013, Definition 3.1]

3.2 Residual styrene monomer content

Unsaturated polyester resin decorative wood-based panels unreacted during processing completely styrene monomer content.

4 Principle

The residual styrene monomer is extracted from the unsaturated polyester resin polymer with methylene chloride, and the content of the styrene monomer in the extract The gas chromatography internal standard method and the standard curve method were used for the determination.

5 Reagent

Dichloromethane is toxic and can cause damage to the central nervous system, liver, cardiovascular system and blood if it is swallowed, inhaled or absorbed through the skin Liquid, irritating to the skin, eyes and respiratory tract as well as carcinogenic risk depending on the level and duration of exposure.

5.1 The reagents used in this standard need to undergo a blank test prior to use, to confirm that the target retention time interval without interference peaks appear.

5.2 Carrier gas. Nitrogen or helium, purity >=99.995%.

5.3 Gas. Hydrogen, purity >=99.995%.

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

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