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GB/T 2969-2020Samarium oxide (English PDF)

氧化钐

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Issued by

SAMR; SAC

Level / Type

National · Recommended

Issue date

September 29, 2020

Implementation date

August 1, 2021

Scope

GB/T 2969-2020 is the English-translated version of 氧化钐.

GB/T 2969-2020 is the Chinese national product standard for samarium oxide.

It sorts the oxide into the five grades Sm2O3-4N, Sm2O3-3N5, Sm2O3-3N, Sm2O3-2N5 and Sm2O3-2N, designated under GB/T 17803, and fixes for each the total rare earth oxide content, the relative purity Sm2O3/REO from 99.0 % up to 99.99 %, the limits on rare earth impurities such as praseodymium, neodymium, europium, gadolinium and yttrium, the non-rare earth impurities, and a combined moisture and loss on ignition figure.

Analysis follows GB/T 14635, GB/T 18115.5 and GB/T 12690, and inspection rules, marking, packaging, transport, storage and the quality certificate complete it. It covers oxide made by extraction or other routes for samarium metal, magnetic materials and electronic components.

It replaces GB/T 2969-2008, was issued on 29 September 2020 and has applied since 1 August 2021.

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Document preview — GB/T 2969-2020

National Standard of the People's Republic of China

ICS
77.120.99
Classification
H 65
Replacing
GB/T 2969-2008

Issued by: State Administration for Market Regulation; Standardization Administration of the PRC

Contents

  • Foreword
  • 1 Scope
  • 2 Normative references
  • 3 Technical requirements

Foreword

This standard was drafted in accordance with the rules given in GB/T 1.1-2009.

This standard replaces GB/T 2969-2008 "Samarium Oxide". Compared with GB/T 2969-2008, the main technical changes except for editorial changes Change as follows.

---Added character brand (see 3.1 and 3.2);

---Modified the assessment index of the rare earth impurity praseodymium and total amount in the grade Sm2O3-4N, and adjusted the non-rare earth impurities Fe2O3 and SiO2 The evaluation indicators (see 3.2, 3.1 of the 2008 edition);

---Added the grade Sm2O3-3N5 (see 3.2);

---Modified some non-rare earth impurities of the grades Sm2O3-2N5 and Sm2O3-2N (see 3.2, 3.1 in the 2008 edition);

---Added the assessment index and calculation method of the main rare earth element Sm2O3 (see 3.2);

--- Modified rare earth impurities, deleted the denominator REO (see 3.2, 3.1 in the 2008 edition);

---The burning loss index is modified as the combined amount index of moisture and burning loss (see 3.2, 3.1 in the 2008 edition);

---Added the note that all tests are the state before burning after removing water (see 3.2);

---Modified the analysis method of the total content of rare earths (REO), and added that when the total amount of rare earths measured is more than 99%, the rare earths are calculated by the subtraction method.

The actual value of the total amount of soil (see 4.1.1, 4.1 in the 2008 edition);

---The calculation method of the relative purity of the main rare earth elements (Sm2O3/REO) has been increased, that is, the amount of the main rare earth elements/the total rare earth elements × 100% (see 4.1.5);

--- Added the requirement that when the appearance inspection result does not conform to this standard, the batch of products is directly judged as non-conforming product (see 5.5.2).

1 Scope

This standard specifies the technical requirements, test methods, inspection rules, signs, packaging, transportation, storage and quality certificates of samarium oxide.

This standard applies to samarium oxide prepared by extraction or other methods for the production of metal samarium, magnetic materials, electronic components, etc.

2 Normative references

The following documents are indispensable for the application of this document. For dated reference documents, only the dated version applies to this document. For undated references, the latest version (including all amendments) applies to this document.

GB/T 8170 Numerical rounding rules and the expression and determination of limit values

GB/T 12690 (all parts) Chemical analysis methods for non-rare earth impurities in rare earth metals and their oxides

GB/T 14635 Methods for chemical analysis of rare earth metals and their compounds Determination of total rare earth

GB/T 17803 Rare earth product designation method

GB/T 18115.5 Methods for chemical analysis of rare earth impurities in rare earth metals and their oxides. Lanthanum, cerium, praseodymium, neodymium, europium, gadolinium, terbium, samarium Determination of the amount of dysprosium, holmium, erbium, thulium, ytterbium, lutetium and yttrium

3 Technical requirements

3.1 Product Classification

The products are divided into five grades of Sm2O3-4N, Sm2O3-3N5, Sm2O3-3N, Sm2O3-2N5, Sm2O3-2N according to their chemical composition. The method of designation should comply with GB/T 17803.

3.2 Chemical composition

The chemical composition of the product should meet the requirements of Table 1. If the buyer has special requirements, the supplier and the buyer can negotiate separately.

Product brand Character brand Sm2O3-4N Sm2O3-3N5 Sm2O3-3N Sm2O3-2N5 Sm2O3-2N Corresponding to the original digital brand 061040 061035 061030 061025 061020 Chemistry ingredient (quality fraction)/ REO, >= 99.0 Sm2O3/REO, >= 99.99 Sm2O3 margina Impurities content, Rare earth Impurities Pr6O11 0.0010 Nd2O3 0.0035 Eu2O3 0.0010 Gd2O3 0.0010 Y2O3 0.0010 Other rare earths Total impurity b 0.0025 99.0 99.0 99.0 99.0 99.95 99.9 99.5 99.0 Margin a Margin a Margin a Margin a The total amount is 0.05, where Eu2O3 is less than

Total amount 0.1 Total amount 0.5 Total amount 1.0 […]

......
This preview omits tables, figures, formulas and parts of the technical clauses. The complete document — 15 pages — is available in the English PDF.

Referenced standards

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Editions of GB/T 2969

EditionTitleRevisionStatus
GB/T 2969-2020Samarium oxidecurrent editionCurrent
GB/T 2969-2008Samarium oxideprevious editionSuperseded

This page sells the current edition, GB/T 2969-2020. Earlier editions are listed for reference only.

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