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GB/T 33069-2016Determination of 1-vinyl-2-pyrrolidinone homopolymer for industrial use (English PDF)

工业用聚N-乙烯基吡咯烷酮检测方法

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

October 13, 2016

Implementation date

May 1, 2017

Scope

GB/T 33069-2016 is the English-translated version of 工业用聚N-乙烯基吡咯烷酮检测方法.

GB/T 33069-2016 is the Chinese standard "Determination of 1-vinyl-2-pyrrolidinone homopolymer for industrial use". Its scope clause reads: This standard specifies the appearance, identification, K value, NVP residual monomer, moisture, solid content, pH value of industrial poly (N-vinylpyrrolidone) Value and sulfate ash detection method.

This standard applies to N-vinyl pyrrolidone (hereinafter referred to as NVP) monomer by solution polymerization made of industrial poly N-vinyl Pyrrolidone (hereinafter referred to as PVP) linear polymer. Its clauses include normative reference documents; reagent; test method.

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Document preview — GB/T 33069-2016

National Standard of the People's Republic of China

ICS
71.080.80
Classification
G 31

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • 1 Scope
  • 2 normative reference documents
  • 3 reagent
  • 4 test method

1 Scope

This standard specifies the appearance, identification, K value, NVP residual monomer, moisture, solid content, pH value of industrial poly (N-vinylpyrrolidone)

Value and sulfate ash detection method.

This standard applies to N-vinyl pyrrolidone (hereinafter referred to as NVP) monomer by solution polymerization made of industrial poly N-vinyl

Pyrrolidone (hereinafter referred to as PVP) linear polymer.

2 normative reference documents

The following documents are indispensable for the application of this document. For dated references, only the dated edition applies to this article

Pieces. For undated references, the latest edition (including all modifications) applies to this document.

Preparation of standard titration solution for GB/T 601 chemical reagents

Preparation of preparations and preparations for use in the test methods for chemical reagents GB/T 603

GB/T 6283 Determination of moisture content in chemical products Karl Fischer method (general method)

GB/T 6682 Analytical laboratory water specifications and test methods

General rules for the determination of pH value of chemical reagents GB/T 9724

3 reagent

Unless otherwise noted, the reagents used are analytical reagents, water are in line with GB/T 6682 provisions of the three water specifications, the standard used

Titration solution, preparation and products, according to GB/T 601, GB/T 603 provisions of the preparation, if the use of other levels of reagents, with its purity will not

Reduce the accuracy of the test shall prevail.

4 test method

4.1 appearance

4.1.1 Solid Specimen

Visualized in indoor natural light.

4.1.2 Liquid sample

Take 50mL ~ 60mL sample, placed in a clean, dry 100mL test tube, under the indoor natural light visual inspection.

4.2 Identification

4.2.1 solution
4.2.1.1 iodine test solution

take 13.0g iodine and 35.0g potassium iodide, dissolved in 100mL water, diluted to 1000mL, shake, stored in brown

Bottle.

4.2.1.2 hydrochloric acid solution

measure the amount of 117mL hydrochloric acid, placed in 1000mL reagent bottle, diluted with water to 1000mL.

4.2.1.3 Potassium dichromate test solution

Weigh 7.5g potassium dichromate, add water to dissolve and dilute to 100mL.

4.2.1.4 cobalt nitrate test solution

Weigh 2.0g cobalt nitrate, diluted with water diluted to 100mL.

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

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